Understanding the Enhanced Separation Mechanism of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> at Low Pressure by HKUST−1

The production of ethylene (C<sub>2</sub>H<sub>4</sub>) is typically accompanied by the formation of impurities like ethane (C<sub>2</sub>H<sub>6</sub>), making the separation of C<sub>2</sub>H<sub>4</sub> and C<sub>2</...

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Main Authors: Wenpeng Xie, Qiuju Fu, Xiangjun Kong, Xiangsen Yuan, Lingzhi Yang, Liting Yan, Xuebo Zhao
Format: Article
Language:English
Published: MDPI AG 2024-10-01
Series:Chemistry
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Online Access:https://www.mdpi.com/2624-8549/6/6/77
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author Wenpeng Xie
Qiuju Fu
Xiangjun Kong
Xiangsen Yuan
Lingzhi Yang
Liting Yan
Xuebo Zhao
author_facet Wenpeng Xie
Qiuju Fu
Xiangjun Kong
Xiangsen Yuan
Lingzhi Yang
Liting Yan
Xuebo Zhao
author_sort Wenpeng Xie
collection DOAJ
description The production of ethylene (C<sub>2</sub>H<sub>4</sub>) is typically accompanied by the formation of impurities like ethane (C<sub>2</sub>H<sub>6</sub>), making the separation of C<sub>2</sub>H<sub>4</sub> and C<sub>2</sub>H<sub>6</sub> crucial in industrial processes. Here, we investigated the S-shaped adsorption phenomenon of C<sub>2</sub>H<sub>6</sub> on the metal–organic framework HKUST−1. The virial equation is used to fit the C<sub>2</sub>H<sub>6</sub> and C<sub>2</sub>H<sub>4</sub> adsorption isotherms under low coverage. The results showed that the repulsion energy between neighboring C<sub>2</sub>H<sub>6</sub> molecules was significantly higher than that between neighboring C<sub>2</sub>H<sub>4</sub> molecules, which was an important reason for the lower adsorption of C<sub>2</sub>H<sub>6</sub> by HKUST−1 at low coverage. As more molecules are adsorbed, gas molecules aggregate within pores, leading to more hydrogen bonds formed between HKUST−1 and larger-sized C<sub>2</sub>H<sub>6</sub> under high coverage conditions. This phenomenon plays a crucial role in the S-shaped adsorption behavior of HKUST−1 on C<sub>2</sub>H<sub>6</sub>. Additionally, this unique adsorption behavior allows for the efficient separation of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> mixtures at low pressures. The ideal adsorbed solution theory (IAST) selectivity of HKUST−1 for C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> mixtures was 3.78 at 283 K and 1 bar, but increased significantly to 7.53 under low pressure. This unique mechanism provides a theoretical basis for the low-pressure separation of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> by HKUST−1 and establishes a solid foundation for future practical research applications.
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spelling doaj-art-814f5a7d966946dcafdf1d5ac4aa86b82025-08-20T02:57:07ZengMDPI AGChemistry2624-85492024-10-01661326133510.3390/chemistry6060077Understanding the Enhanced Separation Mechanism of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> at Low Pressure by HKUST−1Wenpeng Xie0Qiuju Fu1Xiangjun Kong2Xiangsen Yuan3Lingzhi Yang4Liting Yan5Xuebo Zhao6School of Materials Science and Engineering, Qilu University of Technology (Shandong Academy of Sciences), Jinan 250353, ChinaSchool of Materials Science and Engineering, Qilu University of Technology (Shandong Academy of Sciences), Jinan 250353, ChinaSchool of Chemistry & Chemical Engineering and Environmental Engineering, Weifang University, Weifang 261061, ChinaSchool of Materials Science and Engineering, Qilu University of Technology (Shandong Academy of Sciences), Jinan 250353, ChinaSchool of Materials Science and Engineering, Shandong University of Science and Technology, Qingdao 266590, ChinaSchool of Materials Science and Engineering, Qilu University of Technology (Shandong Academy of Sciences), Jinan 250353, ChinaSchool of Materials Science and Engineering, Qilu University of Technology (Shandong Academy of Sciences), Jinan 250353, ChinaThe production of ethylene (C<sub>2</sub>H<sub>4</sub>) is typically accompanied by the formation of impurities like ethane (C<sub>2</sub>H<sub>6</sub>), making the separation of C<sub>2</sub>H<sub>4</sub> and C<sub>2</sub>H<sub>6</sub> crucial in industrial processes. Here, we investigated the S-shaped adsorption phenomenon of C<sub>2</sub>H<sub>6</sub> on the metal–organic framework HKUST−1. The virial equation is used to fit the C<sub>2</sub>H<sub>6</sub> and C<sub>2</sub>H<sub>4</sub> adsorption isotherms under low coverage. The results showed that the repulsion energy between neighboring C<sub>2</sub>H<sub>6</sub> molecules was significantly higher than that between neighboring C<sub>2</sub>H<sub>4</sub> molecules, which was an important reason for the lower adsorption of C<sub>2</sub>H<sub>6</sub> by HKUST−1 at low coverage. As more molecules are adsorbed, gas molecules aggregate within pores, leading to more hydrogen bonds formed between HKUST−1 and larger-sized C<sub>2</sub>H<sub>6</sub> under high coverage conditions. This phenomenon plays a crucial role in the S-shaped adsorption behavior of HKUST−1 on C<sub>2</sub>H<sub>6</sub>. Additionally, this unique adsorption behavior allows for the efficient separation of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> mixtures at low pressures. The ideal adsorbed solution theory (IAST) selectivity of HKUST−1 for C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> mixtures was 3.78 at 283 K and 1 bar, but increased significantly to 7.53 under low pressure. This unique mechanism provides a theoretical basis for the low-pressure separation of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> by HKUST−1 and establishes a solid foundation for future practical research applications.https://www.mdpi.com/2624-8549/6/6/77metal–organic frameworkethaneethyleneS-shaped adsorptionhigh IAST selectivity
spellingShingle Wenpeng Xie
Qiuju Fu
Xiangjun Kong
Xiangsen Yuan
Lingzhi Yang
Liting Yan
Xuebo Zhao
Understanding the Enhanced Separation Mechanism of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> at Low Pressure by HKUST−1
Chemistry
metal–organic framework
ethane
ethylene
S-shaped adsorption
high IAST selectivity
title Understanding the Enhanced Separation Mechanism of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> at Low Pressure by HKUST−1
title_full Understanding the Enhanced Separation Mechanism of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> at Low Pressure by HKUST−1
title_fullStr Understanding the Enhanced Separation Mechanism of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> at Low Pressure by HKUST−1
title_full_unstemmed Understanding the Enhanced Separation Mechanism of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> at Low Pressure by HKUST−1
title_short Understanding the Enhanced Separation Mechanism of C<sub>2</sub>H<sub>4</sub>/C<sub>2</sub>H<sub>6</sub> at Low Pressure by HKUST−1
title_sort understanding the enhanced separation mechanism of c sub 2 sub h sub 4 sub c sub 2 sub h sub 6 sub at low pressure by hkust 1
topic metal–organic framework
ethane
ethylene
S-shaped adsorption
high IAST selectivity
url https://www.mdpi.com/2624-8549/6/6/77
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