Adsorption behavior and structural transformation mechanism of ZIF-8 material on iodine vapor with varying particle sizes

Abstract Developing effective iodine capture technologies is critical for both nuclear safety and environmental protection. This study investigates the iodine adsorption properties of ZIF-8, a metal–organic framework (MOF). ZIF-8 samples with varying particle sizes (∼50 nm, 90 nm, 150 nm, and 8 μm)...

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Main Authors: Tian Lan, Xiaofan Ding, Songtao Xiao, Zhongwei Yuan, Taihong Yan, Qi Chen, Tianchi Li, Weifang Zheng
Format: Article
Language:English
Published: Springer 2025-07-01
Series:Discover Applied Sciences
Subjects:
Online Access:https://doi.org/10.1007/s42452-025-07300-x
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author Tian Lan
Xiaofan Ding
Songtao Xiao
Zhongwei Yuan
Taihong Yan
Qi Chen
Tianchi Li
Weifang Zheng
author_facet Tian Lan
Xiaofan Ding
Songtao Xiao
Zhongwei Yuan
Taihong Yan
Qi Chen
Tianchi Li
Weifang Zheng
author_sort Tian Lan
collection DOAJ
description Abstract Developing effective iodine capture technologies is critical for both nuclear safety and environmental protection. This study investigates the iodine adsorption properties of ZIF-8, a metal–organic framework (MOF). ZIF-8 samples with varying particle sizes (∼50 nm, 90 nm, 150 nm, and 8 μm) were synthesized and tested for iodine vapor adsorption at 80 °C. Iodine uptake continuously increased with time, reaching ~ 3500 mg/g after 24 h without reaching equilibrium, with no significant dependence on particle size. Structural changes in ZIF-8 were observed, as iodine accumulation led to the breakdown of the framework into an amorphous gel-like substance, representing a previously unreported phase transformation. SEM and XRD characterization confirmed the collapse of the crystalline structure after iodine loading. These results indicate that iodine adsorption in ZIF-8 involves strong chemisorption in addition to physical uptake, causing irreversible framework transformations. This work highlights the influence of particle size and provides important insights for using ZIF-8 in effective radioactive iodine capture.
format Article
id doaj-art-7f490a4d887f4a2fa9d6cc2acdedc28e
institution Kabale University
issn 3004-9261
language English
publishDate 2025-07-01
publisher Springer
record_format Article
series Discover Applied Sciences
spelling doaj-art-7f490a4d887f4a2fa9d6cc2acdedc28e2025-08-20T03:45:31ZengSpringerDiscover Applied Sciences3004-92612025-07-017711310.1007/s42452-025-07300-xAdsorption behavior and structural transformation mechanism of ZIF-8 material on iodine vapor with varying particle sizesTian Lan0Xiaofan Ding1Songtao Xiao2Zhongwei Yuan3Taihong Yan4Qi Chen5Tianchi Li6Weifang Zheng7China Institute of Atomic EnergyChina Institute of Atomic EnergyChina Institute of Atomic EnergyChina Institute of Atomic EnergyChina Institute of Atomic EnergyChina Institute of Atomic EnergyChina Institute of Atomic EnergyChina Institute of Atomic EnergyAbstract Developing effective iodine capture technologies is critical for both nuclear safety and environmental protection. This study investigates the iodine adsorption properties of ZIF-8, a metal–organic framework (MOF). ZIF-8 samples with varying particle sizes (∼50 nm, 90 nm, 150 nm, and 8 μm) were synthesized and tested for iodine vapor adsorption at 80 °C. Iodine uptake continuously increased with time, reaching ~ 3500 mg/g after 24 h without reaching equilibrium, with no significant dependence on particle size. Structural changes in ZIF-8 were observed, as iodine accumulation led to the breakdown of the framework into an amorphous gel-like substance, representing a previously unreported phase transformation. SEM and XRD characterization confirmed the collapse of the crystalline structure after iodine loading. These results indicate that iodine adsorption in ZIF-8 involves strong chemisorption in addition to physical uptake, causing irreversible framework transformations. This work highlights the influence of particle size and provides important insights for using ZIF-8 in effective radioactive iodine capture.https://doi.org/10.1007/s42452-025-07300-xNuclear fuel reprocessingExhaust gas129IMOFsZIF-8Adsorption
spellingShingle Tian Lan
Xiaofan Ding
Songtao Xiao
Zhongwei Yuan
Taihong Yan
Qi Chen
Tianchi Li
Weifang Zheng
Adsorption behavior and structural transformation mechanism of ZIF-8 material on iodine vapor with varying particle sizes
Discover Applied Sciences
Nuclear fuel reprocessing
Exhaust gas
129I
MOFs
ZIF-8
Adsorption
title Adsorption behavior and structural transformation mechanism of ZIF-8 material on iodine vapor with varying particle sizes
title_full Adsorption behavior and structural transformation mechanism of ZIF-8 material on iodine vapor with varying particle sizes
title_fullStr Adsorption behavior and structural transformation mechanism of ZIF-8 material on iodine vapor with varying particle sizes
title_full_unstemmed Adsorption behavior and structural transformation mechanism of ZIF-8 material on iodine vapor with varying particle sizes
title_short Adsorption behavior and structural transformation mechanism of ZIF-8 material on iodine vapor with varying particle sizes
title_sort adsorption behavior and structural transformation mechanism of zif 8 material on iodine vapor with varying particle sizes
topic Nuclear fuel reprocessing
Exhaust gas
129I
MOFs
ZIF-8
Adsorption
url https://doi.org/10.1007/s42452-025-07300-x
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