High-quality epitaxial, homogeneous anatase thin films by on-site controlled hydrolysis on LaAlO3 substrates and characterization

The anatase form of TiO₂ is a widely studied material due to its broad range of applications. Epitaxial anatase thin films have attracted significant attention because of their enhanced electrical and optical properties. However, fabricating anatase thin films remains challenging due to their metast...

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Main Authors: Sudu Hakuruge Dilan Priyankara Wijekoon, Kosuke Ono, Masaru Shimomura, Takahiko Kawaguchi, Naonori Sakamoto, Naoki Wakiya
Format: Article
Language:English
Published: Taylor & Francis Group 2025-12-01
Series:Science and Technology of Advanced Materials
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Online Access:https://www.tandfonline.com/doi/10.1080/14686996.2025.2518747
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author Sudu Hakuruge Dilan Priyankara Wijekoon
Kosuke Ono
Masaru Shimomura
Takahiko Kawaguchi
Naonori Sakamoto
Naoki Wakiya
author_facet Sudu Hakuruge Dilan Priyankara Wijekoon
Kosuke Ono
Masaru Shimomura
Takahiko Kawaguchi
Naonori Sakamoto
Naoki Wakiya
author_sort Sudu Hakuruge Dilan Priyankara Wijekoon
collection DOAJ
description The anatase form of TiO₂ is a widely studied material due to its broad range of applications. Epitaxial anatase thin films have attracted significant attention because of their enhanced electrical and optical properties. However, fabricating anatase thin films remains challenging due to their metastability and the need for highly sophisticated fabrication techniques. On-site controlled hydrolysis is a simple, cost-effective, and rapid method for producing smooth, compact thin films on various surfaces. In this study, we demonstrate a straightforward approach to fabricating highly oriented epitaxial anatase thin films on LaAlO₃ substrates using different solvent mixtures. The epitaxial orientation and film quality were analyzed using X-ray diffraction pole figures and rocking curves, while surface morphology was characterized by Scanning electron microscopy and atomic force microscopy. Our results indicate that thin film quality and morphology are primarily influenced by the annealing temperature rather than the choice of solvent or titanium precursor, confirming the feasibility of a scalable, low-cost epitaxial fabrication technique for anatase thin films.
format Article
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issn 1468-6996
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language English
publishDate 2025-12-01
publisher Taylor & Francis Group
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series Science and Technology of Advanced Materials
spelling doaj-art-8180ffbe05314f20b8431f25d776091c2025-08-20T03:11:37ZengTaylor & Francis GroupScience and Technology of Advanced Materials1468-69961878-55142025-12-0126110.1080/14686996.2025.2518747High-quality epitaxial, homogeneous anatase thin films by on-site controlled hydrolysis on LaAlO3 substrates and characterizationSudu Hakuruge Dilan Priyankara Wijekoon0Kosuke Ono1Masaru Shimomura2Takahiko Kawaguchi3Naonori Sakamoto4Naoki Wakiya5Graduate School of Science and Technology, Shizuoka University, Hamamatsu, JapanGraduate School of Science and Technology, Shizuoka University, Hamamatsu, JapanGraduate School of Science and Technology, Shizuoka University, Hamamatsu, JapanGraduate School of Integrated Science and Technology, Department of Engineering, Shizuoka University, Hamamatsu, JapanGraduate School of Science and Technology, Shizuoka University, Hamamatsu, JapanGraduate School of Science and Technology, Shizuoka University, Hamamatsu, JapanThe anatase form of TiO₂ is a widely studied material due to its broad range of applications. Epitaxial anatase thin films have attracted significant attention because of their enhanced electrical and optical properties. However, fabricating anatase thin films remains challenging due to their metastability and the need for highly sophisticated fabrication techniques. On-site controlled hydrolysis is a simple, cost-effective, and rapid method for producing smooth, compact thin films on various surfaces. In this study, we demonstrate a straightforward approach to fabricating highly oriented epitaxial anatase thin films on LaAlO₃ substrates using different solvent mixtures. The epitaxial orientation and film quality were analyzed using X-ray diffraction pole figures and rocking curves, while surface morphology was characterized by Scanning electron microscopy and atomic force microscopy. Our results indicate that thin film quality and morphology are primarily influenced by the annealing temperature rather than the choice of solvent or titanium precursor, confirming the feasibility of a scalable, low-cost epitaxial fabrication technique for anatase thin films.https://www.tandfonline.com/doi/10.1080/14686996.2025.2518747Anatase titanium dioxidesolid state epitaxyon-site controlled hydrolysis
spellingShingle Sudu Hakuruge Dilan Priyankara Wijekoon
Kosuke Ono
Masaru Shimomura
Takahiko Kawaguchi
Naonori Sakamoto
Naoki Wakiya
High-quality epitaxial, homogeneous anatase thin films by on-site controlled hydrolysis on LaAlO3 substrates and characterization
Science and Technology of Advanced Materials
Anatase titanium dioxide
solid state epitaxy
on-site controlled hydrolysis
title High-quality epitaxial, homogeneous anatase thin films by on-site controlled hydrolysis on LaAlO3 substrates and characterization
title_full High-quality epitaxial, homogeneous anatase thin films by on-site controlled hydrolysis on LaAlO3 substrates and characterization
title_fullStr High-quality epitaxial, homogeneous anatase thin films by on-site controlled hydrolysis on LaAlO3 substrates and characterization
title_full_unstemmed High-quality epitaxial, homogeneous anatase thin films by on-site controlled hydrolysis on LaAlO3 substrates and characterization
title_short High-quality epitaxial, homogeneous anatase thin films by on-site controlled hydrolysis on LaAlO3 substrates and characterization
title_sort high quality epitaxial homogeneous anatase thin films by on site controlled hydrolysis on laalo3 substrates and characterization
topic Anatase titanium dioxide
solid state epitaxy
on-site controlled hydrolysis
url https://www.tandfonline.com/doi/10.1080/14686996.2025.2518747
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