Zinc Oxide/Molybdenum Disulfide as Nanocomposite for Multifunctional Sensor Prototype

Different materials are studied for environmental gas sensors as well as photodetection prototypes. A ZnO/MoS<sub>2</sub> p-n junction was synthetized to act as a multifunctional sensor prototype. After the ZnO was prepared on a silicon substrate by using DC sputtering at room temperatur...

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Main Authors: Netzahualcóyotl Palomera, Peter Feng
Format: Article
Language:English
Published: MDPI AG 2025-03-01
Series:Micromachines
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Online Access:https://www.mdpi.com/2072-666X/16/4/358
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author Netzahualcóyotl Palomera
Peter Feng
author_facet Netzahualcóyotl Palomera
Peter Feng
author_sort Netzahualcóyotl Palomera
collection DOAJ
description Different materials are studied for environmental gas sensors as well as photodetection prototypes. A ZnO/MoS<sub>2</sub> p-n junction was synthetized to act as a multifunctional sensor prototype. After the ZnO was prepared on a silicon substrate by using DC sputtering at room temperature, molybdenum disulfide layers were spin-coated on a nanostructured zinc oxide flake-shaped surface to form an active layer. The heterostructure’s composite surface was examined using scanning electron microscopy, energy-dispersed X-ray, and Raman spectroscopy. Responses to light frequencies, light intensities, and gas chemical tracing were characterized, revealing an enhanced multifunctional performance of the prototype. Characterizations of light-induced photocurrents indicted that the obtained response strength (photocurrent/illumination light power) was up to 0.01 A/W, and the response time was less than 5 ms. In contrast, the gas-sensing measurements showed that its response strength (variation in resistance/original resistance) was up to 3.7% and the response time was down to 150 s when the prototype was exposed to ammonia gas, with the concentration down to 168 ppm. The fabricated prototype appears to have high stability and reproducibility, quick response and recovery times, as well as a high signal-to-noise ratio.
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spelling doaj-art-897d64f5ea5b4807af3c33cf7f9012aa2025-08-20T02:28:32ZengMDPI AGMicromachines2072-666X2025-03-0116435810.3390/mi16040358Zinc Oxide/Molybdenum Disulfide as Nanocomposite for Multifunctional Sensor PrototypeNetzahualcóyotl Palomera0Peter Feng1Department of Physics, University of Puerto Rico, San Juan, PR 00931, USADepartment of Physics, University of Puerto Rico, San Juan, PR 00931, USADifferent materials are studied for environmental gas sensors as well as photodetection prototypes. A ZnO/MoS<sub>2</sub> p-n junction was synthetized to act as a multifunctional sensor prototype. After the ZnO was prepared on a silicon substrate by using DC sputtering at room temperature, molybdenum disulfide layers were spin-coated on a nanostructured zinc oxide flake-shaped surface to form an active layer. The heterostructure’s composite surface was examined using scanning electron microscopy, energy-dispersed X-ray, and Raman spectroscopy. Responses to light frequencies, light intensities, and gas chemical tracing were characterized, revealing an enhanced multifunctional performance of the prototype. Characterizations of light-induced photocurrents indicted that the obtained response strength (photocurrent/illumination light power) was up to 0.01 A/W, and the response time was less than 5 ms. In contrast, the gas-sensing measurements showed that its response strength (variation in resistance/original resistance) was up to 3.7% and the response time was down to 150 s when the prototype was exposed to ammonia gas, with the concentration down to 168 ppm. The fabricated prototype appears to have high stability and reproducibility, quick response and recovery times, as well as a high signal-to-noise ratio.https://www.mdpi.com/2072-666X/16/4/358multifunctional composite structurestwo-dimensional semiconductorsmolybdenum disulfidephotodetectiongas chemical tracing
spellingShingle Netzahualcóyotl Palomera
Peter Feng
Zinc Oxide/Molybdenum Disulfide as Nanocomposite for Multifunctional Sensor Prototype
Micromachines
multifunctional composite structures
two-dimensional semiconductors
molybdenum disulfide
photodetection
gas chemical tracing
title Zinc Oxide/Molybdenum Disulfide as Nanocomposite for Multifunctional Sensor Prototype
title_full Zinc Oxide/Molybdenum Disulfide as Nanocomposite for Multifunctional Sensor Prototype
title_fullStr Zinc Oxide/Molybdenum Disulfide as Nanocomposite for Multifunctional Sensor Prototype
title_full_unstemmed Zinc Oxide/Molybdenum Disulfide as Nanocomposite for Multifunctional Sensor Prototype
title_short Zinc Oxide/Molybdenum Disulfide as Nanocomposite for Multifunctional Sensor Prototype
title_sort zinc oxide molybdenum disulfide as nanocomposite for multifunctional sensor prototype
topic multifunctional composite structures
two-dimensional semiconductors
molybdenum disulfide
photodetection
gas chemical tracing
url https://www.mdpi.com/2072-666X/16/4/358
work_keys_str_mv AT netzahualcoyotlpalomera zincoxidemolybdenumdisulfideasnanocompositeformultifunctionalsensorprototype
AT peterfeng zincoxidemolybdenumdisulfideasnanocompositeformultifunctionalsensorprototype