Cyclic polyesters prepared by poly(oxypropylene oxymaloyl) ring-chain reactions

The synthesis of cyclic polyesters of poly(oxypropylene oxymaloyl) from a ring-chain reaction was carried out at 40°C with 'Maghnite' an acid exchanged montmorillonite as acid solid ecocatalyst (Mag–H+). 'Maghnite' is already used as catalyst for polymerization of many vinylic an...

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Format: Article
Language:English
Published: Budapest University of Technology and Economics 2007-01-01
Series:eXPRESS Polymer Letters
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Online Access:http://www.expresspolymlett.com/letolt.php?file=EPL-0000015&mi=cd
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description The synthesis of cyclic polyesters of poly(oxypropylene oxymaloyl) from a ring-chain reaction was carried out at 40°C with 'Maghnite' an acid exchanged montmorillonite as acid solid ecocatalyst (Mag–H+). 'Maghnite' is already used as catalyst for polymerization of many vinylic and heterocyclic monomers [1]. The effect of amount of catalyst on yield and molecular weight of polymer was studied.A typical reaction product was analyzed by gel permeation chromatography (GPC) as well as by nuclear magnetic resonance spectroscopy (1H-NMR) and the existence of cyclic species was proven.
format Article
id doaj-art-8d9ae12aef3d47d6ba61830b55ab49b2
institution Kabale University
issn 1788-618X
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publishDate 2007-01-01
publisher Budapest University of Technology and Economics
record_format Article
series eXPRESS Polymer Letters
spelling doaj-art-8d9ae12aef3d47d6ba61830b55ab49b22025-08-20T03:56:55ZengBudapest University of Technology and EconomicseXPRESS Polymer Letters1788-618X2007-01-0111242610.3144/expresspolymlett.2007.5Cyclic polyesters prepared by poly(oxypropylene oxymaloyl) ring-chain reactionsThe synthesis of cyclic polyesters of poly(oxypropylene oxymaloyl) from a ring-chain reaction was carried out at 40°C with 'Maghnite' an acid exchanged montmorillonite as acid solid ecocatalyst (Mag–H+). 'Maghnite' is already used as catalyst for polymerization of many vinylic and heterocyclic monomers [1]. The effect of amount of catalyst on yield and molecular weight of polymer was studied.A typical reaction product was analyzed by gel permeation chromatography (GPC) as well as by nuclear magnetic resonance spectroscopy (1H-NMR) and the existence of cyclic species was proven.http://www.expresspolymlett.com/letolt.php?file=EPL-0000015&mi=cdPolymer synthesis, molecular eMaghniteMontmorillonite
spellingShingle Cyclic polyesters prepared by poly(oxypropylene oxymaloyl) ring-chain reactions
eXPRESS Polymer Letters
Polymer synthesis, molecular e
Maghnite
Montmorillonite
title Cyclic polyesters prepared by poly(oxypropylene oxymaloyl) ring-chain reactions
title_full Cyclic polyesters prepared by poly(oxypropylene oxymaloyl) ring-chain reactions
title_fullStr Cyclic polyesters prepared by poly(oxypropylene oxymaloyl) ring-chain reactions
title_full_unstemmed Cyclic polyesters prepared by poly(oxypropylene oxymaloyl) ring-chain reactions
title_short Cyclic polyesters prepared by poly(oxypropylene oxymaloyl) ring-chain reactions
title_sort cyclic polyesters prepared by poly oxypropylene oxymaloyl ring chain reactions
topic Polymer synthesis, molecular e
Maghnite
Montmorillonite
url http://www.expresspolymlett.com/letolt.php?file=EPL-0000015&mi=cd