Synthesis, Structure, and Antiproliferative Activity of Three Gallium(III) Azole Complexes

As part of our interest into the bioinorganic chemistry of gallium, gallium(III) complexes of the azole ligands 2,1,3-benzothiadiazole (btd), 1,2,3-benzotriazole (btaH), and 1-methyl-4,5-diphenylimidazole (L) have been isolated. Reaction of btaH or btd with GaBr3 or GaCl3 resulted in the mononuclear...

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Main Authors: Stergios Zanias, Giannis S. Papaefstathiou, Catherine P. Raptopoulou, Konstantinos T. Papazisis, Vasiliki Vala, Dimitra Zambouli, Alexandros H. Kortsaris, Dimitrios A. Kyriakidis, Theodoros F. Zafiropoulos
Format: Article
Language:English
Published: Wiley 2010-01-01
Series:Bioinorganic Chemistry and Applications
Online Access:http://dx.doi.org/10.1155/2010/168030
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author Stergios Zanias
Giannis S. Papaefstathiou
Catherine P. Raptopoulou
Konstantinos T. Papazisis
Vasiliki Vala
Dimitra Zambouli
Alexandros H. Kortsaris
Dimitrios A. Kyriakidis
Theodoros F. Zafiropoulos
author_facet Stergios Zanias
Giannis S. Papaefstathiou
Catherine P. Raptopoulou
Konstantinos T. Papazisis
Vasiliki Vala
Dimitra Zambouli
Alexandros H. Kortsaris
Dimitrios A. Kyriakidis
Theodoros F. Zafiropoulos
author_sort Stergios Zanias
collection DOAJ
description As part of our interest into the bioinorganic chemistry of gallium, gallium(III) complexes of the azole ligands 2,1,3-benzothiadiazole (btd), 1,2,3-benzotriazole (btaH), and 1-methyl-4,5-diphenylimidazole (L) have been isolated. Reaction of btaH or btd with GaBr3 or GaCl3 resulted in the mononuclear complexes [GaBr3(btaH)2] (1) and [GaCl3(btd)2] (2), respectively, while treatment of GaCl3 with L resulted in the anionic complex (LH)2[GaCl4] (3). All three complexes were characterized by single-crystal X-ray crystallography and IR spectroscopy, while their antiproliferative activities were investigated against a series of human and mouse cancer cell lines.
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spelling doaj-art-8656708668844cd8b3ed8723b449e0c62025-08-20T02:08:47ZengWileyBioinorganic Chemistry and Applications1565-36331687-479X2010-01-01201010.1155/2010/168030168030Synthesis, Structure, and Antiproliferative Activity of Three Gallium(III) Azole ComplexesStergios Zanias0Giannis S. Papaefstathiou1Catherine P. Raptopoulou2Konstantinos T. Papazisis3Vasiliki Vala4Dimitra Zambouli5Alexandros H. Kortsaris6Dimitrios A. Kyriakidis7Theodoros F. Zafiropoulos8Department of Chemistry, University of Patras, 265 04 Patras, GreeceLaboratory of Inorganic Chemistry, Department of Chemistry, National and Kapodistrian University of Athens, Panepistimiopolis, 157 71 Zografou, GreeceInstitute of Materials Science, NCSR “Demokritos”, 153 10 Aghia Paraskevi Attikis, Greece“Theagenion” Cancer Hospital, Al. Simeonides str. 2, 540 07 Thessaloniki, Greece“Theagenion” Cancer Hospital, Al. Simeonides str. 2, 540 07 Thessaloniki, Greece“Theagenion” Cancer Hospital, Al. Simeonides str. 2, 540 07 Thessaloniki, Greece“Theagenion” Cancer Hospital, Al. Simeonides str. 2, 540 07 Thessaloniki, GreeceDepartment of Chemistry, Aristotle University of Thessaloniki, 541 24 Thessaloniki, GreeceDepartment of Chemistry, University of Patras, 265 04 Patras, GreeceAs part of our interest into the bioinorganic chemistry of gallium, gallium(III) complexes of the azole ligands 2,1,3-benzothiadiazole (btd), 1,2,3-benzotriazole (btaH), and 1-methyl-4,5-diphenylimidazole (L) have been isolated. Reaction of btaH or btd with GaBr3 or GaCl3 resulted in the mononuclear complexes [GaBr3(btaH)2] (1) and [GaCl3(btd)2] (2), respectively, while treatment of GaCl3 with L resulted in the anionic complex (LH)2[GaCl4] (3). All three complexes were characterized by single-crystal X-ray crystallography and IR spectroscopy, while their antiproliferative activities were investigated against a series of human and mouse cancer cell lines.http://dx.doi.org/10.1155/2010/168030
spellingShingle Stergios Zanias
Giannis S. Papaefstathiou
Catherine P. Raptopoulou
Konstantinos T. Papazisis
Vasiliki Vala
Dimitra Zambouli
Alexandros H. Kortsaris
Dimitrios A. Kyriakidis
Theodoros F. Zafiropoulos
Synthesis, Structure, and Antiproliferative Activity of Three Gallium(III) Azole Complexes
Bioinorganic Chemistry and Applications
title Synthesis, Structure, and Antiproliferative Activity of Three Gallium(III) Azole Complexes
title_full Synthesis, Structure, and Antiproliferative Activity of Three Gallium(III) Azole Complexes
title_fullStr Synthesis, Structure, and Antiproliferative Activity of Three Gallium(III) Azole Complexes
title_full_unstemmed Synthesis, Structure, and Antiproliferative Activity of Three Gallium(III) Azole Complexes
title_short Synthesis, Structure, and Antiproliferative Activity of Three Gallium(III) Azole Complexes
title_sort synthesis structure and antiproliferative activity of three gallium iii azole complexes
url http://dx.doi.org/10.1155/2010/168030
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