Manufacturing of environment friendly biolubricants from vegetable oils

Environment friendly products such as fuels and lubricants are among the candidates which are studied in several countries including Egypt. The purpose of this work was to utilize commercially available palm oil and Jatropha oil for the production of biolubricants, through two stages of Transesterif...

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Main Authors: Ebtisam K. Heikal, M.S. Elmelawy, Salah A. Khalil, N.M. Elbasuny
Format: Article
Language:English
Published: Egyptian Petroleum Research Institute 2017-03-01
Series:Egyptian Journal of Petroleum
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Online Access:http://www.sciencedirect.com/science/article/pii/S1110062115301057
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author Ebtisam K. Heikal
M.S. Elmelawy
Salah A. Khalil
N.M. Elbasuny
author_facet Ebtisam K. Heikal
M.S. Elmelawy
Salah A. Khalil
N.M. Elbasuny
author_sort Ebtisam K. Heikal
collection DOAJ
description Environment friendly products such as fuels and lubricants are among the candidates which are studied in several countries including Egypt. The purpose of this work was to utilize commercially available palm oil and Jatropha oil for the production of biolubricants, through two stages of Transesterification. The first stage is the process of using methanol in the presence of potassium hydroxide to produce biodiesel. The second stage is the reaction of biodiesel with trimethylolpropane using sodium methoxide as catalyst to yield palm or Jatropha oil base trimethylolpropane esters (biolubricants). Palm oil based trimethylolpropane esters with yield of 97.8% was obtained after 4 h of reaction at 130 °C. Under similar reaction conditions, Jatropha oil based trimethylolpropane esters with a yield of 98.2% was obtained. The resulting products were confirmed by FTIR and evaluated by ASTM analyses. The obtained Jatropha oil based trimethylolpropane esters exhibited high viscosity indices (140), low pour point temperature (−3 °C), and moderate thermal stabilities and met the requirement of commercial industrial oil ISO VG46 grade. In spite of the high pour point of Palm oil based trimethylolpropane esters (5 °C), which needs pour point depressant to reduce the pour point, other lubrication properties such as viscosity, viscosity indices and flash point are comparable to commercial industrial oil ISO VG32 and VG46.
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spelling doaj-art-8466fb545bcb4d3ba50e0d9b324087362025-08-20T01:58:20ZengEgyptian Petroleum Research InstituteEgyptian Journal of Petroleum1110-06212017-03-01261535910.1016/j.ejpe.2016.03.003Manufacturing of environment friendly biolubricants from vegetable oilsEbtisam K. HeikalM.S. ElmelawySalah A. KhalilN.M. ElbasunyEnvironment friendly products such as fuels and lubricants are among the candidates which are studied in several countries including Egypt. The purpose of this work was to utilize commercially available palm oil and Jatropha oil for the production of biolubricants, through two stages of Transesterification. The first stage is the process of using methanol in the presence of potassium hydroxide to produce biodiesel. The second stage is the reaction of biodiesel with trimethylolpropane using sodium methoxide as catalyst to yield palm or Jatropha oil base trimethylolpropane esters (biolubricants). Palm oil based trimethylolpropane esters with yield of 97.8% was obtained after 4 h of reaction at 130 °C. Under similar reaction conditions, Jatropha oil based trimethylolpropane esters with a yield of 98.2% was obtained. The resulting products were confirmed by FTIR and evaluated by ASTM analyses. The obtained Jatropha oil based trimethylolpropane esters exhibited high viscosity indices (140), low pour point temperature (−3 °C), and moderate thermal stabilities and met the requirement of commercial industrial oil ISO VG46 grade. In spite of the high pour point of Palm oil based trimethylolpropane esters (5 °C), which needs pour point depressant to reduce the pour point, other lubrication properties such as viscosity, viscosity indices and flash point are comparable to commercial industrial oil ISO VG32 and VG46.http://www.sciencedirect.com/science/article/pii/S1110062115301057BiodieselBiolubricantTransesterificationPalm oil methyl esterJatropha oil methyl ester
spellingShingle Ebtisam K. Heikal
M.S. Elmelawy
Salah A. Khalil
N.M. Elbasuny
Manufacturing of environment friendly biolubricants from vegetable oils
Egyptian Journal of Petroleum
Biodiesel
Biolubricant
Transesterification
Palm oil methyl ester
Jatropha oil methyl ester
title Manufacturing of environment friendly biolubricants from vegetable oils
title_full Manufacturing of environment friendly biolubricants from vegetable oils
title_fullStr Manufacturing of environment friendly biolubricants from vegetable oils
title_full_unstemmed Manufacturing of environment friendly biolubricants from vegetable oils
title_short Manufacturing of environment friendly biolubricants from vegetable oils
title_sort manufacturing of environment friendly biolubricants from vegetable oils
topic Biodiesel
Biolubricant
Transesterification
Palm oil methyl ester
Jatropha oil methyl ester
url http://www.sciencedirect.com/science/article/pii/S1110062115301057
work_keys_str_mv AT ebtisamkheikal manufacturingofenvironmentfriendlybiolubricantsfromvegetableoils
AT mselmelawy manufacturingofenvironmentfriendlybiolubricantsfromvegetableoils
AT salahakhalil manufacturingofenvironmentfriendlybiolubricantsfromvegetableoils
AT nmelbasuny manufacturingofenvironmentfriendlybiolubricantsfromvegetableoils