Oxygen Content and Thermodynamic Stability of YBaCo2O6−δ Double Perovskite

The thermodynamic stability of the double perovskite YBaCo2O6−δ was studied using the coulometric titration technique and verified by measurements of the overall conductivity depending on oxygen partial pressure at a given temperature. As a result, the stability diagram of YBaCo2O6−δ was plotted. YB...

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Main Authors: Anton L. Sednev, Andrey Yu Zuev, Dmitry S. Tsvetkov
Format: Article
Language:English
Published: Wiley 2018-01-01
Series:Advances in Materials Science and Engineering
Online Access:http://dx.doi.org/10.1155/2018/1205708
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author Anton L. Sednev
Andrey Yu Zuev
Dmitry S. Tsvetkov
author_facet Anton L. Sednev
Andrey Yu Zuev
Dmitry S. Tsvetkov
author_sort Anton L. Sednev
collection DOAJ
description The thermodynamic stability of the double perovskite YBaCo2O6−δ was studied using the coulometric titration technique and verified by measurements of the overall conductivity depending on oxygen partial pressure at a given temperature. As a result, the stability diagram of YBaCo2O6−δ was plotted. YBaCo2O6−δ was found to be thermodynamically stable in air at 850°C and higher temperatures, whereas its thermodynamic stability at 900°C is limited by the range of oxygen partial pressures −3.56 ≤ log(pO2/atm) ≤ −0.14. Oxygen content in YBaCo2O6−δ slightly decreases at 900°C from 5.035 at log(pO2/atm) = −0.14 to 4.989 in the atmosphere with log(pO2/atm) = −3.565 indicating a crucial role which variation of Co+3/Co+2 ratio plays in its stability. YBaCo2O6−δ decomposes into the mixture of YCoO3 and BaCoO3−z at the high pO2 stability limit, whereas YBaCo4O7, BaCo1−xYxO3−γ, and Y2O3 were identified as the products of its decomposition at the low pO2 one.
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spelling doaj-art-8e9b8b0534c6426abc23daffd2bd6df92025-08-20T02:09:22ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422018-01-01201810.1155/2018/12057081205708Oxygen Content and Thermodynamic Stability of YBaCo2O6−δ Double PerovskiteAnton L. Sednev0Andrey Yu Zuev1Dmitry S. Tsvetkov2Institute of Natural Sciences and Mathematics, Ural Federal University, Yekaterinburg 620000, RussiaInstitute of Natural Sciences and Mathematics, Ural Federal University, Yekaterinburg 620000, RussiaInstitute of Natural Sciences and Mathematics, Ural Federal University, Yekaterinburg 620000, RussiaThe thermodynamic stability of the double perovskite YBaCo2O6−δ was studied using the coulometric titration technique and verified by measurements of the overall conductivity depending on oxygen partial pressure at a given temperature. As a result, the stability diagram of YBaCo2O6−δ was plotted. YBaCo2O6−δ was found to be thermodynamically stable in air at 850°C and higher temperatures, whereas its thermodynamic stability at 900°C is limited by the range of oxygen partial pressures −3.56 ≤ log(pO2/atm) ≤ −0.14. Oxygen content in YBaCo2O6−δ slightly decreases at 900°C from 5.035 at log(pO2/atm) = −0.14 to 4.989 in the atmosphere with log(pO2/atm) = −3.565 indicating a crucial role which variation of Co+3/Co+2 ratio plays in its stability. YBaCo2O6−δ decomposes into the mixture of YCoO3 and BaCoO3−z at the high pO2 stability limit, whereas YBaCo4O7, BaCo1−xYxO3−γ, and Y2O3 were identified as the products of its decomposition at the low pO2 one.http://dx.doi.org/10.1155/2018/1205708
spellingShingle Anton L. Sednev
Andrey Yu Zuev
Dmitry S. Tsvetkov
Oxygen Content and Thermodynamic Stability of YBaCo2O6−δ Double Perovskite
Advances in Materials Science and Engineering
title Oxygen Content and Thermodynamic Stability of YBaCo2O6−δ Double Perovskite
title_full Oxygen Content and Thermodynamic Stability of YBaCo2O6−δ Double Perovskite
title_fullStr Oxygen Content and Thermodynamic Stability of YBaCo2O6−δ Double Perovskite
title_full_unstemmed Oxygen Content and Thermodynamic Stability of YBaCo2O6−δ Double Perovskite
title_short Oxygen Content and Thermodynamic Stability of YBaCo2O6−δ Double Perovskite
title_sort oxygen content and thermodynamic stability of ybaco2o6 δ double perovskite
url http://dx.doi.org/10.1155/2018/1205708
work_keys_str_mv AT antonlsednev oxygencontentandthermodynamicstabilityofybaco2o6ddoubleperovskite
AT andreyyuzuev oxygencontentandthermodynamicstabilityofybaco2o6ddoubleperovskite
AT dmitrystsvetkov oxygencontentandthermodynamicstabilityofybaco2o6ddoubleperovskite