Se4N4 als präparatives Reagens: Synthese von Chlorselenonitren-Komplexen des Wolframs
[WCl4(NSeCl)]2 (1) is synthesized by the reaction of Se4N4 with tungsten hexachloride in boiling dichloromethane. The complex 1 reacts with tetraphenylphosphonium chloride forming brown crystals of Ph4P[WCl5(NSeCl)] (2) from CH2Cl2 solutions. The monoclinic crystals (space group C 2) are twinned in...
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| Main Authors: | , , , , |
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| Format: | Article |
| Language: | deu |
| Published: |
Swiss Chemical Society
1988-02-01
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| Series: | CHIMIA |
| Online Access: | https://www.chimia.ch/chimia/article/view/9830 |
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