Evaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testing

Background: The analytical performance metrics of ethanol testing are critically important due to their legal implications when presenting and interpreting results. Measurement uncertainty (MU) and total analytical error (TAE) are essential approaches for evaluating and improving the quality of meas...

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Main Authors: Bozdayi Mehmet Akif, Bozdayı İsmet Gamze, Çakırca Gökhan
Format: Article
Language:English
Published: Society of Medical Biochemists of Serbia, Belgrade 2025-01-01
Series:Journal of Medical Biochemistry
Subjects:
Online Access:https://scindeks-clanci.ceon.rs/data/pdf/1452-8258/2025/1452-82582504808B.pdf
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author Bozdayi Mehmet Akif
Bozdayı İsmet Gamze
Çakırca Gökhan
author_facet Bozdayi Mehmet Akif
Bozdayı İsmet Gamze
Çakırca Gökhan
author_sort Bozdayi Mehmet Akif
collection DOAJ
description Background: The analytical performance metrics of ethanol testing are critically important due to their legal implications when presenting and interpreting results. Measurement uncertainty (MU) and total analytical error (TAE) are essential approaches for evaluating and improving the quality of measurement procedures. This study aimed to calculate MU and TAE values, which assess the reliability of ethanol test results from different perspectives, and to evaluate the impact of MU values, calculated using two different methods, on the legal threshold. Methods: MU values were calculated following the guidelines of Nordtest and ISO/TS 20914. TAE was determined using the formula TAE%=1.65×CV%+Bias%. External and internal quality data from ethanol testing conducted between July 1, 2022, and June 30, 2024, were used for calculations. Results: The expanded MU values for ethanol testing were 13.95% according to the Nordtest Guide, 10.94% for low level and 9.59% for high level according to the ISO/TS 20914 Guide. The calculated TAE values were 12.59 for low levels, 11.47 for high levels, and 12.57 overall. MU and TAE values for ethanol testing in our laboratory remained within the allowable total error (±20%) according to CLIA 2024. Conclusions: We believe each laboratory should report ethanol test results and their respective MU values, particularly when evaluating results close to legal thresholds. Furthermore, we suggest that scientific committees standardise the method for calculating MU and define a target limit.
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institution Kabale University
issn 1452-8258
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language English
publishDate 2025-01-01
publisher Society of Medical Biochemists of Serbia, Belgrade
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spelling doaj-art-7ecfb2ba9a59436e8ab0ced8d04c6f9b2025-08-20T03:28:51ZengSociety of Medical Biochemists of Serbia, BelgradeJournal of Medical Biochemistry1452-82581452-82662025-01-0144480881310.5937/jomb0-550931452-82582504808BEvaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testingBozdayi Mehmet Akif0Bozdayı İsmet Gamze1Çakırca Gökhan2Mehmet Akif Inan Education and Research Hospital, Department of Medical Biochemistry, Sanliurfa, TürkiyeSanliurfa Education and Research Hospital, Department of Medical Biochemistry, Sanliurfa, TürkiyeMehmet Akif Inan Education and Research Hospital, Department of Medical Biochemistry, Sanliurfa, TürkiyeBackground: The analytical performance metrics of ethanol testing are critically important due to their legal implications when presenting and interpreting results. Measurement uncertainty (MU) and total analytical error (TAE) are essential approaches for evaluating and improving the quality of measurement procedures. This study aimed to calculate MU and TAE values, which assess the reliability of ethanol test results from different perspectives, and to evaluate the impact of MU values, calculated using two different methods, on the legal threshold. Methods: MU values were calculated following the guidelines of Nordtest and ISO/TS 20914. TAE was determined using the formula TAE%=1.65×CV%+Bias%. External and internal quality data from ethanol testing conducted between July 1, 2022, and June 30, 2024, were used for calculations. Results: The expanded MU values for ethanol testing were 13.95% according to the Nordtest Guide, 10.94% for low level and 9.59% for high level according to the ISO/TS 20914 Guide. The calculated TAE values were 12.59 for low levels, 11.47 for high levels, and 12.57 overall. MU and TAE values for ethanol testing in our laboratory remained within the allowable total error (±20%) according to CLIA 2024. Conclusions: We believe each laboratory should report ethanol test results and their respective MU values, particularly when evaluating results close to legal thresholds. Furthermore, we suggest that scientific committees standardise the method for calculating MU and define a target limit.https://scindeks-clanci.ceon.rs/data/pdf/1452-8258/2025/1452-82582504808B.pdfethanoltotal allowable errormeasurement uncertainty
spellingShingle Bozdayi Mehmet Akif
Bozdayı İsmet Gamze
Çakırca Gökhan
Evaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testing
Journal of Medical Biochemistry
ethanol
total allowable error
measurement uncertainty
title Evaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testing
title_full Evaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testing
title_fullStr Evaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testing
title_full_unstemmed Evaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testing
title_short Evaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testing
title_sort evaluation of measurement uncertainty results calculated by two different methods and total analytical error for ethanol testing
topic ethanol
total allowable error
measurement uncertainty
url https://scindeks-clanci.ceon.rs/data/pdf/1452-8258/2025/1452-82582504808B.pdf
work_keys_str_mv AT bozdayimehmetakif evaluationofmeasurementuncertaintyresultscalculatedbytwodifferentmethodsandtotalanalyticalerrorforethanoltesting
AT bozdayıismetgamze evaluationofmeasurementuncertaintyresultscalculatedbytwodifferentmethodsandtotalanalyticalerrorforethanoltesting
AT cakırcagokhan evaluationofmeasurementuncertaintyresultscalculatedbytwodifferentmethodsandtotalanalyticalerrorforethanoltesting