Facile Solventless Synthesis of a Nylon-6,6/Silver Nanoparticles Composite and Its XPS Study
Silver nanoparticles were synthesized and supported on thin nylon membranes by means of a simple method of impregnation and chemical reduction of Ag ions at ambient conditions. Particles of less than 10 nm were obtained using this methodology, in which the nylon fibers behave as constrained nanoreac...
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| Main Authors: | , , , , , , , |
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| Format: | Article |
| Language: | English |
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Wiley
2013-01-01
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| Series: | International Journal of Polymer Science |
| Online Access: | http://dx.doi.org/10.1155/2013/235850 |
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| author | Raúl A. Morales-Luckie Víctor Sánchez-Mendieta Oscar Olea-Mejia Alfredo R. Vilchis-Nestor Gustavo López-Téllez Víctor Varela-Guerrero L. Huerta Jesús Arenas-Alatorre |
| author_facet | Raúl A. Morales-Luckie Víctor Sánchez-Mendieta Oscar Olea-Mejia Alfredo R. Vilchis-Nestor Gustavo López-Téllez Víctor Varela-Guerrero L. Huerta Jesús Arenas-Alatorre |
| author_sort | Raúl A. Morales-Luckie |
| collection | DOAJ |
| description | Silver nanoparticles were synthesized and supported on thin nylon membranes by means of a simple method of impregnation and chemical reduction of Ag ions at ambient conditions. Particles of less than 10 nm were obtained using this methodology, in which the nylon fibers behave as constrained nanoreactors. Pores on nylon fibres along with oxygen and nitrogen from amide moieties in nylon provide effective sites for in situ reduction of silver ions and for the formation and stabilization of Ag nanoparticles. Transmission electron microscopy (TEM) analysis showed that silver nanoparticles are well dispersed throughout the nylon fibers. Furthermore, an interaction between nitrogen of amides moieties of nylon-6,6 and silver nanoparticles has been found by X-ray photoelectron spectroscopy (XPS). |
| format | Article |
| id | doaj-art-7c52e4e63f2341c8b3a2a3b5927be230 |
| institution | Kabale University |
| issn | 1687-9422 1687-9430 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | International Journal of Polymer Science |
| spelling | doaj-art-7c52e4e63f2341c8b3a2a3b5927be2302025-08-20T03:35:45ZengWileyInternational Journal of Polymer Science1687-94221687-94302013-01-01201310.1155/2013/235850235850Facile Solventless Synthesis of a Nylon-6,6/Silver Nanoparticles Composite and Its XPS StudyRaúl A. Morales-Luckie0Víctor Sánchez-Mendieta1Oscar Olea-Mejia2Alfredo R. Vilchis-Nestor3Gustavo López-Téllez4Víctor Varela-Guerrero5L. Huerta6Jesús Arenas-Alatorre7Centro Conjunto de Investigación en Química Sustentable UAEM-UNAM (CCIQS), Facultad de Química, Universidad Autónoma del Estado de México, Km. 14.5 de la carretera Toluca-Atlacomulco, 50200 San Cayetano, MEX, MexicoFacultad de Química, Universidad Autónoma del Estado de México, Paseo Colón y Paseo Tollocan, 50120 Toluca, MEX, MexicoCentro Conjunto de Investigación en Química Sustentable UAEM-UNAM (CCIQS), Facultad de Química, Universidad Autónoma del Estado de México, Km. 14.5 de la carretera Toluca-Atlacomulco, 50200 San Cayetano, MEX, MexicoCentro Conjunto de Investigación en Química Sustentable UAEM-UNAM (CCIQS), Facultad de Química, Universidad Autónoma del Estado de México, Km. 14.5 de la carretera Toluca-Atlacomulco, 50200 San Cayetano, MEX, MexicoCentro Conjunto de Investigación en Química Sustentable UAEM-UNAM (CCIQS), Facultad de Química, Universidad Autónoma del Estado de México, Km. 14.5 de la carretera Toluca-Atlacomulco, 50200 San Cayetano, MEX, MexicoCentro Conjunto de Investigación en Química Sustentable UAEM-UNAM (CCIQS), Facultad de Química, Universidad Autónoma del Estado de México, Km. 14.5 de la carretera Toluca-Atlacomulco, 50200 San Cayetano, MEX, MexicoInstituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, Apartado Postal 70-360, 04510 México, DF, MexicoInstituto de Física, Universidad Nacional Autónoma de México, Apartado Postal 20-364, 01000 México, DF, MexicoSilver nanoparticles were synthesized and supported on thin nylon membranes by means of a simple method of impregnation and chemical reduction of Ag ions at ambient conditions. Particles of less than 10 nm were obtained using this methodology, in which the nylon fibers behave as constrained nanoreactors. Pores on nylon fibres along with oxygen and nitrogen from amide moieties in nylon provide effective sites for in situ reduction of silver ions and for the formation and stabilization of Ag nanoparticles. Transmission electron microscopy (TEM) analysis showed that silver nanoparticles are well dispersed throughout the nylon fibers. Furthermore, an interaction between nitrogen of amides moieties of nylon-6,6 and silver nanoparticles has been found by X-ray photoelectron spectroscopy (XPS).http://dx.doi.org/10.1155/2013/235850 |
| spellingShingle | Raúl A. Morales-Luckie Víctor Sánchez-Mendieta Oscar Olea-Mejia Alfredo R. Vilchis-Nestor Gustavo López-Téllez Víctor Varela-Guerrero L. Huerta Jesús Arenas-Alatorre Facile Solventless Synthesis of a Nylon-6,6/Silver Nanoparticles Composite and Its XPS Study International Journal of Polymer Science |
| title | Facile Solventless Synthesis of a Nylon-6,6/Silver Nanoparticles Composite and Its XPS Study |
| title_full | Facile Solventless Synthesis of a Nylon-6,6/Silver Nanoparticles Composite and Its XPS Study |
| title_fullStr | Facile Solventless Synthesis of a Nylon-6,6/Silver Nanoparticles Composite and Its XPS Study |
| title_full_unstemmed | Facile Solventless Synthesis of a Nylon-6,6/Silver Nanoparticles Composite and Its XPS Study |
| title_short | Facile Solventless Synthesis of a Nylon-6,6/Silver Nanoparticles Composite and Its XPS Study |
| title_sort | facile solventless synthesis of a nylon 6 6 silver nanoparticles composite and its xps study |
| url | http://dx.doi.org/10.1155/2013/235850 |
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