Optimization of Ni loading amount in Ni-CeZrO2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oil

In response to global efforts to address plastic pollution, pyrolysis of waste plastics offers a sustainable pathway for chemical recycling and clean hydrogen production. This study focuses on the steam reforming of dodecane, a key component of light oil derived from plastic pyrolysis, to produce hy...

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Main Authors: Min-Gyeong Bae, Yeol-Lim Lee, Hak-Min Kim, Ji-Won Son, Beom-Su Cheon, Dae-Woon Jeong
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Fuel Processing Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S0378382025000426
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author Min-Gyeong Bae
Yeol-Lim Lee
Hak-Min Kim
Ji-Won Son
Beom-Su Cheon
Dae-Woon Jeong
author_facet Min-Gyeong Bae
Yeol-Lim Lee
Hak-Min Kim
Ji-Won Son
Beom-Su Cheon
Dae-Woon Jeong
author_sort Min-Gyeong Bae
collection DOAJ
description In response to global efforts to address plastic pollution, pyrolysis of waste plastics offers a sustainable pathway for chemical recycling and clean hydrogen production. This study focuses on the steam reforming of dodecane, a key component of light oil derived from plastic pyrolysis, to produce hydrogen. Nickel-based catalysts supported on Ce0.8Zr0.2O2 (Ni-CeZrO2) with varying Ni loadings (1, 3, 5, and 10 wt%) were synthesized using a co-precipitation method and characterized by various characterization techniques. The catalytic performance was evaluated under steam reforming conditions at 750 °C. Among the prepared catalysts, 5 wt% Ni-CeZrO2 exhibited the highest hydrogen yield and dodecane conversion due to its optimal balance of Ni0 active sites, oxygen storage capacity, and strong metal-support interaction. The 10 wt% Ni-CeZrO2 catalyst showed higher initial activity but suffered rapid deactivation due to excessive carbon formation, while lower Ni loadings (1 and 3 wt%) showed insufficient active sites for effective reforming. The results indicate that 5 wt% Ni-CeZrO2 is the optimal loading amount for the steam reforming of dodecane, providing a balance between high activity and long-term stability.
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spelling doaj-art-8e1aa5a4207d4e5a8331bfe0242093452025-08-20T02:55:13ZengElsevierFuel Processing Technology0378-38202025-07-0127210821810.1016/j.fuproc.2025.108218Optimization of Ni loading amount in Ni-CeZrO2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oilMin-Gyeong Bae0Yeol-Lim Lee1Hak-Min Kim2Ji-Won Son3Beom-Su Cheon4Dae-Woon Jeong5Department of Environmental Engineering, Changwon National University, 20 Changwondaehak-ro, Changwon, Gyeongnam 51140, Republic of KoreaDepartment of Chemical Engineering, Keimyung University, 1095 Dalgubeol-daero, Dalseo-gu, Daegu 42601, Republic of KoreaDepartment of Smart Mobility, Dongseo University, 47 Jurye-ro, Sasang-gu, Busan 47011, Republic of KoreaDepartment of Environmental Engineering, Changwon National University, 20 Changwondaehak-ro, Changwon, Gyeongnam 51140, Republic of KoreaDepartment of Environmental Engineering, Changwon National University, 20 Changwondaehak-ro, Changwon, Gyeongnam 51140, Republic of KoreaDepartment of Environment & Energy Engineering, Changwon National University, 20 Changwondaehak-ro, Changwon, Gyeongnam 51140, Republic of Korea; Corresponding author.In response to global efforts to address plastic pollution, pyrolysis of waste plastics offers a sustainable pathway for chemical recycling and clean hydrogen production. This study focuses on the steam reforming of dodecane, a key component of light oil derived from plastic pyrolysis, to produce hydrogen. Nickel-based catalysts supported on Ce0.8Zr0.2O2 (Ni-CeZrO2) with varying Ni loadings (1, 3, 5, and 10 wt%) were synthesized using a co-precipitation method and characterized by various characterization techniques. The catalytic performance was evaluated under steam reforming conditions at 750 °C. Among the prepared catalysts, 5 wt% Ni-CeZrO2 exhibited the highest hydrogen yield and dodecane conversion due to its optimal balance of Ni0 active sites, oxygen storage capacity, and strong metal-support interaction. The 10 wt% Ni-CeZrO2 catalyst showed higher initial activity but suffered rapid deactivation due to excessive carbon formation, while lower Ni loadings (1 and 3 wt%) showed insufficient active sites for effective reforming. The results indicate that 5 wt% Ni-CeZrO2 is the optimal loading amount for the steam reforming of dodecane, providing a balance between high activity and long-term stability.http://www.sciencedirect.com/science/article/pii/S0378382025000426Dodecane steam reformingNi-CeZrO2Plastic pyrolysis oilHydrogenCarbon formationOxygen storage capacity
spellingShingle Min-Gyeong Bae
Yeol-Lim Lee
Hak-Min Kim
Ji-Won Son
Beom-Su Cheon
Dae-Woon Jeong
Optimization of Ni loading amount in Ni-CeZrO2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oil
Fuel Processing Technology
Dodecane steam reforming
Ni-CeZrO2
Plastic pyrolysis oil
Hydrogen
Carbon formation
Oxygen storage capacity
title Optimization of Ni loading amount in Ni-CeZrO2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oil
title_full Optimization of Ni loading amount in Ni-CeZrO2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oil
title_fullStr Optimization of Ni loading amount in Ni-CeZrO2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oil
title_full_unstemmed Optimization of Ni loading amount in Ni-CeZrO2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oil
title_short Optimization of Ni loading amount in Ni-CeZrO2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oil
title_sort optimization of ni loading amount in ni cezro2 catalyst for dodecane steam reforming for the upcycling of plastic pyrolysis oil
topic Dodecane steam reforming
Ni-CeZrO2
Plastic pyrolysis oil
Hydrogen
Carbon formation
Oxygen storage capacity
url http://www.sciencedirect.com/science/article/pii/S0378382025000426
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