Synthesis of S-aryl dithiocarbamates and its in-silico studies

Environmentally friendly facile synthesis of aryl dithiocarbamates via a one-pot procedure by the reaction between secondary amines and carbon disulphide produced dithiocarbamates, which underwent copper-assisted intermolecular CS cross-coupling with aryl Iodides are developed. Cu2O is employed as...

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Main Authors: Krishnarao Jayaram Desai, Murugesan Santhosh, Padmanaban Akashvarunan, Ponraj Abarna, Boopathi Shagunthala Hariprasad, Sundaram Ganesh Babu, Annamalai Pratheepkumar
Format: Article
Language:English
Published: Elsevier 2025-05-01
Series:Results in Chemistry
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Online Access:http://www.sciencedirect.com/science/article/pii/S2211715625002401
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author Krishnarao Jayaram Desai
Murugesan Santhosh
Padmanaban Akashvarunan
Ponraj Abarna
Boopathi Shagunthala Hariprasad
Sundaram Ganesh Babu
Annamalai Pratheepkumar
author_facet Krishnarao Jayaram Desai
Murugesan Santhosh
Padmanaban Akashvarunan
Ponraj Abarna
Boopathi Shagunthala Hariprasad
Sundaram Ganesh Babu
Annamalai Pratheepkumar
author_sort Krishnarao Jayaram Desai
collection DOAJ
description Environmentally friendly facile synthesis of aryl dithiocarbamates via a one-pot procedure by the reaction between secondary amines and carbon disulphide produced dithiocarbamates, which underwent copper-assisted intermolecular CS cross-coupling with aryl Iodides are developed. Cu2O is employed as a catalyst and water used as a green solvent, owing to their high reaction efficiency and benign reaction conditions in the context of green chemistry. We demonstrated detailed studies of possible intermediates, product diversification, and in-silico properties for some of the novel S-Aryl dithiocarbamates. Further, the compound 3cg possess good binding affinity towards alpha-amylase protein in comparison with Metformin.
format Article
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issn 2211-7156
language English
publishDate 2025-05-01
publisher Elsevier
record_format Article
series Results in Chemistry
spelling doaj-art-8a5a56672ab143cbb24811a6f98fded62025-08-20T03:10:42ZengElsevierResults in Chemistry2211-71562025-05-011510225710.1016/j.rechem.2025.102257Synthesis of S-aryl dithiocarbamates and its in-silico studiesKrishnarao Jayaram Desai0Murugesan Santhosh1Padmanaban Akashvarunan2Ponraj Abarna3Boopathi Shagunthala Hariprasad4Sundaram Ganesh Babu5Annamalai Pratheepkumar6Department of Chemistry, School of Advanced Sciences, Vellore Institute of Technology, Vellore, Tamil Nadu 632014, IndiaDepartment of Chemistry, School of Advanced Sciences, Vellore Institute of Technology, Vellore, Tamil Nadu 632014, IndiaDepartment of Chemistry, School of Advanced Sciences, Vellore Institute of Technology, Vellore, Tamil Nadu 632014, IndiaDepartment of Chemistry, School of Advanced Sciences, Vellore Institute of Technology, Vellore, Tamil Nadu 632014, IndiaNano-Catalysis Research Lab, Department of Chemistry, School of Advanced Sciences, Vellore Institute of Technology, Vellore, Tamil Nadu 632014, IndiaNano-Catalysis Research Lab, Department of Chemistry, School of Advanced Sciences, Vellore Institute of Technology, Vellore, Tamil Nadu 632014, IndiaDepartment of Chemistry, School of Advanced Sciences, Vellore Institute of Technology, Vellore, Tamil Nadu 632014, India; Corresponding author.Environmentally friendly facile synthesis of aryl dithiocarbamates via a one-pot procedure by the reaction between secondary amines and carbon disulphide produced dithiocarbamates, which underwent copper-assisted intermolecular CS cross-coupling with aryl Iodides are developed. Cu2O is employed as a catalyst and water used as a green solvent, owing to their high reaction efficiency and benign reaction conditions in the context of green chemistry. We demonstrated detailed studies of possible intermediates, product diversification, and in-silico properties for some of the novel S-Aryl dithiocarbamates. Further, the compound 3cg possess good binding affinity towards alpha-amylase protein in comparison with Metformin.http://www.sciencedirect.com/science/article/pii/S2211715625002401CS couplingGreen solventLate-stage functionalizationIn-silicoMolecular docking
spellingShingle Krishnarao Jayaram Desai
Murugesan Santhosh
Padmanaban Akashvarunan
Ponraj Abarna
Boopathi Shagunthala Hariprasad
Sundaram Ganesh Babu
Annamalai Pratheepkumar
Synthesis of S-aryl dithiocarbamates and its in-silico studies
Results in Chemistry
CS coupling
Green solvent
Late-stage functionalization
In-silico
Molecular docking
title Synthesis of S-aryl dithiocarbamates and its in-silico studies
title_full Synthesis of S-aryl dithiocarbamates and its in-silico studies
title_fullStr Synthesis of S-aryl dithiocarbamates and its in-silico studies
title_full_unstemmed Synthesis of S-aryl dithiocarbamates and its in-silico studies
title_short Synthesis of S-aryl dithiocarbamates and its in-silico studies
title_sort synthesis of s aryl dithiocarbamates and its in silico studies
topic CS coupling
Green solvent
Late-stage functionalization
In-silico
Molecular docking
url http://www.sciencedirect.com/science/article/pii/S2211715625002401
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AT murugesansanthosh synthesisofsaryldithiocarbamatesanditsinsilicostudies
AT padmanabanakashvarunan synthesisofsaryldithiocarbamatesanditsinsilicostudies
AT ponrajabarna synthesisofsaryldithiocarbamatesanditsinsilicostudies
AT boopathishagunthalahariprasad synthesisofsaryldithiocarbamatesanditsinsilicostudies
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