Preparation of nanocellulose from bagasse and its application in chitosan composite films

Cellulose nanocrystals (CNC) are promising for preparing composite materials for food packaging and preservation; however, few studies have utilized nanocellulose from sugarcane bagasse for developing composite membranes. In this study, CNC from bagasse was prepared, CNC/chitosan (CS)/glycerol compo...

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Main Authors: Li Wu, Shengli Gao, Hao Cheng, Chengjie Wu, Shuai Zhang, Ruiping Gao, Xiaohua Zhu
Format: Article
Language:English
Published: The Royal Society 2025-07-01
Series:Royal Society Open Science
Subjects:
Online Access:https://royalsocietypublishing.org/doi/10.1098/rsos.242253
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author Li Wu
Shengli Gao
Hao Cheng
Chengjie Wu
Shuai Zhang
Ruiping Gao
Xiaohua Zhu
author_facet Li Wu
Shengli Gao
Hao Cheng
Chengjie Wu
Shuai Zhang
Ruiping Gao
Xiaohua Zhu
author_sort Li Wu
collection DOAJ
description Cellulose nanocrystals (CNC) are promising for preparing composite materials for food packaging and preservation; however, few studies have utilized nanocellulose from sugarcane bagasse for developing composite membranes. In this study, CNC from bagasse was prepared, CNC/chitosan (CS)/glycerol composite membranes were obtained by the mixing and extensional flow method, and the formulations were optimized using single-factor and orthogonal tests to investigate the effects of CNC, CS and glycerol on the mechanical properties, barrier properties, structure and thermal stability of the composite films. The composite film prepared showed better performance at CNC, CS and glycerol concentrations of 1, 1.5 and 0.75%, respectively. Compared with those of the CS membrane, the barrier performance was improved (p < 0.05). The morphology of CNC and CNC/CS composite films was observed by scanning electron microscopy. The structure was characterized by Fourier transform infrared spectroscopy and X-ray diffraction, and thermal stability was analysed by thermogravimetric analysis. Hydrogen bonding between nanocellulose and CS enhanced the cohesion of the composite film. The newly prepared CNC/CS composite film showed good mechanical properties, barrier properties and stability. It has potential applications in the food packaging industry to extend the shelf life of food and is energy-saving and environmentally friendly.
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publishDate 2025-07-01
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spelling doaj-art-7ffe73e215374ff985600392a0bbc91c2025-08-20T03:15:08ZengThe Royal SocietyRoyal Society Open Science2054-57032025-07-0112710.1098/rsos.242253Preparation of nanocellulose from bagasse and its application in chitosan composite filmsLi Wu0Shengli Gao1Hao Cheng2Chengjie Wu3Shuai Zhang4Ruiping Gao5Xiaohua Zhu6Chongqing Technology and Business University, Chongqing, People’s Republic of ChinaChongqing Technology and Business University, Chongqing, People’s Republic of ChinaGuangxi University of Science and Technology, Liuzhou, Guangxi, People’s Republic of ChinaChongqing Technology and Business University, Chongqing, People’s Republic of ChinaGuangxi University of Science and Technology, Liuzhou, Guangxi, People’s Republic of ChinaChongqing Technology and Business University, Chongqing, People’s Republic of ChinaGuangxi University of Science and Technology, Liuzhou, Guangxi, People’s Republic of ChinaCellulose nanocrystals (CNC) are promising for preparing composite materials for food packaging and preservation; however, few studies have utilized nanocellulose from sugarcane bagasse for developing composite membranes. In this study, CNC from bagasse was prepared, CNC/chitosan (CS)/glycerol composite membranes were obtained by the mixing and extensional flow method, and the formulations were optimized using single-factor and orthogonal tests to investigate the effects of CNC, CS and glycerol on the mechanical properties, barrier properties, structure and thermal stability of the composite films. The composite film prepared showed better performance at CNC, CS and glycerol concentrations of 1, 1.5 and 0.75%, respectively. Compared with those of the CS membrane, the barrier performance was improved (p < 0.05). The morphology of CNC and CNC/CS composite films was observed by scanning electron microscopy. The structure was characterized by Fourier transform infrared spectroscopy and X-ray diffraction, and thermal stability was analysed by thermogravimetric analysis. Hydrogen bonding between nanocellulose and CS enhanced the cohesion of the composite film. The newly prepared CNC/CS composite film showed good mechanical properties, barrier properties and stability. It has potential applications in the food packaging industry to extend the shelf life of food and is energy-saving and environmentally friendly.https://royalsocietypublishing.org/doi/10.1098/rsos.242253nanocellulosechitosancomposite membranebarrier properties
spellingShingle Li Wu
Shengli Gao
Hao Cheng
Chengjie Wu
Shuai Zhang
Ruiping Gao
Xiaohua Zhu
Preparation of nanocellulose from bagasse and its application in chitosan composite films
Royal Society Open Science
nanocellulose
chitosan
composite membrane
barrier properties
title Preparation of nanocellulose from bagasse and its application in chitosan composite films
title_full Preparation of nanocellulose from bagasse and its application in chitosan composite films
title_fullStr Preparation of nanocellulose from bagasse and its application in chitosan composite films
title_full_unstemmed Preparation of nanocellulose from bagasse and its application in chitosan composite films
title_short Preparation of nanocellulose from bagasse and its application in chitosan composite films
title_sort preparation of nanocellulose from bagasse and its application in chitosan composite films
topic nanocellulose
chitosan
composite membrane
barrier properties
url https://royalsocietypublishing.org/doi/10.1098/rsos.242253
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