Supramolecular Aggregates of Amide‐ and Urea‐Functionalized Nanographene

Controlling the morphology of supramolecular nanographene (NG) aggregates is challenging. This study confirms that amide‐ and urea‐functionalized NG undergo self‐assembly to form supramolecular aggregates with a morphology that depends on the incorporated functional group. Amide‐functionalized NG fo...

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Main Authors: Haruka Moriguchi, Ryo Sekiya, Takeharu Haino
Format: Article
Language:English
Published: Wiley-VCH 2025-07-01
Series:ChemistryEurope
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Online Access:https://doi.org/10.1002/ceur.202500015
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author Haruka Moriguchi
Ryo Sekiya
Takeharu Haino
author_facet Haruka Moriguchi
Ryo Sekiya
Takeharu Haino
author_sort Haruka Moriguchi
collection DOAJ
description Controlling the morphology of supramolecular nanographene (NG) aggregates is challenging. This study confirms that amide‐ and urea‐functionalized NG undergo self‐assembly to form supramolecular aggregates with a morphology that depends on the incorporated functional group. Amide‐functionalized NG forms stacked aggregates, whereas urea‐functionalized NG organizes into network polymers. These distinct morphologies suggest that amide groups drive NG stacking, whereas urea groups support NG vertically and horizontally, likely owing to differences in the strengths of single and bifurcated NH/O hydrogen bonds. Moreover, the functional group incorporated into NG influences the gelation properties of the system. Among the two tested systems, only urea‐functionalized NG formed organogels, possibly because urea–urea hydrogen bonds, enable solvent‐molecule trapping inside the network polymers formed in these NG systems. Thus, hydrogen bonds can regulate the morphology and function of supramolecular NG aggregates.
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spelling doaj-art-7dab64f861ec4a2b96dd9a38c7c1bcbf2025-08-20T03:11:57ZengWiley-VCHChemistryEurope2751-47652025-07-0134n/an/a10.1002/ceur.202500015Supramolecular Aggregates of Amide‐ and Urea‐Functionalized NanographeneHaruka Moriguchi0Ryo Sekiya1Takeharu Haino2Department of Chemistry, Graduate School of Advanced Science and Engineering Hiroshima University 1-3-1 Kagamiyama Higashi-Hiroshima Hiroshima 739-8526 JapanDepartment of Frontier Materials Chemistry Graduate School of Science and Technology Hirosaki University 3 Bunkyo-cho Hirosaki Aomori 036-8561 JapanDepartment of Chemistry, Graduate School of Advanced Science and Engineering Hiroshima University 1-3-1 Kagamiyama Higashi-Hiroshima Hiroshima 739-8526 JapanControlling the morphology of supramolecular nanographene (NG) aggregates is challenging. This study confirms that amide‐ and urea‐functionalized NG undergo self‐assembly to form supramolecular aggregates with a morphology that depends on the incorporated functional group. Amide‐functionalized NG forms stacked aggregates, whereas urea‐functionalized NG organizes into network polymers. These distinct morphologies suggest that amide groups drive NG stacking, whereas urea groups support NG vertically and horizontally, likely owing to differences in the strengths of single and bifurcated NH/O hydrogen bonds. Moreover, the functional group incorporated into NG influences the gelation properties of the system. Among the two tested systems, only urea‐functionalized NG formed organogels, possibly because urea–urea hydrogen bonds, enable solvent‐molecule trapping inside the network polymers formed in these NG systems. Thus, hydrogen bonds can regulate the morphology and function of supramolecular NG aggregates.https://doi.org/10.1002/ceur.2025000152D materialsgraphene quantum dotsnanographeneself-assemblysupramolecular chemistry
spellingShingle Haruka Moriguchi
Ryo Sekiya
Takeharu Haino
Supramolecular Aggregates of Amide‐ and Urea‐Functionalized Nanographene
ChemistryEurope
2D materials
graphene quantum dots
nanographene
self-assembly
supramolecular chemistry
title Supramolecular Aggregates of Amide‐ and Urea‐Functionalized Nanographene
title_full Supramolecular Aggregates of Amide‐ and Urea‐Functionalized Nanographene
title_fullStr Supramolecular Aggregates of Amide‐ and Urea‐Functionalized Nanographene
title_full_unstemmed Supramolecular Aggregates of Amide‐ and Urea‐Functionalized Nanographene
title_short Supramolecular Aggregates of Amide‐ and Urea‐Functionalized Nanographene
title_sort supramolecular aggregates of amide and urea functionalized nanographene
topic 2D materials
graphene quantum dots
nanographene
self-assembly
supramolecular chemistry
url https://doi.org/10.1002/ceur.202500015
work_keys_str_mv AT harukamoriguchi supramolecularaggregatesofamideandureafunctionalizednanographene
AT ryosekiya supramolecularaggregatesofamideandureafunctionalizednanographene
AT takeharuhaino supramolecularaggregatesofamideandureafunctionalizednanographene