Additive manufacturing of continuous regenerated cellulose fiber reinforced polylactic acid composites using in-situ impregnation material extrusion technique

This study explores an innovative approach to additively manufacture 100 % bio-derived, biodegradable polylactic acid (PLA) reinforced with continuous regenerated cellulose fibres (RCFs) using an in-situ infiltration material extrusion technique. The impact of fiber crystallinity, surface properties...

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Bibliographic Details
Main Authors: Nishant Jain, Mathias Czasny, Till Butzmann, Delf Kober, David Karl, David Schmiedjell, Sabine Hild, Aleksander Gurlo
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Composites Part C: Open Access
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Online Access:http://www.sciencedirect.com/science/article/pii/S2666682025000386
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Summary:This study explores an innovative approach to additively manufacture 100 % bio-derived, biodegradable polylactic acid (PLA) reinforced with continuous regenerated cellulose fibres (RCFs) using an in-situ infiltration material extrusion technique. The impact of fiber crystallinity, surface properties, cross-sectional geometry and PLA's thermal and rheological behaviour is analysed. Single fiber pull-out test (SFPT) is utilised to evaluate fibre-matrix interactions, while tensile and flexural properties are assessed in conjunction with void analysis via optical and AFM micrographs. The results show that Biomid fibres, which exhibit ∼65 % crystallinity, demonstrate ∼31 % higher apparent interfacial shear strength (IFSS) compared to Cordenka fibres, which exhibit ∼42 % crystallinity. Furthermore, Biomid-PLA composites show a substantial increase in tensile strength, reaching ∼290 % higher and tensile modulus reaching ∼470 % higher than unreinforced PLA. In addition, the flexural strength and modulus of the Biomid-PLA composite increased by ∼71 % and ∼120 %, compared to unreinforced PLA.
ISSN:2666-6820