Investigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurement

The purpose of this study is to elucidate the origin of the additional response signals arising from the surface topography of samples during piezoresponse force microscopy (PFM) measurements. Periodic mountain-shaped protrusions with triangular cross-sections were fabricated on the surface of a sil...

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Main Authors: Shotaro IKEMOTO, Masataka ABE, Azusa N. HATTORI, Takashi SUMIGAWA
Format: Article
Language:Japanese
Published: The Japan Society of Mechanical Engineers 2025-04-01
Series:Nihon Kikai Gakkai ronbunshu
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Online Access:https://www.jstage.jst.go.jp/article/transjsme/91/944/91_25-00034/_pdf/-char/en
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author Shotaro IKEMOTO
Masataka ABE
Azusa N. HATTORI
Takashi SUMIGAWA
author_facet Shotaro IKEMOTO
Masataka ABE
Azusa N. HATTORI
Takashi SUMIGAWA
author_sort Shotaro IKEMOTO
collection DOAJ
description The purpose of this study is to elucidate the origin of the additional response signals arising from the surface topography of samples during piezoresponse force microscopy (PFM) measurements. Periodic mountain-shaped protrusions with triangular cross-sections were fabricated on the surface of a silicon single crystal, a material with no inherent piezoelectricity, and PFM measurements were performed. The results indicated that when the measurement sensitivity direction of the PFM and the ridge direction of the protrusions formed specific angles, piezoelectric response images influenced by the surface topography were generated. Two-dimensional electrostatic field analysis confirmed that the contribution of converse flexoelectricity to this phenomenon was very small and negligible. Conversely, PFM measurements conducted both in-plane and out-of-plane on the sample, as well as measurements on a conductive material, revealed that the additional piezoelectric response - which was dependent on the surface topography - was induced by electrostatic forces due to the charging of the sample surface. The signal intensity was found to increase as the angle between the direction of the inclined plane and the in-plane sensitivity direction became smaller, as the tip diameter increased. These findings highlight the importance of accounting for the dominant influence of electrostatic forces in the interpretation of piezoelectric response data. Furthermore, they provide valuable insights into the effect of sample topography on PFM measurements.
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institution DOAJ
issn 2187-9761
language Japanese
publishDate 2025-04-01
publisher The Japan Society of Mechanical Engineers
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series Nihon Kikai Gakkai ronbunshu
spelling doaj-art-8211ee87a7a44e38bf41906b3d4579bd2025-08-20T02:56:02ZjpnThe Japan Society of Mechanical EngineersNihon Kikai Gakkai ronbunshu2187-97612025-04-019194425-0003425-0003410.1299/transjsme.25-00034transjsmeInvestigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurementShotaro IKEMOTO0Masataka ABE1Azusa N. HATTORI2Takashi SUMIGAWA3Graduate School of Energy Science, Kyoto UniversityGraduate School of Energy Science, Kyoto UniversitySANKEN (The Institute of Scientific and Industrial Research; ISIR), Osaka UniversityGraduate School of Energy Science, Kyoto UniversityThe purpose of this study is to elucidate the origin of the additional response signals arising from the surface topography of samples during piezoresponse force microscopy (PFM) measurements. Periodic mountain-shaped protrusions with triangular cross-sections were fabricated on the surface of a silicon single crystal, a material with no inherent piezoelectricity, and PFM measurements were performed. The results indicated that when the measurement sensitivity direction of the PFM and the ridge direction of the protrusions formed specific angles, piezoelectric response images influenced by the surface topography were generated. Two-dimensional electrostatic field analysis confirmed that the contribution of converse flexoelectricity to this phenomenon was very small and negligible. Conversely, PFM measurements conducted both in-plane and out-of-plane on the sample, as well as measurements on a conductive material, revealed that the additional piezoelectric response - which was dependent on the surface topography - was induced by electrostatic forces due to the charging of the sample surface. The signal intensity was found to increase as the angle between the direction of the inclined plane and the in-plane sensitivity direction became smaller, as the tip diameter increased. These findings highlight the importance of accounting for the dominant influence of electrostatic forces in the interpretation of piezoelectric response data. Furthermore, they provide valuable insights into the effect of sample topography on PFM measurements.https://www.jstage.jst.go.jp/article/transjsme/91/944/91_25-00034/_pdf/-char/enpiezoresponse force microscopyelectrostatic forceelectrostatic field simulationconverse flexoelectricityferroelectrics
spellingShingle Shotaro IKEMOTO
Masataka ABE
Azusa N. HATTORI
Takashi SUMIGAWA
Investigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurement
Nihon Kikai Gakkai ronbunshu
piezoresponse force microscopy
electrostatic force
electrostatic field simulation
converse flexoelectricity
ferroelectrics
title Investigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurement
title_full Investigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurement
title_fullStr Investigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurement
title_full_unstemmed Investigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurement
title_short Investigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurement
title_sort investigation of additional responses caused by sample surface topography in piezoresponse force microscopy measurement
topic piezoresponse force microscopy
electrostatic force
electrostatic field simulation
converse flexoelectricity
ferroelectrics
url https://www.jstage.jst.go.jp/article/transjsme/91/944/91_25-00034/_pdf/-char/en
work_keys_str_mv AT shotaroikemoto investigationofadditionalresponsescausedbysamplesurfacetopographyinpiezoresponseforcemicroscopymeasurement
AT masatakaabe investigationofadditionalresponsescausedbysamplesurfacetopographyinpiezoresponseforcemicroscopymeasurement
AT azusanhattori investigationofadditionalresponsescausedbysamplesurfacetopographyinpiezoresponseforcemicroscopymeasurement
AT takashisumigawa investigationofadditionalresponsescausedbysamplesurfacetopographyinpiezoresponseforcemicroscopymeasurement