Synthesis of Nanocrystalline Yttria Stabilized Zirconia for SOFC
Nanocrystalline zirconia powders stabilized with varying concentration of yttria (YSZ) were synthesized following urea solution combustion route. Thermogravimetric analysis combined with differential scanning calorimetry was carried out for the intermediate gel for analyzing reaction kinetics. The f...
Saved in:
| Main Authors: | , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Wiley
2011-12-01
|
| Series: | Nanomaterials and Nanotechnology |
| Subjects: | |
| Online Access: | http://www.intechopen.com/journals/nanomaterials_and_nanotechnology/synthesis_of_nanocrystalline_yttria_stabilized_zirconia_for_sofc |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| _version_ | 1850219303603798016 |
|---|---|
| author | Mridula Biswas Prasant Kumar Ojha E. Moses Jayasingh C. Durga Prasad |
| author_facet | Mridula Biswas Prasant Kumar Ojha E. Moses Jayasingh C. Durga Prasad |
| author_sort | Mridula Biswas |
| collection | DOAJ |
| description | Nanocrystalline zirconia powders stabilized with varying concentration of yttria (YSZ) were synthesized following urea solution combustion route. Thermogravimetric analysis combined with differential scanning calorimetry was carried out for the intermediate gel for analyzing reaction kinetics. The final products were characterized by X‐ray diffractometry, transmission electron microscopy and specific surface area measurements. Sintering behavior of theses powders were studied. The powder quality is poor in respect of surface area and sintered density. |
| format | Article |
| id | doaj-art-7cc840aaf67d4d869236007e099017ec |
| institution | OA Journals |
| issn | 1847-9804 |
| language | English |
| publishDate | 2011-12-01 |
| publisher | Wiley |
| record_format | Article |
| series | Nanomaterials and Nanotechnology |
| spelling | doaj-art-7cc840aaf67d4d869236007e099017ec2025-08-20T02:07:25ZengWileyNanomaterials and Nanotechnology1847-98042011-12-0112http://dx.doi.org/10.5772/50961Synthesis of Nanocrystalline Yttria Stabilized Zirconia for SOFCMridula BiswasPrasant Kumar OjhaE. Moses JayasinghC. Durga PrasadNanocrystalline zirconia powders stabilized with varying concentration of yttria (YSZ) were synthesized following urea solution combustion route. Thermogravimetric analysis combined with differential scanning calorimetry was carried out for the intermediate gel for analyzing reaction kinetics. The final products were characterized by X‐ray diffractometry, transmission electron microscopy and specific surface area measurements. Sintering behavior of theses powders were studied. The powder quality is poor in respect of surface area and sintered density.http://www.intechopen.com/journals/nanomaterials_and_nanotechnology/synthesis_of_nanocrystalline_yttria_stabilized_zirconia_for_sofc Combustion synthesisDSC‐TGAXRDTEMsintered density |
| spellingShingle | Mridula Biswas Prasant Kumar Ojha E. Moses Jayasingh C. Durga Prasad Synthesis of Nanocrystalline Yttria Stabilized Zirconia for SOFC Nanomaterials and Nanotechnology Combustion synthesis DSC‐TGA XRD TEM sintered density |
| title | Synthesis of Nanocrystalline Yttria Stabilized Zirconia for SOFC |
| title_full | Synthesis of Nanocrystalline Yttria Stabilized Zirconia for SOFC |
| title_fullStr | Synthesis of Nanocrystalline Yttria Stabilized Zirconia for SOFC |
| title_full_unstemmed | Synthesis of Nanocrystalline Yttria Stabilized Zirconia for SOFC |
| title_short | Synthesis of Nanocrystalline Yttria Stabilized Zirconia for SOFC |
| title_sort | synthesis of nanocrystalline yttria stabilized zirconia for sofc |
| topic | Combustion synthesis DSC‐TGA XRD TEM sintered density |
| url | http://www.intechopen.com/journals/nanomaterials_and_nanotechnology/synthesis_of_nanocrystalline_yttria_stabilized_zirconia_for_sofc |
| work_keys_str_mv | AT mridulabiswas synthesisofnanocrystallineyttriastabilizedzirconiaforsofc AT prasantkumarojha synthesisofnanocrystallineyttriastabilizedzirconiaforsofc AT emosesjayasingh synthesisofnanocrystallineyttriastabilizedzirconiaforsofc AT cdurgaprasad synthesisofnanocrystallineyttriastabilizedzirconiaforsofc |