Practical Enzymatic Resolution of Chiral Auxiliaries – Enantiomerically Pure trans-2-Phenylcyclohexanol and trans-2-(α-Cumyl)cyclohexanol

Commercially available, crude pig liver material (Pig Liver Acetone Powder, PLAP) is demonstrated to be effective for the preparation of enantiomerically pure alcohols that are, in turn, effective chiral auxiliaries for asymmetric induction. Resolution of the title alcohols in large scale is effect...

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Main Authors: James K. Whitesell, Robert M. Lawrence
Format: Article
Language:deu
Published: Swiss Chemical Society 1986-09-01
Series:CHIMIA
Online Access:https://www.chimia.ch/chimia/article/view/9750
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author James K. Whitesell
Robert M. Lawrence
author_facet James K. Whitesell
Robert M. Lawrence
author_sort James K. Whitesell
collection DOAJ
description Commercially available, crude pig liver material (Pig Liver Acetone Powder, PLAP) is demonstrated to be effective for the preparation of enantiomerically pure alcohols that are, in turn, effective chiral auxiliaries for asymmetric induction. Resolution of the title alcohols in large scale is effected by selective enzymatic cleavage of the corresponding acetic acid esters.
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publishDate 1986-09-01
publisher Swiss Chemical Society
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series CHIMIA
spelling doaj-art-83ff6ebe314542f9872eec3811effeab2025-08-20T01:47:43ZdeuSwiss Chemical SocietyCHIMIA0009-42932673-24241986-09-0140910.2533/chimia.1986.318Practical Enzymatic Resolution of Chiral Auxiliaries – Enantiomerically Pure trans-2-Phenylcyclohexanol and trans-2-(α-Cumyl)cyclohexanolJames K. Whitesell0Robert M. Lawrence1Department of Chemistry The University of Texas at Austin Austin, TX 78712 (USA)Department of Chemistry The University of Texas at Austin Austin, TX 78712 (USA) Commercially available, crude pig liver material (Pig Liver Acetone Powder, PLAP) is demonstrated to be effective for the preparation of enantiomerically pure alcohols that are, in turn, effective chiral auxiliaries for asymmetric induction. Resolution of the title alcohols in large scale is effected by selective enzymatic cleavage of the corresponding acetic acid esters. https://www.chimia.ch/chimia/article/view/9750
spellingShingle James K. Whitesell
Robert M. Lawrence
Practical Enzymatic Resolution of Chiral Auxiliaries – Enantiomerically Pure trans-2-Phenylcyclohexanol and trans-2-(α-Cumyl)cyclohexanol
CHIMIA
title Practical Enzymatic Resolution of Chiral Auxiliaries – Enantiomerically Pure trans-2-Phenylcyclohexanol and trans-2-(α-Cumyl)cyclohexanol
title_full Practical Enzymatic Resolution of Chiral Auxiliaries – Enantiomerically Pure trans-2-Phenylcyclohexanol and trans-2-(α-Cumyl)cyclohexanol
title_fullStr Practical Enzymatic Resolution of Chiral Auxiliaries – Enantiomerically Pure trans-2-Phenylcyclohexanol and trans-2-(α-Cumyl)cyclohexanol
title_full_unstemmed Practical Enzymatic Resolution of Chiral Auxiliaries – Enantiomerically Pure trans-2-Phenylcyclohexanol and trans-2-(α-Cumyl)cyclohexanol
title_short Practical Enzymatic Resolution of Chiral Auxiliaries – Enantiomerically Pure trans-2-Phenylcyclohexanol and trans-2-(α-Cumyl)cyclohexanol
title_sort practical enzymatic resolution of chiral auxiliaries enantiomerically pure trans 2 phenylcyclohexanol and trans 2 α cumyl cyclohexanol
url https://www.chimia.ch/chimia/article/view/9750
work_keys_str_mv AT jameskwhitesell practicalenzymaticresolutionofchiralauxiliariesenantiomericallypuretrans2phenylcyclohexanolandtrans2acumylcyclohexanol
AT robertmlawrence practicalenzymaticresolutionofchiralauxiliariesenantiomericallypuretrans2phenylcyclohexanolandtrans2acumylcyclohexanol