Carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide production

The photocatalytic hydrogen peroxide (H2O2) production by graphitic carbon nitride is a sustainable and environment-benign alternative approach of conventional anthraquinone autoxidation technology, but it is great challenges to promote two-electron O2 reduction and water oxidation. Herein, we prese...

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Main Authors: Ke Kong, Hong Zhong, Dejian Chen, Fushuai Zhang, Xiaoju Li, Ruihu Wang
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2025-07-01
Series:Green Energy & Environment
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Online Access:http://www.sciencedirect.com/science/article/pii/S2468025725000044
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author Ke Kong
Hong Zhong
Dejian Chen
Fushuai Zhang
Xiaoju Li
Ruihu Wang
author_facet Ke Kong
Hong Zhong
Dejian Chen
Fushuai Zhang
Xiaoju Li
Ruihu Wang
author_sort Ke Kong
collection DOAJ
description The photocatalytic hydrogen peroxide (H2O2) production by graphitic carbon nitride is a sustainable and environment-benign alternative approach of conventional anthraquinone autoxidation technology, but it is great challenges to promote two-electron O2 reduction and water oxidation. Herein, we present the well-dispersed graphitic carbon nitride quantum dots decorated with cyano groups (Na-CNQD and K-CNQD) by thermal polymerization of melamine in the presence of metal fluoride. The quantum confinement and edge effect have endowed the photocatalysts with rich active sites, wide light absorption range and the inhibited charge recombination. The cyano moieties function as O2 reduction centers to accept the photogenerated electrons and facilitate their rapid transfer to O2 molecules. This process enables the selective two-electron reduction of O2, leading to the production of H2O2. Concurrently, the valence band holes on the heptazine moiety oxidize water into H2O2. These synergistic effects promote photocatalytic H2O2 production from O2 and H2O without the need for additional photosensitizers, organic scavengers and co-catalysts. In contrast, pristine carbon nitride nanosheets remain inactive under the same conditions. This study offers new strategies for rational design of carbon-based materials for solar-to-chemical energy conversion.
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institution Kabale University
issn 2468-0257
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publishDate 2025-07-01
publisher KeAi Communications Co., Ltd.
record_format Article
series Green Energy & Environment
spelling doaj-art-89a87b2dbb0748bb958bfa15634dc70e2025-08-20T03:32:23ZengKeAi Communications Co., Ltd.Green Energy & Environment2468-02572025-07-011071551155810.1016/j.gee.2025.01.004Carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide productionKe Kong0Hong Zhong1Dejian Chen2Fushuai Zhang3Xiaoju Li4Ruihu Wang5Hebei Key Laboratory of Functional Polymer, School of Chemical Engineering and Technology, Hebei University of Technology, Tianjin, 300130, China; State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, ChinaKey Laboratory of Jiangxi Province for Special Optoelectronic Artificial Crystal Materials, School of Chemistry and Chemical Engineering, Jinggangshan University, Ji'an, Jiangxi, 343009, China; State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China; Corresponding authors. Key Laboratory of Jiangxi Province for Special Optoelectronic Artificial Crystal Materials, School of Chemistry and Chemical Engineering, Jinggangshan University, Ji'an, Jiangxi, 343009, China.State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, ChinaHebei Key Laboratory of Functional Polymer, School of Chemical Engineering and Technology, Hebei University of Technology, Tianjin, 300130, ChinaHebei Key Laboratory of Functional Polymer, School of Chemical Engineering and Technology, Hebei University of Technology, Tianjin, 300130, China; State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, ChinaHebei Key Laboratory of Functional Polymer, School of Chemical Engineering and Technology, Hebei University of Technology, Tianjin, 300130, China; Key Laboratory of Jiangxi Province for Special Optoelectronic Artificial Crystal Materials, School of Chemistry and Chemical Engineering, Jinggangshan University, Ji'an, Jiangxi, 343009, China; State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China; Corresponding authors. Key Laboratory of Jiangxi Province for Special Optoelectronic Artificial Crystal Materials, School of Chemistry and Chemical Engineering, Jinggangshan University, Ji'an, Jiangxi, 343009, China.The photocatalytic hydrogen peroxide (H2O2) production by graphitic carbon nitride is a sustainable and environment-benign alternative approach of conventional anthraquinone autoxidation technology, but it is great challenges to promote two-electron O2 reduction and water oxidation. Herein, we present the well-dispersed graphitic carbon nitride quantum dots decorated with cyano groups (Na-CNQD and K-CNQD) by thermal polymerization of melamine in the presence of metal fluoride. The quantum confinement and edge effect have endowed the photocatalysts with rich active sites, wide light absorption range and the inhibited charge recombination. The cyano moieties function as O2 reduction centers to accept the photogenerated electrons and facilitate their rapid transfer to O2 molecules. This process enables the selective two-electron reduction of O2, leading to the production of H2O2. Concurrently, the valence band holes on the heptazine moiety oxidize water into H2O2. These synergistic effects promote photocatalytic H2O2 production from O2 and H2O without the need for additional photosensitizers, organic scavengers and co-catalysts. In contrast, pristine carbon nitride nanosheets remain inactive under the same conditions. This study offers new strategies for rational design of carbon-based materials for solar-to-chemical energy conversion.http://www.sciencedirect.com/science/article/pii/S2468025725000044PhotocatalysisCarbon nitrideHydrogen peroxideQuantum dotsCyano groups
spellingShingle Ke Kong
Hong Zhong
Dejian Chen
Fushuai Zhang
Xiaoju Li
Ruihu Wang
Carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide production
Green Energy & Environment
Photocatalysis
Carbon nitride
Hydrogen peroxide
Quantum dots
Cyano groups
title Carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide production
title_full Carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide production
title_fullStr Carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide production
title_full_unstemmed Carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide production
title_short Carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide production
title_sort carbon nitride quantum dots decorated with cyano groups for boosting photocatalytic hydrogen peroxide production
topic Photocatalysis
Carbon nitride
Hydrogen peroxide
Quantum dots
Cyano groups
url http://www.sciencedirect.com/science/article/pii/S2468025725000044
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AT fushuaizhang carbonnitridequantumdotsdecoratedwithcyanogroupsforboostingphotocatalytichydrogenperoxideproduction
AT xiaojuli carbonnitridequantumdotsdecoratedwithcyanogroupsforboostingphotocatalytichydrogenperoxideproduction
AT ruihuwang carbonnitridequantumdotsdecoratedwithcyanogroupsforboostingphotocatalytichydrogenperoxideproduction