A novel optimized silver nitrate staining method for visualizing the osteocyte lacuno-canalicular system

A 50% (w/v, equivalent to 2.943 mol/L) silver nitrate solution is commonly used to stain and characterize the osteocyte lacuno-canalicular system (LCS) in bone biology research. However, variability in reagent concentrations and types, along with inconsistent staining procedures, have limited the br...

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Main Authors: Jinlian Wu, Chunchun Xue, Qiang Li, Hongjin Wu, Jie Zhang, Chenglong Wang, Weiwei Dai, Libo Wang
Format: Article
Language:English
Published: Frontiers Media S.A. 2025-05-01
Series:Frontiers in Endocrinology
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Online Access:https://www.frontiersin.org/articles/10.3389/fendo.2025.1561576/full
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author Jinlian Wu
Jinlian Wu
Chunchun Xue
Qiang Li
Hongjin Wu
Jie Zhang
Chenglong Wang
Weiwei Dai
Libo Wang
author_facet Jinlian Wu
Jinlian Wu
Chunchun Xue
Qiang Li
Hongjin Wu
Jie Zhang
Chenglong Wang
Weiwei Dai
Libo Wang
author_sort Jinlian Wu
collection DOAJ
description A 50% (w/v, equivalent to 2.943 mol/L) silver nitrate solution is commonly used to stain and characterize the osteocyte lacuno-canalicular system (LCS) in bone biology research. However, variability in reagent concentrations and types, along with inconsistent staining procedures, have limited the broader application of this method in osteocyte research. In this study, we present a novel optimized silver nitrate staining technique aimed at addressing these limitations. This new method utilizes a 1 mol/L (equivalent to 16.987%, w/v) silver nitrate solution in combination with a type-B gelatin-formic acid solution at various concentrations (0.05%-0.5% gelatin and 0.05%-5% formic acid, or 1%-2% gelatin and 0.1%-2% formic acid) in volume ratios of 4:1, 2:1, or 1:1, or a 0.5 mol/L silver nitrate solution at a 4:1 ratio. The staining process is carried out for 1 hour under ultraviolet light or 90 minutes under regular room light (or dark), followed by washing with Milli-Q water to terminate the reaction. We applied this new method to stain the osteocyte LCS in bone samples from different species and pathological bone models. The technique consistently produced clear, distinct staining patterns across all samples. Moreover, our novel method revealed a greater number of LCS compared to the traditional 50% silver nitrate solution. This suggests that the commonly used 50% silver nitrate method may disrupt or inadequately reveal the LCS in bones, potentially leading to an underestimation of LCS density and number. In conclusion, our novel silver nitrate staining method provides a simpler and more cost-effective alternative to the traditional technique. By offering a more accurate and comprehensive analysis of the LCS across species, this approach has the potential to advance research on osteocyte morphogenesis, as well as the functional and evolutionary adaptations of the osteocyte LCS across different taxa.
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issn 1664-2392
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publishDate 2025-05-01
publisher Frontiers Media S.A.
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series Frontiers in Endocrinology
spelling doaj-art-8f7f0ed36ca84302a569bc00f4c57f322025-08-20T03:49:42ZengFrontiers Media S.A.Frontiers in Endocrinology1664-23922025-05-011610.3389/fendo.2025.15615761561576A novel optimized silver nitrate staining method for visualizing the osteocyte lacuno-canalicular systemJinlian Wu0Jinlian Wu1Chunchun Xue2Qiang Li3Hongjin Wu4Jie Zhang5Chenglong Wang6Weiwei Dai7Libo Wang8Central Laboratory of Science and Technology, Longhua Hospital Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaDepartment of Rheumatology and Immunology, Longhua Hospital Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaShanghai Municipal Hospital of Traditional Chinese Medicine, Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaLonghua Hospital Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaCentral Laboratory of Science and Technology, Longhua Hospital Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaCentral Laboratory of Science and Technology, Longhua Hospital Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaCentral Laboratory of Science and Technology, Longhua Hospital Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaCentral Laboratory of Science and Technology, Longhua Hospital Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaCentral Laboratory of Science and Technology, Longhua Hospital Shanghai University of Traditional Chinese Medicine, Shanghai, ChinaA 50% (w/v, equivalent to 2.943 mol/L) silver nitrate solution is commonly used to stain and characterize the osteocyte lacuno-canalicular system (LCS) in bone biology research. However, variability in reagent concentrations and types, along with inconsistent staining procedures, have limited the broader application of this method in osteocyte research. In this study, we present a novel optimized silver nitrate staining technique aimed at addressing these limitations. This new method utilizes a 1 mol/L (equivalent to 16.987%, w/v) silver nitrate solution in combination with a type-B gelatin-formic acid solution at various concentrations (0.05%-0.5% gelatin and 0.05%-5% formic acid, or 1%-2% gelatin and 0.1%-2% formic acid) in volume ratios of 4:1, 2:1, or 1:1, or a 0.5 mol/L silver nitrate solution at a 4:1 ratio. The staining process is carried out for 1 hour under ultraviolet light or 90 minutes under regular room light (or dark), followed by washing with Milli-Q water to terminate the reaction. We applied this new method to stain the osteocyte LCS in bone samples from different species and pathological bone models. The technique consistently produced clear, distinct staining patterns across all samples. Moreover, our novel method revealed a greater number of LCS compared to the traditional 50% silver nitrate solution. This suggests that the commonly used 50% silver nitrate method may disrupt or inadequately reveal the LCS in bones, potentially leading to an underestimation of LCS density and number. In conclusion, our novel silver nitrate staining method provides a simpler and more cost-effective alternative to the traditional technique. By offering a more accurate and comprehensive analysis of the LCS across species, this approach has the potential to advance research on osteocyte morphogenesis, as well as the functional and evolutionary adaptations of the osteocyte LCS across different taxa.https://www.frontiersin.org/articles/10.3389/fendo.2025.1561576/fullsilver nitrategelatinformic acidosteocytelacuno-canalicular system (LCS)
spellingShingle Jinlian Wu
Jinlian Wu
Chunchun Xue
Qiang Li
Hongjin Wu
Jie Zhang
Chenglong Wang
Weiwei Dai
Libo Wang
A novel optimized silver nitrate staining method for visualizing the osteocyte lacuno-canalicular system
Frontiers in Endocrinology
silver nitrate
gelatin
formic acid
osteocyte
lacuno-canalicular system (LCS)
title A novel optimized silver nitrate staining method for visualizing the osteocyte lacuno-canalicular system
title_full A novel optimized silver nitrate staining method for visualizing the osteocyte lacuno-canalicular system
title_fullStr A novel optimized silver nitrate staining method for visualizing the osteocyte lacuno-canalicular system
title_full_unstemmed A novel optimized silver nitrate staining method for visualizing the osteocyte lacuno-canalicular system
title_short A novel optimized silver nitrate staining method for visualizing the osteocyte lacuno-canalicular system
title_sort novel optimized silver nitrate staining method for visualizing the osteocyte lacuno canalicular system
topic silver nitrate
gelatin
formic acid
osteocyte
lacuno-canalicular system (LCS)
url https://www.frontiersin.org/articles/10.3389/fendo.2025.1561576/full
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