Photoelectrochemical Performance of Smooth TiO2 Nanotube Arrays: Effect of Anodization Temperature and Cleaning Methods

The formation of self-organized titanium dioxide (TiO2) nanotube arrays without bundling or clustering is essential for their high efficiency in photoelectrochemical (PEC) application. The present paper reports on the use of different temperatures to control the specific architecture of nanotube arr...

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Main Authors: Chin Wei Lai, Srimala Sreekantan
Format: Article
Language:English
Published: Wiley 2012-01-01
Series:International Journal of Photoenergy
Online Access:http://dx.doi.org/10.1155/2012/356943
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author Chin Wei Lai
Srimala Sreekantan
author_facet Chin Wei Lai
Srimala Sreekantan
author_sort Chin Wei Lai
collection DOAJ
description The formation of self-organized titanium dioxide (TiO2) nanotube arrays without bundling or clustering is essential for their high efficiency in photoelectrochemical (PEC) application. The present paper reports on the use of different temperatures to control the specific architecture of nanotube arrays and effective cleaning techniques to ensure the formation of clean TiO2 nanotube surface. The wall thickness of nanotube arrays could be controlled from 12.5 nm to 37.5 nm through different anodization temperature ranging from 10°C to 80°C. Furthermore, ultrasonic cleaning combined with acetone showed the high-ordered TiO2 nanotube arrays without morphological disorder, bundling, and microcrack problems. Based on the results obtained, a higher PEC response of 1 mA/cm2 and a photoconversion efficiency of 1.3% could be achieved using a wall thickness of 12.5 nm and defect-free TiO2 nanotube arrays for low charge transfer resistance.
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issn 1110-662X
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publishDate 2012-01-01
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series International Journal of Photoenergy
spelling doaj-art-95cc96bf78be4b46857e61b5d3ff1b562025-08-20T02:10:06ZengWileyInternational Journal of Photoenergy1110-662X1687-529X2012-01-01201210.1155/2012/356943356943Photoelectrochemical Performance of Smooth TiO2 Nanotube Arrays: Effect of Anodization Temperature and Cleaning MethodsChin Wei Lai0Srimala Sreekantan1School of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, Engineering Campus, Seberang Perai Selatan, Pulau Pinang, 14300 Nibong Tebal, MalaysiaSchool of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, Engineering Campus, Seberang Perai Selatan, Pulau Pinang, 14300 Nibong Tebal, MalaysiaThe formation of self-organized titanium dioxide (TiO2) nanotube arrays without bundling or clustering is essential for their high efficiency in photoelectrochemical (PEC) application. The present paper reports on the use of different temperatures to control the specific architecture of nanotube arrays and effective cleaning techniques to ensure the formation of clean TiO2 nanotube surface. The wall thickness of nanotube arrays could be controlled from 12.5 nm to 37.5 nm through different anodization temperature ranging from 10°C to 80°C. Furthermore, ultrasonic cleaning combined with acetone showed the high-ordered TiO2 nanotube arrays without morphological disorder, bundling, and microcrack problems. Based on the results obtained, a higher PEC response of 1 mA/cm2 and a photoconversion efficiency of 1.3% could be achieved using a wall thickness of 12.5 nm and defect-free TiO2 nanotube arrays for low charge transfer resistance.http://dx.doi.org/10.1155/2012/356943
spellingShingle Chin Wei Lai
Srimala Sreekantan
Photoelectrochemical Performance of Smooth TiO2 Nanotube Arrays: Effect of Anodization Temperature and Cleaning Methods
International Journal of Photoenergy
title Photoelectrochemical Performance of Smooth TiO2 Nanotube Arrays: Effect of Anodization Temperature and Cleaning Methods
title_full Photoelectrochemical Performance of Smooth TiO2 Nanotube Arrays: Effect of Anodization Temperature and Cleaning Methods
title_fullStr Photoelectrochemical Performance of Smooth TiO2 Nanotube Arrays: Effect of Anodization Temperature and Cleaning Methods
title_full_unstemmed Photoelectrochemical Performance of Smooth TiO2 Nanotube Arrays: Effect of Anodization Temperature and Cleaning Methods
title_short Photoelectrochemical Performance of Smooth TiO2 Nanotube Arrays: Effect of Anodization Temperature and Cleaning Methods
title_sort photoelectrochemical performance of smooth tio2 nanotube arrays effect of anodization temperature and cleaning methods
url http://dx.doi.org/10.1155/2012/356943
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AT srimalasreekantan photoelectrochemicalperformanceofsmoothtio2nanotubearrayseffectofanodizationtemperatureandcleaningmethods