Adsorption of Nitrate Ions Using Magnesium-Loaded Bamboo Powder and Nano-Sized Crushed Oyster Shells

Excess nitrate ions should be avoided in agriculture as they are absorbed by plants and ingested by humans, which can have serious effects on soil and groundwater. In this study, environmentally friendly bamboo flour and nano-sized oyster shells were used as adsorbents. The equilibrium time for nitr...

Full description

Saved in:
Bibliographic Details
Main Authors: Harada Hiroyuki, Nur Maisarah Mohamad Sarbani, Aoyagi Misturu, Jun Nishimoto
Format: Article
Language:English
Published: MDPI AG 2025-03-01
Series:Separations
Subjects:
Online Access:https://www.mdpi.com/2297-8739/12/4/76
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849713817626345472
author Harada Hiroyuki
Nur Maisarah Mohamad Sarbani
Aoyagi Misturu
Jun Nishimoto
author_facet Harada Hiroyuki
Nur Maisarah Mohamad Sarbani
Aoyagi Misturu
Jun Nishimoto
author_sort Harada Hiroyuki
collection DOAJ
description Excess nitrate ions should be avoided in agriculture as they are absorbed by plants and ingested by humans, which can have serious effects on soil and groundwater. In this study, environmentally friendly bamboo flour and nano-sized oyster shells were used as adsorbents. The equilibrium time for nitrate adsorption was found to be short, less than five minutes, and the treatment temperature had little effect on adsorption. The adsorption capacity and adsorption mechanism were investigated using experiments and adsorption isotherms. Bamboo powder treated with magnesium chloride (Mg bamboo), crushed oyster shell (oyster shell), and hydrogel induced with sodium alginate (hydrogel) were used. The maximum adsorption of nitrate ions on the magnesium-treated bamboo flour was estimated to be 399 mg NO<sub>3</sub><sup>−</sup>/g by the Dubin–Radushakevich equation (correlation coefficient 0.84), with the Langmuir (correlation coefficient 0.91) and Freundlich (correlation coefficient 0.91) equations also fitting relatively well. The D-R equation (correlation coefficient 0.938) and Freundlich equation (correlation coefficient 0.943) also fitted oyster shells relatively well. The maximum adsorption was estimated at 354 mg NO<sub>3</sub><sup>−</sup>/g. In oyster shell treatments where phosphate and nitrate ions were present, it was observed that both substances were adsorbed simultaneously. For the hydrogels, only the D-R equation (correlation coefficient 0.944) and the Freundlich isotherm were applicable. The maximum adsorption was estimated at 156 mg/g.
format Article
id doaj-art-86d3f55474ff49058be97dd1eb758b6d
institution DOAJ
issn 2297-8739
language English
publishDate 2025-03-01
publisher MDPI AG
record_format Article
series Separations
spelling doaj-art-86d3f55474ff49058be97dd1eb758b6d2025-08-20T03:13:51ZengMDPI AGSeparations2297-87392025-03-011247610.3390/separations12040076Adsorption of Nitrate Ions Using Magnesium-Loaded Bamboo Powder and Nano-Sized Crushed Oyster ShellsHarada Hiroyuki0Nur Maisarah Mohamad Sarbani1Aoyagi Misturu2Jun Nishimoto3Graduate School of Comprehensive and Scientific Research, Prefectural University of Hiroshima, Nanatsuka-machi, Shobara-shi 727-0023, JapanGraduate School of Comprehensive and Scientific Research, Prefectural University of Hiroshima, Nanatsuka-machi, Shobara-shi 727-0023, JapanGraduate School of Comprehensive and Scientific Research, Prefectural University of Hiroshima, Nanatsuka-machi, Shobara-shi 727-0023, JapanGraduate School of Comprehensive and Scientific Research, Prefectural University of Hiroshima, Nanatsuka-machi, Shobara-shi 727-0023, JapanExcess nitrate ions should be avoided in agriculture as they are absorbed by plants and ingested by humans, which can have serious effects on soil and groundwater. In this study, environmentally friendly bamboo flour and nano-sized oyster shells were used as adsorbents. The equilibrium time for nitrate adsorption was found to be short, less than five minutes, and the treatment temperature had little effect on adsorption. The adsorption capacity and adsorption mechanism were investigated using experiments and adsorption isotherms. Bamboo powder treated with magnesium chloride (Mg bamboo), crushed oyster shell (oyster shell), and hydrogel induced with sodium alginate (hydrogel) were used. The maximum adsorption of nitrate ions on the magnesium-treated bamboo flour was estimated to be 399 mg NO<sub>3</sub><sup>−</sup>/g by the Dubin–Radushakevich equation (correlation coefficient 0.84), with the Langmuir (correlation coefficient 0.91) and Freundlich (correlation coefficient 0.91) equations also fitting relatively well. The D-R equation (correlation coefficient 0.938) and Freundlich equation (correlation coefficient 0.943) also fitted oyster shells relatively well. The maximum adsorption was estimated at 354 mg NO<sub>3</sub><sup>−</sup>/g. In oyster shell treatments where phosphate and nitrate ions were present, it was observed that both substances were adsorbed simultaneously. For the hydrogels, only the D-R equation (correlation coefficient 0.944) and the Freundlich isotherm were applicable. The maximum adsorption was estimated at 156 mg/g.https://www.mdpi.com/2297-8739/12/4/76nitrate adsorptionbamboo powdernano-sized oyster shellsisotherm equations
spellingShingle Harada Hiroyuki
Nur Maisarah Mohamad Sarbani
Aoyagi Misturu
Jun Nishimoto
Adsorption of Nitrate Ions Using Magnesium-Loaded Bamboo Powder and Nano-Sized Crushed Oyster Shells
Separations
nitrate adsorption
bamboo powder
nano-sized oyster shells
isotherm equations
title Adsorption of Nitrate Ions Using Magnesium-Loaded Bamboo Powder and Nano-Sized Crushed Oyster Shells
title_full Adsorption of Nitrate Ions Using Magnesium-Loaded Bamboo Powder and Nano-Sized Crushed Oyster Shells
title_fullStr Adsorption of Nitrate Ions Using Magnesium-Loaded Bamboo Powder and Nano-Sized Crushed Oyster Shells
title_full_unstemmed Adsorption of Nitrate Ions Using Magnesium-Loaded Bamboo Powder and Nano-Sized Crushed Oyster Shells
title_short Adsorption of Nitrate Ions Using Magnesium-Loaded Bamboo Powder and Nano-Sized Crushed Oyster Shells
title_sort adsorption of nitrate ions using magnesium loaded bamboo powder and nano sized crushed oyster shells
topic nitrate adsorption
bamboo powder
nano-sized oyster shells
isotherm equations
url https://www.mdpi.com/2297-8739/12/4/76
work_keys_str_mv AT haradahiroyuki adsorptionofnitrateionsusingmagnesiumloadedbamboopowderandnanosizedcrushedoystershells
AT nurmaisarahmohamadsarbani adsorptionofnitrateionsusingmagnesiumloadedbamboopowderandnanosizedcrushedoystershells
AT aoyagimisturu adsorptionofnitrateionsusingmagnesiumloadedbamboopowderandnanosizedcrushedoystershells
AT junnishimoto adsorptionofnitrateionsusingmagnesiumloadedbamboopowderandnanosizedcrushedoystershells