Corona triode poling of P(VDF-TrFE) nanofibers: Mechanisms and optimization strategies

The effectiveness of the poling process of poly(vinylidene fluoride-trifluoroethylene) (P(VDF-TrFE)) nanofibers is essential for their use in engineering applications (i.e., artificial piezoelectric skins, self-sensing composite materials). While traditional contact poling methods present electrical...

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Main Authors: Leonardo Gasperini, Giacomo Selleri, Davide Pegoraro, Daniele Mariani, Alberto Rumi, Paolo Seri, Davide Fabiani
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:Journal of Science: Advanced Materials and Devices
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Online Access:http://www.sciencedirect.com/science/article/pii/S2468217925000231
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author Leonardo Gasperini
Giacomo Selleri
Davide Pegoraro
Daniele Mariani
Alberto Rumi
Paolo Seri
Davide Fabiani
author_facet Leonardo Gasperini
Giacomo Selleri
Davide Pegoraro
Daniele Mariani
Alberto Rumi
Paolo Seri
Davide Fabiani
author_sort Leonardo Gasperini
collection DOAJ
description The effectiveness of the poling process of poly(vinylidene fluoride-trifluoroethylene) (P(VDF-TrFE)) nanofibers is essential for their use in engineering applications (i.e., artificial piezoelectric skins, self-sensing composite materials). While traditional contact poling methods present electrical breakdown risks through the highly porous nanofibrous membranes, the corona poling technique offers a non-contact alternative, utilizing ion generation to polarize piezoelectric materials without direct interaction between the high-voltage electrode and the sample. The corona poling process is well-established for P(VDF-TrFE) thin films, but literature lacks a reliable methodology for P(VDF-TrFE) nanofibers. This study addresses this gap by systematically investigating the differences between the corona poling of P(VDF-TrFE) films and nanofibers and aims to disclose the distinct physical mechanisms involved. First, the corona triode setup is optimized for P(VDF-TrFE) films, achieving a piezoelectric strain coefficient d33 of 23 pC N−1. The parameters of the corona setup are then methodically recalibrated for the nanofiber's polarization, with the rationale behind these adjustments discussed and validated through experimental investigations. Such a refined corona poling method leads to a d33 equal to −20.8 pC N−1 for the nanofibers, contemporary allowing for a comprehensive understanding of the physical mechanisms behind the two distinct methods.
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spelling doaj-art-8bd538433a9e4a5cb37542204f348d442025-08-20T02:30:10ZengElsevierJournal of Science: Advanced Materials and Devices2468-21792025-06-0110210087010.1016/j.jsamd.2025.100870Corona triode poling of P(VDF-TrFE) nanofibers: Mechanisms and optimization strategiesLeonardo Gasperini0Giacomo Selleri1Davide Pegoraro2Daniele Mariani3Alberto Rumi4Paolo Seri5Davide Fabiani6Corresponding author.; Department of Electrical, Electronic, and Information Engineering, University of Bologna, Viale Risorgimento 2, 40136, Bologna, ItalyCorresponding author.; Department of Electrical, Electronic, and Information Engineering, University of Bologna, Viale Risorgimento 2, 40136, Bologna, ItalyDepartment of Electrical, Electronic, and Information Engineering, University of Bologna, Viale Risorgimento 2, 40136, Bologna, ItalyDepartment of Electrical, Electronic, and Information Engineering, University of Bologna, Viale Risorgimento 2, 40136, Bologna, ItalyDepartment of Electrical, Electronic, and Information Engineering, University of Bologna, Viale Risorgimento 2, 40136, Bologna, ItalyDepartment of Electrical, Electronic, and Information Engineering, University of Bologna, Viale Risorgimento 2, 40136, Bologna, ItalyDepartment of Electrical, Electronic, and Information Engineering, University of Bologna, Viale Risorgimento 2, 40136, Bologna, ItalyThe effectiveness of the poling process of poly(vinylidene fluoride-trifluoroethylene) (P(VDF-TrFE)) nanofibers is essential for their use in engineering applications (i.e., artificial piezoelectric skins, self-sensing composite materials). While traditional contact poling methods present electrical breakdown risks through the highly porous nanofibrous membranes, the corona poling technique offers a non-contact alternative, utilizing ion generation to polarize piezoelectric materials without direct interaction between the high-voltage electrode and the sample. The corona poling process is well-established for P(VDF-TrFE) thin films, but literature lacks a reliable methodology for P(VDF-TrFE) nanofibers. This study addresses this gap by systematically investigating the differences between the corona poling of P(VDF-TrFE) films and nanofibers and aims to disclose the distinct physical mechanisms involved. First, the corona triode setup is optimized for P(VDF-TrFE) films, achieving a piezoelectric strain coefficient d33 of 23 pC N−1. The parameters of the corona setup are then methodically recalibrated for the nanofiber's polarization, with the rationale behind these adjustments discussed and validated through experimental investigations. Such a refined corona poling method leads to a d33 equal to −20.8 pC N−1 for the nanofibers, contemporary allowing for a comprehensive understanding of the physical mechanisms behind the two distinct methods.http://www.sciencedirect.com/science/article/pii/S2468217925000231Corona polingPiezoelectricP(VDF-TrFE) nanofibersFactorial design
spellingShingle Leonardo Gasperini
Giacomo Selleri
Davide Pegoraro
Daniele Mariani
Alberto Rumi
Paolo Seri
Davide Fabiani
Corona triode poling of P(VDF-TrFE) nanofibers: Mechanisms and optimization strategies
Journal of Science: Advanced Materials and Devices
Corona poling
Piezoelectric
P(VDF-TrFE) nanofibers
Factorial design
title Corona triode poling of P(VDF-TrFE) nanofibers: Mechanisms and optimization strategies
title_full Corona triode poling of P(VDF-TrFE) nanofibers: Mechanisms and optimization strategies
title_fullStr Corona triode poling of P(VDF-TrFE) nanofibers: Mechanisms and optimization strategies
title_full_unstemmed Corona triode poling of P(VDF-TrFE) nanofibers: Mechanisms and optimization strategies
title_short Corona triode poling of P(VDF-TrFE) nanofibers: Mechanisms and optimization strategies
title_sort corona triode poling of p vdf trfe nanofibers mechanisms and optimization strategies
topic Corona poling
Piezoelectric
P(VDF-TrFE) nanofibers
Factorial design
url http://www.sciencedirect.com/science/article/pii/S2468217925000231
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