Exploring the factors influencing the co-pyrolysis of walnut shells, pistachio shells, and polypropylene based on thermal behavior, kinetics and reaction mechanism

The complex co-pyrolysis process of biomass with polypropylene (PP) and the limited research on microscopic reaction mechanisms have hindered its advance application in mitigating environmental issues and addressing the supply-demand imbalance of fossil fuels. In this study, walnut shells (WS) and p...

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Main Authors: Zhigang Huang, Tong Zhang, Chen Wang, Wenbo Xiao, Zihan Wang, Obid Tursunov, Jiahui Wu, Yuguang Zhou, Xiaolong Yao, Gang Li
Format: Article
Language:English
Published: Elsevier 2025-01-01
Series:Case Studies in Thermal Engineering
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Online Access:http://www.sciencedirect.com/science/article/pii/S2214157X24017106
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author Zhigang Huang
Tong Zhang
Chen Wang
Wenbo Xiao
Zihan Wang
Obid Tursunov
Jiahui Wu
Yuguang Zhou
Xiaolong Yao
Gang Li
author_facet Zhigang Huang
Tong Zhang
Chen Wang
Wenbo Xiao
Zihan Wang
Obid Tursunov
Jiahui Wu
Yuguang Zhou
Xiaolong Yao
Gang Li
author_sort Zhigang Huang
collection DOAJ
description The complex co-pyrolysis process of biomass with polypropylene (PP) and the limited research on microscopic reaction mechanisms have hindered its advance application in mitigating environmental issues and addressing the supply-demand imbalance of fossil fuels. In this study, walnut shells (WS) and pistachio shells (PS) were chosen as representative biomass materials to systematically investigate their co-pyrolysis characteristics with PP. Model-free isoconversional methods such as Flynn-Wall-Ozawa, Kissinger-Akahira-Sunose, Starink and Vyazovkin, were employed to analyze pyrolysis kinetics. The results demonstrate that the synergistic effect between PS and PP significantly decreased the activation energy of the reaction system (460.64–112.80 kJ/mol). Product analysis showed that the feedstock ratio and pyrolysis temperature had a significant effect on the composition of the product. The experimental findings indicated that at 600 °C with a PS:PP ratio of 1:2, the activation energy was minimized while the total content of phenols and hydrocarbons reached its highest level (75.42 %). By integrating thermogravimetric, kinetic, and product analyzes, this study establishes a comprehensive characterization system for understanding pyrolysis processes at multiple scale levels, providing a novel approach for optimizing pyrolysis conditions while providing theoretical guidance for designing efficient and selective pyrolysis processes.
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spelling doaj-art-7ffffd172bd7485784cf31584df341532025-08-20T02:44:46ZengElsevierCase Studies in Thermal Engineering2214-157X2025-01-016510567910.1016/j.csite.2024.105679Exploring the factors influencing the co-pyrolysis of walnut shells, pistachio shells, and polypropylene based on thermal behavior, kinetics and reaction mechanismZhigang Huang0Tong Zhang1Chen Wang2Wenbo Xiao3Zihan Wang4Obid Tursunov5Jiahui Wu6Yuguang Zhou7Xiaolong Yao8Gang Li9School of Computer and Artificial Intelligence, Beijing Technology and Business University, Beijing, 100048, ChinaSchool of Computer and Artificial Intelligence, Beijing Technology and Business University, Beijing, 100048, ChinaSchool of Computer and Artificial Intelligence, Beijing Technology and Business University, Beijing, 100048, ChinaSchool of Computer and Artificial Intelligence, Beijing Technology and Business University, Beijing, 100048, ChinaSchool of Computer and Artificial Intelligence, Beijing Technology and Business University, Beijing, 100048, ChinaBioenergy and Environment Science & Technology Laboratory, College of Engineering, China Agricultural University, Beijing, 100083, China; Department of Power Supply and Renewable Energy Sources, National Research University TIIAME, Tashkent, 100000, UzbekistanSchool of Computer and Artificial Intelligence, Beijing Technology and Business University, Beijing, 100048, ChinaBioenergy and Environment Science & Technology Laboratory, College of Engineering, China Agricultural University, Beijing, 100083, ChinaSchool of Light Industry Science and Engineering, Beijing Technology and Business University, Beijing, 100048, China; Corresponding author.School of Computer and Artificial Intelligence, Beijing Technology and Business University, Beijing, 100048, China; Corresponding author.The complex co-pyrolysis process of biomass with polypropylene (PP) and the limited research on microscopic reaction mechanisms have hindered its advance application in mitigating environmental issues and addressing the supply-demand imbalance of fossil fuels. In this study, walnut shells (WS) and pistachio shells (PS) were chosen as representative biomass materials to systematically investigate their co-pyrolysis characteristics with PP. Model-free isoconversional methods such as Flynn-Wall-Ozawa, Kissinger-Akahira-Sunose, Starink and Vyazovkin, were employed to analyze pyrolysis kinetics. The results demonstrate that the synergistic effect between PS and PP significantly decreased the activation energy of the reaction system (460.64–112.80 kJ/mol). Product analysis showed that the feedstock ratio and pyrolysis temperature had a significant effect on the composition of the product. The experimental findings indicated that at 600 °C with a PS:PP ratio of 1:2, the activation energy was minimized while the total content of phenols and hydrocarbons reached its highest level (75.42 %). By integrating thermogravimetric, kinetic, and product analyzes, this study establishes a comprehensive characterization system for understanding pyrolysis processes at multiple scale levels, providing a novel approach for optimizing pyrolysis conditions while providing theoretical guidance for designing efficient and selective pyrolysis processes.http://www.sciencedirect.com/science/article/pii/S2214157X24017106Co-pyrolysisBiomassPolypropyleneKinetic modelSynergistic effectSynergistic mechanism
spellingShingle Zhigang Huang
Tong Zhang
Chen Wang
Wenbo Xiao
Zihan Wang
Obid Tursunov
Jiahui Wu
Yuguang Zhou
Xiaolong Yao
Gang Li
Exploring the factors influencing the co-pyrolysis of walnut shells, pistachio shells, and polypropylene based on thermal behavior, kinetics and reaction mechanism
Case Studies in Thermal Engineering
Co-pyrolysis
Biomass
Polypropylene
Kinetic model
Synergistic effect
Synergistic mechanism
title Exploring the factors influencing the co-pyrolysis of walnut shells, pistachio shells, and polypropylene based on thermal behavior, kinetics and reaction mechanism
title_full Exploring the factors influencing the co-pyrolysis of walnut shells, pistachio shells, and polypropylene based on thermal behavior, kinetics and reaction mechanism
title_fullStr Exploring the factors influencing the co-pyrolysis of walnut shells, pistachio shells, and polypropylene based on thermal behavior, kinetics and reaction mechanism
title_full_unstemmed Exploring the factors influencing the co-pyrolysis of walnut shells, pistachio shells, and polypropylene based on thermal behavior, kinetics and reaction mechanism
title_short Exploring the factors influencing the co-pyrolysis of walnut shells, pistachio shells, and polypropylene based on thermal behavior, kinetics and reaction mechanism
title_sort exploring the factors influencing the co pyrolysis of walnut shells pistachio shells and polypropylene based on thermal behavior kinetics and reaction mechanism
topic Co-pyrolysis
Biomass
Polypropylene
Kinetic model
Synergistic effect
Synergistic mechanism
url http://www.sciencedirect.com/science/article/pii/S2214157X24017106
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