Pump–probe reciprocal-space mapping using energy-resolved XFEL pink beam pulses

We present a 3D reciprocal-space mapping (RSM) method using a pink self-amplified spontaneous emission (SASE) X-ray free-electron laser beam. The energy of each specific pulse in a SASE beam can be determined using the diffraction pattern of a specimen excited by pumping itself as a spectroscopic re...

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Main Authors: Ouyoung Kwon, Sungsoo Ha, Do Young Noh, Hyonchol Kang, Mazhar Iqbal, Muhammad Ijaz Anwar, Sunam Kim
Format: Article
Language:English
Published: International Union of Crystallography 2025-03-01
Series:Journal of Synchrotron Radiation
Subjects:
Online Access:https://journals.iucr.org/paper?S1600577525000463
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author Ouyoung Kwon
Sungsoo Ha
Do Young Noh
Hyonchol Kang
Mazhar Iqbal
Muhammad Ijaz Anwar
Sunam Kim
author_facet Ouyoung Kwon
Sungsoo Ha
Do Young Noh
Hyonchol Kang
Mazhar Iqbal
Muhammad Ijaz Anwar
Sunam Kim
author_sort Ouyoung Kwon
collection DOAJ
description We present a 3D reciprocal-space mapping (RSM) method using a pink self-amplified spontaneous emission (SASE) X-ray free-electron laser beam. The energy of each specific pulse in a SASE beam can be determined using the diffraction pattern of a specimen excited by pumping itself as a spectroscopic reference. A thin slab of RSM, whose thickness corresponds to the energy bandwidth of the pink beam, is successfully reconstructed using the proposed method. By rocking a sample in a few steps, we obtained a 3D RSM covering both the diffuse scattering and the Bragg rod in NiO thin films during a pump–probe X-ray diffraction measurement.
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publishDate 2025-03-01
publisher International Union of Crystallography
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series Journal of Synchrotron Radiation
spelling doaj-art-912d4270a51f46c4a071da2b1184dd8c2025-08-20T02:58:36ZengInternational Union of CrystallographyJournal of Synchrotron Radiation1600-57752025-03-0132228128710.1107/S1600577525000463yi5166Pump–probe reciprocal-space mapping using energy-resolved XFEL pink beam pulsesOuyoung Kwon0Sungsoo Ha1Do Young Noh2Hyonchol Kang3Mazhar Iqbal4Muhammad Ijaz Anwar5Sunam Kim6Department of Physics and Photon Science, Gwangju Institute of Science and Technology, Gwangju 61005, Republic of KoreaDepartment of Physics and Photon Science, Gwangju Institute of Science and Technology, Gwangju 61005, Republic of KoreaDepartment of Physics and Photon Science, Gwangju Institute of Science and Technology, Gwangju 61005, Republic of KoreaDepartment of Materials Science and Engineering, Chosun University, Gwangju 61452, Republic of KoreaNational Institute of Lasers & Optronics (NILOP), Islamabad 22869, PakistanNational Institute of Lasers & Optronics (NILOP), Islamabad 22869, PakistanPAL-XFEL Division, Pohang Accelerator Laboratory, Pohang 37673, Republic of KoreaWe present a 3D reciprocal-space mapping (RSM) method using a pink self-amplified spontaneous emission (SASE) X-ray free-electron laser beam. The energy of each specific pulse in a SASE beam can be determined using the diffraction pattern of a specimen excited by pumping itself as a spectroscopic reference. A thin slab of RSM, whose thickness corresponds to the energy bandwidth of the pink beam, is successfully reconstructed using the proposed method. By rocking a sample in a few steps, we obtained a 3D RSM covering both the diffuse scattering and the Bragg rod in NiO thin films during a pump–probe X-ray diffraction measurement.https://journals.iucr.org/paper?S16005775250004633d reciprocal-space mappingpink sase xfelsenergy-resolved pulsespump–probes
spellingShingle Ouyoung Kwon
Sungsoo Ha
Do Young Noh
Hyonchol Kang
Mazhar Iqbal
Muhammad Ijaz Anwar
Sunam Kim
Pump–probe reciprocal-space mapping using energy-resolved XFEL pink beam pulses
Journal of Synchrotron Radiation
3d reciprocal-space mapping
pink sase xfels
energy-resolved pulses
pump–probes
title Pump–probe reciprocal-space mapping using energy-resolved XFEL pink beam pulses
title_full Pump–probe reciprocal-space mapping using energy-resolved XFEL pink beam pulses
title_fullStr Pump–probe reciprocal-space mapping using energy-resolved XFEL pink beam pulses
title_full_unstemmed Pump–probe reciprocal-space mapping using energy-resolved XFEL pink beam pulses
title_short Pump–probe reciprocal-space mapping using energy-resolved XFEL pink beam pulses
title_sort pump probe reciprocal space mapping using energy resolved xfel pink beam pulses
topic 3d reciprocal-space mapping
pink sase xfels
energy-resolved pulses
pump–probes
url https://journals.iucr.org/paper?S1600577525000463
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