Effect of Silica Addition on Mechanical Properties of Eggshell-Derived Hydroxyapatite

Eggshell is a solid waste that is available in abundance but is being left unused. Eggshell containing calcium in a high amount. Calcium can be used as a precursor for hydroxyapatite (HAp). Modification of HAp with SiO2 is expected to improve its low mechanical properties for biomedical applications...

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Main Authors: Fatma Fatma, Desnelli Desnelli, Fahma Riyanti, Mustafa Kamal, Muhammad Ramdan Abdul Mannan, Poedji Loekitowati Hariani*
Format: Article
Language:English
Published: Syiah Kuala University 2021-09-01
Series:Aceh International Journal of Science and Technology
Subjects:
Online Access:https://jurnal.usk.ac.id/AIJST/article/view/21982
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author Fatma Fatma
Desnelli Desnelli
Fahma Riyanti
Mustafa Kamal
Muhammad Ramdan Abdul Mannan
Poedji Loekitowati Hariani*
author_facet Fatma Fatma
Desnelli Desnelli
Fahma Riyanti
Mustafa Kamal
Muhammad Ramdan Abdul Mannan
Poedji Loekitowati Hariani*
author_sort Fatma Fatma
collection DOAJ
description Eggshell is a solid waste that is available in abundance but is being left unused. Eggshell containing calcium in a high amount. Calcium can be used as a precursor for hydroxyapatite (HAp). Modification of HAp with SiO2 is expected to improve its low mechanical properties for biomedical applications. In this study, HAp is synthesized from the eggshell. Then, it was modified by adding SiO2 utilizing the coprecipitation method with concentrations of 10%, 20%, 30%, and 40%, respectively. The HAp and HAp/SiO2 were characterized using; X-ray diffraction and Fourier transform infrared spectroscopy. The analysis HAp and HAp/SiO2 were density, compressive strength, and hardness. The best mechanical properties of HAp/SiO2 were characterized using SEM-EDS. The HAp were prepared successfully with a ratio of Ca/P was 1.673, close to the theoretical 1.67. The addition of SiO2 caused a decrease in crystallite size and density but increased compressive strength and hardness. The best mechanical properties of HAp/SiO2 were obtained with SiO2 of 30% and 40% with similar values.
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institution Kabale University
issn 2088-9860
language English
publishDate 2021-09-01
publisher Syiah Kuala University
record_format Article
series Aceh International Journal of Science and Technology
spelling doaj-art-7ea7cc6c9fe54b488fe4218be3d4b9a62025-08-20T03:59:39ZengSyiah Kuala UniversityAceh International Journal of Science and Technology2088-98602021-09-0110212913810.13170/aijst.10.2.2198213241Effect of Silica Addition on Mechanical Properties of Eggshell-Derived HydroxyapatiteFatma Fatma0Desnelli Desnelli1Fahma Riyanti2Mustafa Kamal3Muhammad Ramdan Abdul Mannan4Poedji Loekitowati Hariani*5Universitas SriwijayaUniversitas SriwijayaUniversitas SrwijayaUniversitas SriwijayaUniversitas SriwijayaSriwijaya UniversityEggshell is a solid waste that is available in abundance but is being left unused. Eggshell containing calcium in a high amount. Calcium can be used as a precursor for hydroxyapatite (HAp). Modification of HAp with SiO2 is expected to improve its low mechanical properties for biomedical applications. In this study, HAp is synthesized from the eggshell. Then, it was modified by adding SiO2 utilizing the coprecipitation method with concentrations of 10%, 20%, 30%, and 40%, respectively. The HAp and HAp/SiO2 were characterized using; X-ray diffraction and Fourier transform infrared spectroscopy. The analysis HAp and HAp/SiO2 were density, compressive strength, and hardness. The best mechanical properties of HAp/SiO2 were characterized using SEM-EDS. The HAp were prepared successfully with a ratio of Ca/P was 1.673, close to the theoretical 1.67. The addition of SiO2 caused a decrease in crystallite size and density but increased compressive strength and hardness. The best mechanical properties of HAp/SiO2 were obtained with SiO2 of 30% and 40% with similar values.https://jurnal.usk.ac.id/AIJST/article/view/21982eggshell, hydroxyapatite, sio2, mechanical properties
spellingShingle Fatma Fatma
Desnelli Desnelli
Fahma Riyanti
Mustafa Kamal
Muhammad Ramdan Abdul Mannan
Poedji Loekitowati Hariani*
Effect of Silica Addition on Mechanical Properties of Eggshell-Derived Hydroxyapatite
Aceh International Journal of Science and Technology
eggshell, hydroxyapatite, sio2, mechanical properties
title Effect of Silica Addition on Mechanical Properties of Eggshell-Derived Hydroxyapatite
title_full Effect of Silica Addition on Mechanical Properties of Eggshell-Derived Hydroxyapatite
title_fullStr Effect of Silica Addition on Mechanical Properties of Eggshell-Derived Hydroxyapatite
title_full_unstemmed Effect of Silica Addition on Mechanical Properties of Eggshell-Derived Hydroxyapatite
title_short Effect of Silica Addition on Mechanical Properties of Eggshell-Derived Hydroxyapatite
title_sort effect of silica addition on mechanical properties of eggshell derived hydroxyapatite
topic eggshell, hydroxyapatite, sio2, mechanical properties
url https://jurnal.usk.ac.id/AIJST/article/view/21982
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AT desnellidesnelli effectofsilicaadditiononmechanicalpropertiesofeggshellderivedhydroxyapatite
AT fahmariyanti effectofsilicaadditiononmechanicalpropertiesofeggshellderivedhydroxyapatite
AT mustafakamal effectofsilicaadditiononmechanicalpropertiesofeggshellderivedhydroxyapatite
AT muhammadramdanabdulmannan effectofsilicaadditiononmechanicalpropertiesofeggshellderivedhydroxyapatite
AT poedjiloekitowatihariani effectofsilicaadditiononmechanicalpropertiesofeggshellderivedhydroxyapatite