Separation and Identification of Terpenoids in Three Pineapple Fibers Using Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry

In this study, ultra-high performance liquid chromatography-tandem mass spectrometry was used to isolate and identify terpenoids in three types of pineapple fibers (pineapple leaf fiber, pineapple stem fiber, and pineapple root fiber). The research results showed that in the positive and negative io...

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Main Authors: Yijun Liu, Yuliang Chen, Jiameng Liu, Lin Zhu, Lijing Lin, Zhikai Zhuang, Jiangxiu He, Tao Li, Gang Chen, Siru Yao
Format: Article
Language:English
Published: Taylor & Francis Group 2024-12-01
Series:Journal of Natural Fibers
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Online Access:https://www.tandfonline.com/doi/10.1080/15440478.2024.2315596
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author Yijun Liu
Yuliang Chen
Jiameng Liu
Lin Zhu
Lijing Lin
Zhikai Zhuang
Jiangxiu He
Tao Li
Gang Chen
Siru Yao
author_facet Yijun Liu
Yuliang Chen
Jiameng Liu
Lin Zhu
Lijing Lin
Zhikai Zhuang
Jiangxiu He
Tao Li
Gang Chen
Siru Yao
author_sort Yijun Liu
collection DOAJ
description In this study, ultra-high performance liquid chromatography-tandem mass spectrometry was used to isolate and identify terpenoids in three types of pineapple fibers (pineapple leaf fiber, pineapple stem fiber, and pineapple root fiber). The research results showed that in the positive and negative ion modes, 9 and 26 terpenoid compounds were identified from the three types of pineapple fibers, totaling 35 species in 12 categories, among which triterpene saponins had the largest number of species. Pineapple root fiber contains the highest total terpenoid content, followed by pineapple stem fiber and leaf fiber. In the OPLS-DA model, the VIP and S-plot methods revealed the differences in terpenoid compounds in three pineapple fibers. The research results showed that there were 9, 8 and 7 significantly different terpenoid compounds in pineapple leaf fiber and pineapple stem fiber, pineapple leaf fiber and pineapple root fiber, and pineapple stem fiber and pineapple root fiber respectively. Functional terpenoids such as ivy saponin, dehydroabietic acid, myrcene and ginsenoside are distributed in different parts of pineapple with varying degrees of enrichment. This study provides a basis for differentiated utilization and value-added use of pineapple leaves, stems and roots. Utilization provides scientific basis.
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institution OA Journals
issn 1544-0478
1544-046X
language English
publishDate 2024-12-01
publisher Taylor & Francis Group
record_format Article
series Journal of Natural Fibers
spelling doaj-art-7c8b4f69469d4c669de3e3e8eca590192025-08-20T01:56:16ZengTaylor & Francis GroupJournal of Natural Fibers1544-04781544-046X2024-12-0121110.1080/15440478.2024.2315596Separation and Identification of Terpenoids in Three Pineapple Fibers Using Ultra-High Performance Liquid Chromatography-Tandem Mass SpectrometryYijun Liu0Yuliang Chen1Jiameng Liu2Lin Zhu3Lijing Lin4Zhikai Zhuang5Jiangxiu He6Tao Li7Gang Chen8Siru Yao9State Key Laboratory of Pulp and Paper Engineering, College of Light Industry and Engineering, South China University of Technology, Guangzhou, ChinaHainan Key Laboratory of Storage & Processing of Fruits and Vegetables, Agricultural Products Processing Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang, ChinaHainan Key Laboratory of Storage & Processing of Fruits and Vegetables, Agricultural Products Processing Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang, ChinaHainan Key Laboratory of Storage & Processing of Fruits and Vegetables, Agricultural Products Processing Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang, ChinaHainan Key Laboratory of Storage & Processing of Fruits and Vegetables, Agricultural Products Processing Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang, ChinaHainan Key Laboratory of Storage & Processing of Fruits and Vegetables, Agricultural Products Processing Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang, ChinaHainan Key Laboratory of Storage & Processing of Fruits and Vegetables, Agricultural Products Processing Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang, ChinaHainan Key Laboratory of Storage & Processing of Fruits and Vegetables, Agricultural Products Processing Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang, ChinaState Key Laboratory of Pulp and Paper Engineering, College of Light Industry and Engineering, South China University of Technology, Guangzhou, ChinaHainan Key Laboratory of Storage & Processing of Fruits and Vegetables, Agricultural Products Processing Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang, ChinaIn this study, ultra-high performance liquid chromatography-tandem mass spectrometry was used to isolate and identify terpenoids in three types of pineapple fibers (pineapple leaf fiber, pineapple stem fiber, and pineapple root fiber). The research results showed that in the positive and negative ion modes, 9 and 26 terpenoid compounds were identified from the three types of pineapple fibers, totaling 35 species in 12 categories, among which triterpene saponins had the largest number of species. Pineapple root fiber contains the highest total terpenoid content, followed by pineapple stem fiber and leaf fiber. In the OPLS-DA model, the VIP and S-plot methods revealed the differences in terpenoid compounds in three pineapple fibers. The research results showed that there were 9, 8 and 7 significantly different terpenoid compounds in pineapple leaf fiber and pineapple stem fiber, pineapple leaf fiber and pineapple root fiber, and pineapple stem fiber and pineapple root fiber respectively. Functional terpenoids such as ivy saponin, dehydroabietic acid, myrcene and ginsenoside are distributed in different parts of pineapple with varying degrees of enrichment. This study provides a basis for differentiated utilization and value-added use of pineapple leaves, stems and roots. Utilization provides scientific basis.https://www.tandfonline.com/doi/10.1080/15440478.2024.2315596Terpenoidspineapple fiberseparationidentificationultra-performance liquid chromatography-tandem mass spectrometry萜类化合物
spellingShingle Yijun Liu
Yuliang Chen
Jiameng Liu
Lin Zhu
Lijing Lin
Zhikai Zhuang
Jiangxiu He
Tao Li
Gang Chen
Siru Yao
Separation and Identification of Terpenoids in Three Pineapple Fibers Using Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry
Journal of Natural Fibers
Terpenoids
pineapple fiber
separation
identification
ultra-performance liquid chromatography-tandem mass spectrometry
萜类化合物
title Separation and Identification of Terpenoids in Three Pineapple Fibers Using Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry
title_full Separation and Identification of Terpenoids in Three Pineapple Fibers Using Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry
title_fullStr Separation and Identification of Terpenoids in Three Pineapple Fibers Using Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry
title_full_unstemmed Separation and Identification of Terpenoids in Three Pineapple Fibers Using Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry
title_short Separation and Identification of Terpenoids in Three Pineapple Fibers Using Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry
title_sort separation and identification of terpenoids in three pineapple fibers using ultra high performance liquid chromatography tandem mass spectrometry
topic Terpenoids
pineapple fiber
separation
identification
ultra-performance liquid chromatography-tandem mass spectrometry
萜类化合物
url https://www.tandfonline.com/doi/10.1080/15440478.2024.2315596
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