Synthesis and Characterization of TiO<sub>2</sub> Nanotubes for High-Performance Gas Sensor Applications

In this study, we investigated the fabrication, properties, and sensing applications of TiO<sub>2</sub> nanotubes. A pure titanium metal sheet was used to demonstrate how titanium dioxide nanotubes can be used for gas-sensing applications through the electrochemical anodization method. S...

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Bibliographic Details
Main Authors: Belgacem Bouktif, Marzaini Rashid, Anouar Hajjaji, Karim Choubani, Nashmi H. Alrasheedi, Borhen Louhichi, Wissem Dimassi, Mohamed Ben Rabha
Format: Article
Language:English
Published: MDPI AG 2024-10-01
Series:Crystals
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Online Access:https://www.mdpi.com/2073-4352/14/11/928
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Summary:In this study, we investigated the fabrication, properties, and sensing applications of TiO<sub>2</sub> nanotubes. A pure titanium metal sheet was used to demonstrate how titanium dioxide nanotubes can be used for gas-sensing applications through the electrochemical anodization method. Subsequently, X-ray diffraction indicated the crystallization of the titanium dioxide layer. Scanning electron microscopy and transmission electron microscopy then revealed the average diameter of the TiO<sub>2</sub> nanotubes to be approximately 100 nm, with tube lengths ranging between 3 and 9 µm and the thickness of the nanotube walls being about 25 nm. This type of TiO<sub>2</sub> nanotube was found to be suitable for NO<sub>2</sub> gas sensor applications. With an oxidation time of 15 min, its detection of NO<sub>2</sub> gas showed a good result at 250 °C, especially when exposed to a NO<sub>2</sub> gas flow of 100 ppm, where a maximum NO<sub>2</sub> gas response of 96% was obtained. The NO<sub>2</sub> sensors based on the TiO<sub>2</sub> nanotube arrays all exhibited a high level of stability, good reproducibility, and high sensitivity.
ISSN:2073-4352