Synergistic Pd-La Catalysts on ATO for Clean Conversion of Methane into Methanol and Electricity

This study investigates the electrochemical conversion of methane to methanol using fuel-cell-type reactors with palladium- and lanthanum-based catalysts supported on antimony-doped tin oxide (ATO). The combination of these elements demonstrated promising characteristics for selective methanol produ...

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Main Authors: Paulo Victor. R. Gomes, Dolores R. R. Lazar, Gabriel Silvestrin, Victoria Amatheus Maia, Rodrigo Fernando B. de Souza, Almir Oliveira Neto
Format: Article
Language:English
Published: MDPI AG 2025-01-01
Series:Reactions
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Online Access:https://www.mdpi.com/2624-781X/6/1/2
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author Paulo Victor. R. Gomes
Dolores R. R. Lazar
Gabriel Silvestrin
Victoria Amatheus Maia
Rodrigo Fernando B. de Souza
Almir Oliveira Neto
author_facet Paulo Victor. R. Gomes
Dolores R. R. Lazar
Gabriel Silvestrin
Victoria Amatheus Maia
Rodrigo Fernando B. de Souza
Almir Oliveira Neto
author_sort Paulo Victor. R. Gomes
collection DOAJ
description This study investigates the electrochemical conversion of methane to methanol using fuel-cell-type reactors with palladium- and lanthanum-based catalysts supported on antimony-doped tin oxide (ATO). The combination of these elements demonstrated promising characteristics for selective methanol production. Transmission electron microscopy (TEM) analysis revealed the impact of lanthanum addition on palladium nanoparticles, influencing size distribution and clusters. Polarization curves and power density plots highlighted the Pd<sub>50</sub>La<sub>50</sub>/ATO catalyst, indicating an optimal palladium/lanthanum ratio for methanol optimization. FTIR analysis confirmed the presence of methanol in the reaction products, while the methanol production rate showcased the superior performance of the Pd<sub>50</sub>La<sub>50</sub>/ATO catalyst compared to other compositions. The synergistic effects between lanthanum’s water activation capability and the carbophilic nature of PdO emerged as crucial factors for the catalyst’s success.
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id doaj-art-890fb661fbc9481fbf9debfce7188b88
institution DOAJ
issn 2624-781X
language English
publishDate 2025-01-01
publisher MDPI AG
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series Reactions
spelling doaj-art-890fb661fbc9481fbf9debfce7188b882025-08-20T02:43:06ZengMDPI AGReactions2624-781X2025-01-0161210.3390/reactions6010002Synergistic Pd-La Catalysts on ATO for Clean Conversion of Methane into Methanol and ElectricityPaulo Victor. R. Gomes0Dolores R. R. Lazar1Gabriel Silvestrin2Victoria Amatheus Maia3Rodrigo Fernando B. de Souza4Almir Oliveira Neto5IPEN—CCCH (Células a Combustível e Hidrogênio), Cidade Universitária, Av. Professor Lineu Prestes, 2242, São Paulo 05508-000, SP, BrazilIPEN—CCCH (Células a Combustível e Hidrogênio), Cidade Universitária, Av. Professor Lineu Prestes, 2242, São Paulo 05508-000, SP, BrazilIPEN—CCCH (Células a Combustível e Hidrogênio), Cidade Universitária, Av. Professor Lineu Prestes, 2242, São Paulo 05508-000, SP, BrazilIPEN—CCCH (Células a Combustível e Hidrogênio), Cidade Universitária, Av. Professor Lineu Prestes, 2242, São Paulo 05508-000, SP, BrazilIPEN—CCCH (Células a Combustível e Hidrogênio), Cidade Universitária, Av. Professor Lineu Prestes, 2242, São Paulo 05508-000, SP, BrazilIPEN—CCCH (Células a Combustível e Hidrogênio), Cidade Universitária, Av. Professor Lineu Prestes, 2242, São Paulo 05508-000, SP, BrazilThis study investigates the electrochemical conversion of methane to methanol using fuel-cell-type reactors with palladium- and lanthanum-based catalysts supported on antimony-doped tin oxide (ATO). The combination of these elements demonstrated promising characteristics for selective methanol production. Transmission electron microscopy (TEM) analysis revealed the impact of lanthanum addition on palladium nanoparticles, influencing size distribution and clusters. Polarization curves and power density plots highlighted the Pd<sub>50</sub>La<sub>50</sub>/ATO catalyst, indicating an optimal palladium/lanthanum ratio for methanol optimization. FTIR analysis confirmed the presence of methanol in the reaction products, while the methanol production rate showcased the superior performance of the Pd<sub>50</sub>La<sub>50</sub>/ATO catalyst compared to other compositions. The synergistic effects between lanthanum’s water activation capability and the carbophilic nature of PdO emerged as crucial factors for the catalyst’s success.https://www.mdpi.com/2624-781X/6/1/2ATOPEM fuel cellmethanolcatalysis
spellingShingle Paulo Victor. R. Gomes
Dolores R. R. Lazar
Gabriel Silvestrin
Victoria Amatheus Maia
Rodrigo Fernando B. de Souza
Almir Oliveira Neto
Synergistic Pd-La Catalysts on ATO for Clean Conversion of Methane into Methanol and Electricity
Reactions
ATO
PEM fuel cell
methanol
catalysis
title Synergistic Pd-La Catalysts on ATO for Clean Conversion of Methane into Methanol and Electricity
title_full Synergistic Pd-La Catalysts on ATO for Clean Conversion of Methane into Methanol and Electricity
title_fullStr Synergistic Pd-La Catalysts on ATO for Clean Conversion of Methane into Methanol and Electricity
title_full_unstemmed Synergistic Pd-La Catalysts on ATO for Clean Conversion of Methane into Methanol and Electricity
title_short Synergistic Pd-La Catalysts on ATO for Clean Conversion of Methane into Methanol and Electricity
title_sort synergistic pd la catalysts on ato for clean conversion of methane into methanol and electricity
topic ATO
PEM fuel cell
methanol
catalysis
url https://www.mdpi.com/2624-781X/6/1/2
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AT doloresrrlazar synergisticpdlacatalystsonatoforcleanconversionofmethaneintomethanolandelectricity
AT gabrielsilvestrin synergisticpdlacatalystsonatoforcleanconversionofmethaneintomethanolandelectricity
AT victoriaamatheusmaia synergisticpdlacatalystsonatoforcleanconversionofmethaneintomethanolandelectricity
AT rodrigofernandobdesouza synergisticpdlacatalystsonatoforcleanconversionofmethaneintomethanolandelectricity
AT almiroliveiraneto synergisticpdlacatalystsonatoforcleanconversionofmethaneintomethanolandelectricity