Enhanced electrocatalytic hydrogen evolution with CoNiFe(Cr/V) based high entropy alloy electrodes

In this study, the electrocatalytic properties of single-phase face-centered cubic high entropy alloy electrodes with equiatomic compositions of CoNiFeCr, CoNiFeV, and CoNiFe(Cr/V) are explored for the hydrogen evolution reaction (HER) in 1M KOH and 0.5M H2SO4. Among these, the CoNiFe(Cr/V) High Ent...

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Main Authors: Tahir Nawaz, Shahbaz Ahmad, Wael Abuzaid, Faisal Mustafa, Waqas Ahmad, Sami El-Khatib, Mohamad Jawad Kaddoura, Abdul Hai Alami, Hussain Alawadhi, Mehmet Egilmez
Format: Article
Language:English
Published: AIP Publishing LLC 2025-05-01
Series:APL Materials
Online Access:http://dx.doi.org/10.1063/5.0271005
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author Tahir Nawaz
Shahbaz Ahmad
Wael Abuzaid
Faisal Mustafa
Waqas Ahmad
Sami El-Khatib
Mohamad Jawad Kaddoura
Abdul Hai Alami
Hussain Alawadhi
Mehmet Egilmez
author_facet Tahir Nawaz
Shahbaz Ahmad
Wael Abuzaid
Faisal Mustafa
Waqas Ahmad
Sami El-Khatib
Mohamad Jawad Kaddoura
Abdul Hai Alami
Hussain Alawadhi
Mehmet Egilmez
author_sort Tahir Nawaz
collection DOAJ
description In this study, the electrocatalytic properties of single-phase face-centered cubic high entropy alloy electrodes with equiatomic compositions of CoNiFeCr, CoNiFeV, and CoNiFe(Cr/V) are explored for the hydrogen evolution reaction (HER) in 1M KOH and 0.5M H2SO4. Among these, the CoNiFe(Cr/V) High Entropy Alloy (HEA) electrodes exhibited superior performance, achieving overpotentials of 277 and 45 mV (vs reference hydrogen electrode) at 10 mA/cm2 in alkaline and acidic media, respectively, surpassing their counterparts and approaching the efficiency of commercial Raney-Ni and Pt/C catalysts. Long-term stability tests, including steady state chronoamperometry and potentiodynamic cyclic voltammetry, revealed remarkable corrosion resistance in both environments. The catalytic activity was significantly enhanced by the inclusion of Cr and V. These oxyphilic elements, with their larger atomic radii, induce a heterogeneous surface charge distribution that enhances the electrocatalytic performance of the CoNiFe(Cr/V) HEA. This work highlights a promising candidate for HER applications and sets the stage for a broader exploration of high entropy alloys in advanced catalytic systems.
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issn 2166-532X
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publishDate 2025-05-01
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series APL Materials
spelling doaj-art-84c362a1638c409eac1f65e2b02aac182025-08-20T03:18:56ZengAIP Publishing LLCAPL Materials2166-532X2025-05-01135051114051114-1610.1063/5.0271005Enhanced electrocatalytic hydrogen evolution with CoNiFe(Cr/V) based high entropy alloy electrodesTahir Nawaz0Shahbaz Ahmad1Wael Abuzaid2Faisal Mustafa3Waqas Ahmad4Sami El-Khatib5Mohamad Jawad Kaddoura6Abdul Hai Alami7Hussain Alawadhi8Mehmet Egilmez9Department of Physics, College of Arts and Sciences, American University of Sharjah, Sharjah, United Arab EmiratesDepartment of Physics, College of Arts and Sciences, American University of Sharjah, Sharjah, United Arab EmiratesMaterials Research Center, American University of Sharjah, Sharjah, United Arab EmiratesDepartment of Physics, College of Arts and Sciences, American University of Sharjah, Sharjah, United Arab EmiratesMaterials Research Center, American University of Sharjah, Sharjah, United Arab EmiratesDepartment of Physics, College of Arts and Sciences, American University of Sharjah, Sharjah, United Arab EmiratesDepartment of Physics, College of Arts and Sciences, American University of Sharjah, Sharjah, United Arab EmiratesSustainable and Renewable Energy Engineering, University of Sharjah, P.O. Box 27272, Sharjah, United Arab EmiratesCenter for Advanced Materials Research, University of Sharjah, P.O. Box 27272, Sharjah, United Arab EmiratesDepartment of Physics, College of Arts and Sciences, American University of Sharjah, Sharjah, United Arab EmiratesIn this study, the electrocatalytic properties of single-phase face-centered cubic high entropy alloy electrodes with equiatomic compositions of CoNiFeCr, CoNiFeV, and CoNiFe(Cr/V) are explored for the hydrogen evolution reaction (HER) in 1M KOH and 0.5M H2SO4. Among these, the CoNiFe(Cr/V) High Entropy Alloy (HEA) electrodes exhibited superior performance, achieving overpotentials of 277 and 45 mV (vs reference hydrogen electrode) at 10 mA/cm2 in alkaline and acidic media, respectively, surpassing their counterparts and approaching the efficiency of commercial Raney-Ni and Pt/C catalysts. Long-term stability tests, including steady state chronoamperometry and potentiodynamic cyclic voltammetry, revealed remarkable corrosion resistance in both environments. The catalytic activity was significantly enhanced by the inclusion of Cr and V. These oxyphilic elements, with their larger atomic radii, induce a heterogeneous surface charge distribution that enhances the electrocatalytic performance of the CoNiFe(Cr/V) HEA. This work highlights a promising candidate for HER applications and sets the stage for a broader exploration of high entropy alloys in advanced catalytic systems.http://dx.doi.org/10.1063/5.0271005
spellingShingle Tahir Nawaz
Shahbaz Ahmad
Wael Abuzaid
Faisal Mustafa
Waqas Ahmad
Sami El-Khatib
Mohamad Jawad Kaddoura
Abdul Hai Alami
Hussain Alawadhi
Mehmet Egilmez
Enhanced electrocatalytic hydrogen evolution with CoNiFe(Cr/V) based high entropy alloy electrodes
APL Materials
title Enhanced electrocatalytic hydrogen evolution with CoNiFe(Cr/V) based high entropy alloy electrodes
title_full Enhanced electrocatalytic hydrogen evolution with CoNiFe(Cr/V) based high entropy alloy electrodes
title_fullStr Enhanced electrocatalytic hydrogen evolution with CoNiFe(Cr/V) based high entropy alloy electrodes
title_full_unstemmed Enhanced electrocatalytic hydrogen evolution with CoNiFe(Cr/V) based high entropy alloy electrodes
title_short Enhanced electrocatalytic hydrogen evolution with CoNiFe(Cr/V) based high entropy alloy electrodes
title_sort enhanced electrocatalytic hydrogen evolution with conife cr v based high entropy alloy electrodes
url http://dx.doi.org/10.1063/5.0271005
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