Mixture Design and Doehlert Matrix for Optimization of Energized Dispersive Guided Extraction (EDGE) of Theobromine and Caffeine from Cocoa Bean Shells

Mixture Design and Doehlert Matrix for Optimization of Energized Dispersive Guided Extraction (EDGE) of Theobromine and Caffeine from Cocoa Bean Shells

This work describes the development of a method for the extraction of methylxanthines from cocoa bean shell (CBS) by employing the novel Energized Dispersive Guided Extraction (EDGE) system. The mixtures were composed of ethanol–methanol–water and the ratio was optimized using a simplex-centroid des...

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Bibliographic Details
Main Authors: Luciana Lordêlo Nascimento, Paulo Natan Alves dos Santos, Honnara Santos Granja, Larissa da Silveira Ferreira, João Victor Ferreira Lima, Bruna Louise de Moura Pita, Allan dos Santos Polidoro, Lisiane dos Santos Freitas, Elina Bastos Caramão, Fabio de Souza Dias, Alini Tinoco Fricks
Format: Article
Language:English
Published: MDPI AG 2025-02-01
Series:Foods
Subjects:
energized dispersive guided extraction (EDGE)
cocoa waste valorization
methylxanthines
optimization
Doehlert matrix
green chemistry
Online Access:https://www.mdpi.com/2304-8158/14/5/740
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