Single-faceted IrO2 monolayer enabling high-performing proton exchange membrane water electrolysis beyond 10,000 h stability at 1.5 A cm-2

Abstract Both commercial and laboratory-synthesized IrO2 catalysts typically possess rutile-type structures with multiple facets. Theoretical results predict the (101) facet is the most energetically favorable for oxygen evolution reaction owing to its lowest energy barrier. Achieving monolayer thic...

Full description

Saved in:
Bibliographic Details
Main Authors: Deren Yang, Chunyang Zhang, Yufeng Qin, Yang Yue, Yubo Liu, Xiaoyun Shi, Kang Hua, Xuemin An, Louyu Jin, Yipeng Zhang, Shouwei Zuo, Aidong Tan, Jianguo Liu
Format: Article
Language:English
Published: Nature Portfolio 2025-08-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-025-62665-2
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849234638048854016
author Deren Yang
Chunyang Zhang
Yufeng Qin
Yang Yue
Yubo Liu
Xiaoyun Shi
Kang Hua
Xuemin An
Louyu Jin
Yipeng Zhang
Shouwei Zuo
Aidong Tan
Jianguo Liu
author_facet Deren Yang
Chunyang Zhang
Yufeng Qin
Yang Yue
Yubo Liu
Xiaoyun Shi
Kang Hua
Xuemin An
Louyu Jin
Yipeng Zhang
Shouwei Zuo
Aidong Tan
Jianguo Liu
author_sort Deren Yang
collection DOAJ
description Abstract Both commercial and laboratory-synthesized IrO2 catalysts typically possess rutile-type structures with multiple facets. Theoretical results predict the (101) facet is the most energetically favorable for oxygen evolution reaction owing to its lowest energy barrier. Achieving monolayer thickness while exposing this desired facet is a significant opportunity for IrO2. Herein, we develop an ammonia-induced facet engineering for the synthesis of single-faceted IrO2(101) monolayer. It achieves 230 mV overpotential at 10 mA cmgeo -2 in a three-electrode system and 1.70 V at 2 A cmgeo -2 in a proton exchange membrane (PEM) electrolyzer. Though facet engineering primarily contributes to modulating the intrinsic activity rather than stability, single-faceted IrO2 monolayer performs over 10,000-hour stability at constant 1.5 A cmgeo -2 (3.95 mV kh-1 decay) and 1000-hour stability at 0.2 mgIr cmgeo -2 under fluctuating conditions. This work proposes that ammonia-induced facet engineering of IrO2 monolayer enables facet-dependent oxygen evolution reaction (OER) performance and high stability in industrial-scale PEM electrolysis.
format Article
id doaj-art-99371ca35cb74175aa80919726f90ea7
institution Kabale University
issn 2041-1723
language English
publishDate 2025-08-01
publisher Nature Portfolio
record_format Article
series Nature Communications
spelling doaj-art-99371ca35cb74175aa80919726f90ea72025-08-20T04:03:06ZengNature PortfolioNature Communications2041-17232025-08-0116111610.1038/s41467-025-62665-2Single-faceted IrO2 monolayer enabling high-performing proton exchange membrane water electrolysis beyond 10,000 h stability at 1.5 A cm-2Deren Yang0Chunyang Zhang1Yufeng Qin2Yang Yue3Yubo Liu4Xiaoyun Shi5Kang Hua6Xuemin An7Louyu Jin8Yipeng Zhang9Shouwei Zuo10Aidong Tan11Jianguo Liu12Beijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of SciencesBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadBeijing Laboratory of New Energy Storage Technology, Institute of Energy Power Innovation, North China Electric Power University, 2 Beinong RoadAbstract Both commercial and laboratory-synthesized IrO2 catalysts typically possess rutile-type structures with multiple facets. Theoretical results predict the (101) facet is the most energetically favorable for oxygen evolution reaction owing to its lowest energy barrier. Achieving monolayer thickness while exposing this desired facet is a significant opportunity for IrO2. Herein, we develop an ammonia-induced facet engineering for the synthesis of single-faceted IrO2(101) monolayer. It achieves 230 mV overpotential at 10 mA cmgeo -2 in a three-electrode system and 1.70 V at 2 A cmgeo -2 in a proton exchange membrane (PEM) electrolyzer. Though facet engineering primarily contributes to modulating the intrinsic activity rather than stability, single-faceted IrO2 monolayer performs over 10,000-hour stability at constant 1.5 A cmgeo -2 (3.95 mV kh-1 decay) and 1000-hour stability at 0.2 mgIr cmgeo -2 under fluctuating conditions. This work proposes that ammonia-induced facet engineering of IrO2 monolayer enables facet-dependent oxygen evolution reaction (OER) performance and high stability in industrial-scale PEM electrolysis.https://doi.org/10.1038/s41467-025-62665-2
spellingShingle Deren Yang
Chunyang Zhang
Yufeng Qin
Yang Yue
Yubo Liu
Xiaoyun Shi
Kang Hua
Xuemin An
Louyu Jin
Yipeng Zhang
Shouwei Zuo
Aidong Tan
Jianguo Liu
Single-faceted IrO2 monolayer enabling high-performing proton exchange membrane water electrolysis beyond 10,000 h stability at 1.5 A cm-2
Nature Communications
title Single-faceted IrO2 monolayer enabling high-performing proton exchange membrane water electrolysis beyond 10,000 h stability at 1.5 A cm-2
title_full Single-faceted IrO2 monolayer enabling high-performing proton exchange membrane water electrolysis beyond 10,000 h stability at 1.5 A cm-2
title_fullStr Single-faceted IrO2 monolayer enabling high-performing proton exchange membrane water electrolysis beyond 10,000 h stability at 1.5 A cm-2
title_full_unstemmed Single-faceted IrO2 monolayer enabling high-performing proton exchange membrane water electrolysis beyond 10,000 h stability at 1.5 A cm-2
title_short Single-faceted IrO2 monolayer enabling high-performing proton exchange membrane water electrolysis beyond 10,000 h stability at 1.5 A cm-2
title_sort single faceted iro2 monolayer enabling high performing proton exchange membrane water electrolysis beyond 10 000 h stability at 1 5 a cm 2
url https://doi.org/10.1038/s41467-025-62665-2
work_keys_str_mv AT derenyang singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT chunyangzhang singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT yufengqin singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT yangyue singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT yuboliu singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT xiaoyunshi singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT kanghua singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT xueminan singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT louyujin singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT yipengzhang singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT shouweizuo singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT aidongtan singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2
AT jianguoliu singlefacetediro2monolayerenablinghighperformingprotonexchangemembranewaterelectrolysisbeyond10000hstabilityat15acm2