Preparation and performance study of low heat storage flame retardant polyurethane for coal mines

In order to meet the requirements for the use of polyurethane for reinforcement in mines, the synthesis temperature of polyurethane needs to be lowered, and the flame-retardant and mechanical properties of polyurethane should also be considered comprehensively. Factors affecting the synthesis temper...

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Main Authors: Haiyan Wang, Xiao Chen, Chengxiang Zou, Cheng Fan, Lei Chen, Mengen Zhao
Format: Article
Language:English
Published: Elsevier 2024-12-01
Series:Case Studies in Thermal Engineering
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2214157X2401445X
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author Haiyan Wang
Xiao Chen
Chengxiang Zou
Cheng Fan
Lei Chen
Mengen Zhao
author_facet Haiyan Wang
Xiao Chen
Chengxiang Zou
Cheng Fan
Lei Chen
Mengen Zhao
author_sort Haiyan Wang
collection DOAJ
description In order to meet the requirements for the use of polyurethane for reinforcement in mines, the synthesis temperature of polyurethane needs to be lowered, and the flame-retardant and mechanical properties of polyurethane should also be considered comprehensively. Factors affecting the synthesis temperature of polyurethanes are investigated, low heat storage polyurethanes that meet the temperature requirements for use in plugging crushed coal bodies in coal mines are formulated, and the synthesized polyurethanes are characterised for their flame retardant properties by FTIR, SEM, TG-FTIR and CONE experiments. It was found that in this paper, a new type of polyurethane for coal mines was formed by flame retardant modification of polyurethane by adding nano-system flame retardant and phosphorus-system flame retardant, and the synthetic reaction temperature of the material could reach as low as 51.2 °C, and the pyrolysis onset temperature was increased to 286 °C. The experimental results show that the flame retardant property of this synthetic polyurethane has been significantly improved, and the heat accumulation effect of the synthesis process on the surrounding coal body has been greatly reduced. The physical properties and thermal stability of this synthetic polyurethane in the grouting process meet the safety requirements for use in underground coal mines.
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publishDate 2024-12-01
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series Case Studies in Thermal Engineering
spelling doaj-art-8e1c3d3a1f0941828ff7595376e97e932025-08-20T02:37:33ZengElsevierCase Studies in Thermal Engineering2214-157X2024-12-016410541410.1016/j.csite.2024.105414Preparation and performance study of low heat storage flame retardant polyurethane for coal minesHaiyan Wang0Xiao Chen1Chengxiang Zou2Cheng Fan3Lei Chen4Mengen Zhao5School of Emergency Management and Safety Engineering, China University of Mining and Technology-Beijing, Beijing, 100083, ChinaCorresponding author.; School of Emergency Management and Safety Engineering, China University of Mining and Technology-Beijing, Beijing, 100083, ChinaSchool of Emergency Management and Safety Engineering, China University of Mining and Technology-Beijing, Beijing, 100083, ChinaSchool of Emergency Management and Safety Engineering, China University of Mining and Technology-Beijing, Beijing, 100083, ChinaSchool of Emergency Management and Safety Engineering, China University of Mining and Technology-Beijing, Beijing, 100083, ChinaSchool of Emergency Management and Safety Engineering, China University of Mining and Technology-Beijing, Beijing, 100083, ChinaIn order to meet the requirements for the use of polyurethane for reinforcement in mines, the synthesis temperature of polyurethane needs to be lowered, and the flame-retardant and mechanical properties of polyurethane should also be considered comprehensively. Factors affecting the synthesis temperature of polyurethanes are investigated, low heat storage polyurethanes that meet the temperature requirements for use in plugging crushed coal bodies in coal mines are formulated, and the synthesized polyurethanes are characterised for their flame retardant properties by FTIR, SEM, TG-FTIR and CONE experiments. It was found that in this paper, a new type of polyurethane for coal mines was formed by flame retardant modification of polyurethane by adding nano-system flame retardant and phosphorus-system flame retardant, and the synthetic reaction temperature of the material could reach as low as 51.2 °C, and the pyrolysis onset temperature was increased to 286 °C. The experimental results show that the flame retardant property of this synthetic polyurethane has been significantly improved, and the heat accumulation effect of the synthesis process on the surrounding coal body has been greatly reduced. The physical properties and thermal stability of this synthetic polyurethane in the grouting process meet the safety requirements for use in underground coal mines.http://www.sciencedirect.com/science/article/pii/S2214157X2401445XSynthesis temperatureFlame retardantPolyurethaneGroutingCoal mines
spellingShingle Haiyan Wang
Xiao Chen
Chengxiang Zou
Cheng Fan
Lei Chen
Mengen Zhao
Preparation and performance study of low heat storage flame retardant polyurethane for coal mines
Case Studies in Thermal Engineering
Synthesis temperature
Flame retardant
Polyurethane
Grouting
Coal mines
title Preparation and performance study of low heat storage flame retardant polyurethane for coal mines
title_full Preparation and performance study of low heat storage flame retardant polyurethane for coal mines
title_fullStr Preparation and performance study of low heat storage flame retardant polyurethane for coal mines
title_full_unstemmed Preparation and performance study of low heat storage flame retardant polyurethane for coal mines
title_short Preparation and performance study of low heat storage flame retardant polyurethane for coal mines
title_sort preparation and performance study of low heat storage flame retardant polyurethane for coal mines
topic Synthesis temperature
Flame retardant
Polyurethane
Grouting
Coal mines
url http://www.sciencedirect.com/science/article/pii/S2214157X2401445X
work_keys_str_mv AT haiyanwang preparationandperformancestudyoflowheatstorageflameretardantpolyurethaneforcoalmines
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AT chengxiangzou preparationandperformancestudyoflowheatstorageflameretardantpolyurethaneforcoalmines
AT chengfan preparationandperformancestudyoflowheatstorageflameretardantpolyurethaneforcoalmines
AT leichen preparationandperformancestudyoflowheatstorageflameretardantpolyurethaneforcoalmines
AT mengenzhao preparationandperformancestudyoflowheatstorageflameretardantpolyurethaneforcoalmines