Study on supercritical CO2 extraction process, volatile components and antioxidant activity of rose oil from Dianhong rose

Objective: Comprehensive utilization of Dianhong rose resources to improve the added value of products. Methods: The single-factor experiment and response surface experiment were used to optimize the extraction process of supercritical CO<sub>2</sub> with essential oil yield as the measu...

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Main Authors: LIU Jin-yun, CHANG Jian, JIANG Zhuo-fang, XU Chong-jun, CHENG Wan, WU Heng
Format: Article
Language:English
Published: The Editorial Office of Food and Machinery 2023-04-01
Series:Shipin yu jixie
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Online Access:http://www.ifoodmm.com/spyjxen/article/abstract/20230329
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author LIU Jin-yun
CHANG Jian
JIANG Zhuo-fang
XU Chong-jun
CHENG Wan
WU Heng
author_facet LIU Jin-yun
CHANG Jian
JIANG Zhuo-fang
XU Chong-jun
CHENG Wan
WU Heng
author_sort LIU Jin-yun
collection DOAJ
description Objective: Comprehensive utilization of Dianhong rose resources to improve the added value of products. Methods: The single-factor experiment and response surface experiment were used to optimize the extraction process of supercritical CO<sub>2</sub> with essential oil yield as the measurement index. The composition and relative content of different rose oils were analyzed by GC-MS. The components and relative contents of different rose oils were analyzed by GC-MS, and the antioxidant activities of different rose oils were evaluated. Results: The results showed that the optimal extraction parameters were as followed: particle size of 40 mesh, extraction pressure of 25.5 MPa, extraction temperature of 45.5 ℃, extraction time of 123 min, CO<sub>2</sub> flow rate of 20 L/h. Under these conditions, the essential oil yield of rose was 1.185%. A total of 74 compounds were identified from different Dianhong rose oil, and the total volatile substances of Anning Dianhong rose essential oil were the highest. The essential oil of Yunnan Dianhong rose had good ability to scavenge free radicals. The antioxidant activities of essential oil from different producing areas were obviously different. Conclusion: The essential oil extracted by supercritical CO<sub>2</sub> has good quality and can be used as a natural antioxidant.
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spelling doaj-art-8f01645ca816422486d63b26f7c203be2025-08-20T02:22:37ZengThe Editorial Office of Food and MachineryShipin yu jixie1003-57882023-04-0139317518210.13652/j.spjx.1003.5788.2022.80792Study on supercritical CO2 extraction process, volatile components and antioxidant activity of rose oil from Dianhong roseLIU Jin-yun0CHANG Jian1JIANG Zhuo-fang2XU Chong-jun3CHENG Wan4WU Heng5 Yunnan Tobacco Industrial Hi-Tech Material Co., Ltd., Kunming, Yunnan 650106 , China Yunnan Tobacco Industrial Hi-Tech Material Co., Ltd., Kunming, Yunnan 650106 , China Yunnan Tobacco Industrial Hi-Tech Material Co., Ltd., Kunming, Yunnan 650106 , China Yunnan Tobacco Industrial Hi-Tech Material Co., Ltd., Kunming, Yunnan 650106 , China Yunnan Tobacco Industrial Hi-Tech Material Co., Ltd., Kunming, Yunnan 650106 , China Yunnan Tobacco Industrial Hi-Tech Material Co., Ltd., Kunming, Yunnan 650106 , China Objective: Comprehensive utilization of Dianhong rose resources to improve the added value of products. Methods: The single-factor experiment and response surface experiment were used to optimize the extraction process of supercritical CO<sub>2</sub> with essential oil yield as the measurement index. The composition and relative content of different rose oils were analyzed by GC-MS. The components and relative contents of different rose oils were analyzed by GC-MS, and the antioxidant activities of different rose oils were evaluated. Results: The results showed that the optimal extraction parameters were as followed: particle size of 40 mesh, extraction pressure of 25.5 MPa, extraction temperature of 45.5 ℃, extraction time of 123 min, CO<sub>2</sub> flow rate of 20 L/h. Under these conditions, the essential oil yield of rose was 1.185%. A total of 74 compounds were identified from different Dianhong rose oil, and the total volatile substances of Anning Dianhong rose essential oil were the highest. The essential oil of Yunnan Dianhong rose had good ability to scavenge free radicals. The antioxidant activities of essential oil from different producing areas were obviously different. Conclusion: The essential oil extracted by supercritical CO<sub>2</sub> has good quality and can be used as a natural antioxidant.http://www.ifoodmm.com/spyjxen/article/abstract/20230329 rose essential oil supercritical fluid co2 extraction volatile constituent gc/ms antioxidant
spellingShingle LIU Jin-yun
CHANG Jian
JIANG Zhuo-fang
XU Chong-jun
CHENG Wan
WU Heng
Study on supercritical CO2 extraction process, volatile components and antioxidant activity of rose oil from Dianhong rose
Shipin yu jixie
rose
essential oil
supercritical fluid co2 extraction
volatile constituent
gc/ms
antioxidant
title Study on supercritical CO2 extraction process, volatile components and antioxidant activity of rose oil from Dianhong rose
title_full Study on supercritical CO2 extraction process, volatile components and antioxidant activity of rose oil from Dianhong rose
title_fullStr Study on supercritical CO2 extraction process, volatile components and antioxidant activity of rose oil from Dianhong rose
title_full_unstemmed Study on supercritical CO2 extraction process, volatile components and antioxidant activity of rose oil from Dianhong rose
title_short Study on supercritical CO2 extraction process, volatile components and antioxidant activity of rose oil from Dianhong rose
title_sort study on supercritical co2 extraction process volatile components and antioxidant activity of rose oil from dianhong rose
topic rose
essential oil
supercritical fluid co2 extraction
volatile constituent
gc/ms
antioxidant
url http://www.ifoodmm.com/spyjxen/article/abstract/20230329
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AT jiangzhuofang studyonsupercriticalco2extractionprocessvolatilecomponentsandantioxidantactivityofroseoilfromdianhongrose
AT xuchongjun studyonsupercriticalco2extractionprocessvolatilecomponentsandantioxidantactivityofroseoilfromdianhongrose
AT chengwan studyonsupercriticalco2extractionprocessvolatilecomponentsandantioxidantactivityofroseoilfromdianhongrose
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