Reprogramming FGF1 from the natural growth factor to the engineered heparan sulphate biosensor

Abstract Heparan sulphate proteoglycans (HSPGs) are cell surface and extracellular matrix proteoglycan family members, playing a key role in diverse biological activities including signal transduction or endocytosis. To date, many HSPG ligands have been identified, including growth factors interacti...

Full description

Saved in:
Bibliographic Details
Main Authors: Krzysztof Ciura, Olimpia Sobota, Aleksandra Chorążewska, Daniel Krowarsch, Natalia Porębska, Łukasz Opaliński
Format: Article
Language:English
Published: BMC 2025-05-01
Series:Cell Communication and Signaling
Subjects:
Online Access:https://doi.org/10.1186/s12964-025-02269-x
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850231205388091392
author Krzysztof Ciura
Olimpia Sobota
Aleksandra Chorążewska
Daniel Krowarsch
Natalia Porębska
Łukasz Opaliński
author_facet Krzysztof Ciura
Olimpia Sobota
Aleksandra Chorążewska
Daniel Krowarsch
Natalia Porębska
Łukasz Opaliński
author_sort Krzysztof Ciura
collection DOAJ
description Abstract Heparan sulphate proteoglycans (HSPGs) are cell surface and extracellular matrix proteoglycan family members, playing a key role in diverse biological activities including signal transduction or endocytosis. To date, many HSPG ligands have been identified, including growth factors interacting via sulfated domains of heparan sulphate (HS) chains. Due to significant overexpression of HSPGs in various cancers, discovering novel biomolecules capable of HSPGs recognition, which may act as HSPGs biosensors or drug carriers targeting HSPGs, is essential. Fibroblast growth factors (FGFs), mainly paracrine FGFs, are natural ligands of membrane-bound HSPGs, forming ternary signaling complex with HSPGs and fibroblast growth factor receptors (FGFRs). Here we employed the natural capability of FGF1 to bind HSPGs to develop HSPGs-specific proteinaceous probe. We identified three point mutations within FGF1 that elevate its affinity for heparin—S116R, S17K and L72R, named B, C and D respectively. Together with substitutions increasing FGF1 stability and abolishing FGF1 binding to FGFRs, we have generated eight HSPGs-specific variants. Among tested mutants, FGF1HSBCD exhibits the highest affinity for heparin and HS/HSPGs, showing over 20-fold increase in affinity for glypican-4 and requiring 0.23 M higher salt concentration for elution from heparin column compared to the initial FGF1HS molecule. Finally, we demonstrated FGF1HSBCD potential to act as a molecular sensor of HSPGs level in cancer cell lines overproducing HSPGs, implicating that FGF1HSBCD can be used as HSPGs biosensor or as a drug delivery carrier in protein-drug conjugates (PDC) targeting HSPGs.
format Article
id doaj-art-7c498fc407854fbaad468f76814202cb
institution OA Journals
issn 1478-811X
language English
publishDate 2025-05-01
publisher BMC
record_format Article
series Cell Communication and Signaling
spelling doaj-art-7c498fc407854fbaad468f76814202cb2025-08-20T02:03:36ZengBMCCell Communication and Signaling1478-811X2025-05-0123111310.1186/s12964-025-02269-xReprogramming FGF1 from the natural growth factor to the engineered heparan sulphate biosensorKrzysztof Ciura0Olimpia Sobota1Aleksandra Chorążewska2Daniel Krowarsch3Natalia Porębska4Łukasz Opaliński5Department of Medical Biotechnology, Faculty of Biotechnology, University of WroclawDepartment of Medical Biotechnology, Faculty of Biotechnology, University of WroclawDepartment of Medical Biotechnology, Faculty of Biotechnology, University of WroclawDepartment of Protein Engineering, Faculty of Biotechnology, University of WroclawDepartment of Medical Biotechnology, Faculty of Biotechnology, University of WroclawDepartment of Medical Biotechnology, Faculty of Biotechnology, University of WroclawAbstract Heparan sulphate proteoglycans (HSPGs) are cell surface and extracellular matrix proteoglycan family members, playing a key role in diverse biological activities including signal transduction or endocytosis. To date, many HSPG ligands have been identified, including growth factors interacting via sulfated domains of heparan sulphate (HS) chains. Due to significant overexpression of HSPGs in various cancers, discovering novel biomolecules capable of HSPGs recognition, which may act as HSPGs biosensors or drug carriers targeting HSPGs, is essential. Fibroblast growth factors (FGFs), mainly paracrine FGFs, are natural ligands of membrane-bound HSPGs, forming ternary signaling complex with HSPGs and fibroblast growth factor receptors (FGFRs). Here we employed the natural capability of FGF1 to bind HSPGs to develop HSPGs-specific proteinaceous probe. We identified three point mutations within FGF1 that elevate its affinity for heparin—S116R, S17K and L72R, named B, C and D respectively. Together with substitutions increasing FGF1 stability and abolishing FGF1 binding to FGFRs, we have generated eight HSPGs-specific variants. Among tested mutants, FGF1HSBCD exhibits the highest affinity for heparin and HS/HSPGs, showing over 20-fold increase in affinity for glypican-4 and requiring 0.23 M higher salt concentration for elution from heparin column compared to the initial FGF1HS molecule. Finally, we demonstrated FGF1HSBCD potential to act as a molecular sensor of HSPGs level in cancer cell lines overproducing HSPGs, implicating that FGF1HSBCD can be used as HSPGs biosensor or as a drug delivery carrier in protein-drug conjugates (PDC) targeting HSPGs.https://doi.org/10.1186/s12964-025-02269-xFGF1FGFRHSPGHeparinHeparan sulfateProtein engineering
spellingShingle Krzysztof Ciura
Olimpia Sobota
Aleksandra Chorążewska
Daniel Krowarsch
Natalia Porębska
Łukasz Opaliński
Reprogramming FGF1 from the natural growth factor to the engineered heparan sulphate biosensor
Cell Communication and Signaling
FGF1
FGFR
HSPG
Heparin
Heparan sulfate
Protein engineering
title Reprogramming FGF1 from the natural growth factor to the engineered heparan sulphate biosensor
title_full Reprogramming FGF1 from the natural growth factor to the engineered heparan sulphate biosensor
title_fullStr Reprogramming FGF1 from the natural growth factor to the engineered heparan sulphate biosensor
title_full_unstemmed Reprogramming FGF1 from the natural growth factor to the engineered heparan sulphate biosensor
title_short Reprogramming FGF1 from the natural growth factor to the engineered heparan sulphate biosensor
title_sort reprogramming fgf1 from the natural growth factor to the engineered heparan sulphate biosensor
topic FGF1
FGFR
HSPG
Heparin
Heparan sulfate
Protein engineering
url https://doi.org/10.1186/s12964-025-02269-x
work_keys_str_mv AT krzysztofciura reprogrammingfgf1fromthenaturalgrowthfactortotheengineeredheparansulphatebiosensor
AT olimpiasobota reprogrammingfgf1fromthenaturalgrowthfactortotheengineeredheparansulphatebiosensor
AT aleksandrachorazewska reprogrammingfgf1fromthenaturalgrowthfactortotheengineeredheparansulphatebiosensor
AT danielkrowarsch reprogrammingfgf1fromthenaturalgrowthfactortotheengineeredheparansulphatebiosensor
AT nataliaporebska reprogrammingfgf1fromthenaturalgrowthfactortotheengineeredheparansulphatebiosensor
AT łukaszopalinski reprogrammingfgf1fromthenaturalgrowthfactortotheengineeredheparansulphatebiosensor