Synthesis and characterization of glass-ceramic sponge from borosilicate waste glass

Abstract Glass-ceramic sponges are promising structures for many technical applications. This work deals with the preparation and characterization of porous glass-ceramic using borosilicate glass waste. The particle size distribution of Pyrex waste glass used in this study was d10:42, d50:10, and d9...

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Main Author: Firas J. Hmood
Format: Article
Language:English
Published: Associação Brasileira de Cerâmica 2024-11-01
Series:Cerâmica
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132024000100314&lng=en&tlng=en
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author Firas J. Hmood
author_facet Firas J. Hmood
author_sort Firas J. Hmood
collection DOAJ
description Abstract Glass-ceramic sponges are promising structures for many technical applications. This work deals with the preparation and characterization of porous glass-ceramic using borosilicate glass waste. The particle size distribution of Pyrex waste glass used in this study was d10:42, d50:10, and d90:2 µm. Cubic samples of 1 cm3 were shaped using the replica method. A polyurethane sponge of 25 ppi was employed as a print back for the glass-ceramic sponge. A suspension of 70% solid loading was prepared for the replication. The samples were firstly annealed at 450°C for 1 h to burn out the polyurethane sponge. Then, the temperature was raised to 650, 700, and 750°C, respectively, to enhance the strength of samples. The results revealed that the density of sintered bodies at 750 °C was 0.47 g/cm3, which represents the highest value of density reached. Moreover, the fabricated glass-ceramic sponges revealed sintering temperature-dependent properties. For instance, samples sintered at 750 ºC showed compressive strength of 0.145 ± 0.15 MPa corresponding to 65% porosity.
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spelling doaj-art-84c2ca618fa84f51aa7ac9cc297bc1e62025-08-20T01:58:28ZengAssociação Brasileira de CerâmicaCerâmica1678-45532024-11-017010.1590/qspl6036Synthesis and characterization of glass-ceramic sponge from borosilicate waste glassFiras J. Hmoodhttps://orcid.org/0000-0003-0471-2067Abstract Glass-ceramic sponges are promising structures for many technical applications. This work deals with the preparation and characterization of porous glass-ceramic using borosilicate glass waste. The particle size distribution of Pyrex waste glass used in this study was d10:42, d50:10, and d90:2 µm. Cubic samples of 1 cm3 were shaped using the replica method. A polyurethane sponge of 25 ppi was employed as a print back for the glass-ceramic sponge. A suspension of 70% solid loading was prepared for the replication. The samples were firstly annealed at 450°C for 1 h to burn out the polyurethane sponge. Then, the temperature was raised to 650, 700, and 750°C, respectively, to enhance the strength of samples. The results revealed that the density of sintered bodies at 750 °C was 0.47 g/cm3, which represents the highest value of density reached. Moreover, the fabricated glass-ceramic sponges revealed sintering temperature-dependent properties. For instance, samples sintered at 750 ºC showed compressive strength of 0.145 ± 0.15 MPa corresponding to 65% porosity.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132024000100314&lng=en&tlng=enwaste glassPyrex®glass spongepolyurethanecatalysis
spellingShingle Firas J. Hmood
Synthesis and characterization of glass-ceramic sponge from borosilicate waste glass
Cerâmica
waste glass
Pyrex®
glass sponge
polyurethane
catalysis
title Synthesis and characterization of glass-ceramic sponge from borosilicate waste glass
title_full Synthesis and characterization of glass-ceramic sponge from borosilicate waste glass
title_fullStr Synthesis and characterization of glass-ceramic sponge from borosilicate waste glass
title_full_unstemmed Synthesis and characterization of glass-ceramic sponge from borosilicate waste glass
title_short Synthesis and characterization of glass-ceramic sponge from borosilicate waste glass
title_sort synthesis and characterization of glass ceramic sponge from borosilicate waste glass
topic waste glass
Pyrex®
glass sponge
polyurethane
catalysis
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132024000100314&lng=en&tlng=en
work_keys_str_mv AT firasjhmood synthesisandcharacterizationofglassceramicspongefromborosilicatewasteglass