Composite electrochemical coatings of Ni-CrB2 from sulfuric acid and sulfamate electrolytes: formation, structure and properties

Electrodeposited coatings are in demand in many industries: due to the high adhesive strength to the base metal, they can be applied to complex-shaped products, and the thickness of the deposited coating can be controlled. However, standard electrolytic coatings do not always meet the necessary oper...

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Main Authors: Polina Petukhova, Evdokiya Bushueva, Oksana Novgorodtseva
Format: Article
Language:English
Published: Ural Federal University 2024-10-01
Series:Chimica Techno Acta
Subjects:
Online Access:https://chimicatechnoacta.ru/article/view/8019
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author Polina Petukhova
Evdokiya Bushueva
Oksana Novgorodtseva
author_facet Polina Petukhova
Evdokiya Bushueva
Oksana Novgorodtseva
author_sort Polina Petukhova
collection DOAJ
description Electrodeposited coatings are in demand in many industries: due to the high adhesive strength to the base metal, they can be applied to complex-shaped products, and the thickness of the deposited coating can be controlled. However, standard electrolytic coatings do not always meet the necessary operating requirements. In this case, the formation of composite electrolytic coatings, which consist in the modification of electrolytes by various dispersed particles, becomes an urgent task. These particles are introduced into the electrolyte and deposited together with the precipitate metals, which leads to changes in the coating properties. In this article, the structure, adhesive and corrosion properties of nickel-chromium diboride composite coatings obtained in the electrodeposition process are studied. Precipitation was carried out in sulfuric acid and sulfamate electrolytes with a concentration of dispersed chromium diboride particles of 10-40 g/l. The coatings consist of nickel and CrB2 phases. The adhesive strength of the coating with a steel base is satisfactory; chipping and peeling were not observed. The corrosion resistance of sulfamate electrolyte coatings is higher than that of the coatings obtained from sulfuric acid electrolyte due to the compactness of nickel precipitates. Chromium diboride in the coating provides 1.5-2 times greater corrosion resistance.
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issn 2411-1414
language English
publishDate 2024-10-01
publisher Ural Federal University
record_format Article
series Chimica Techno Acta
spelling doaj-art-7bf2c1f681b343e1bc5d904a2344ab7d2025-08-20T03:06:42ZengUral Federal UniversityChimica Techno Acta2411-14142024-10-0111410.15826/chimtech.2024.11.4.065478Composite electrochemical coatings of Ni-CrB2 from sulfuric acid and sulfamate electrolytes: formation, structure and propertiesPolina Petukhova0Evdokiya Bushueva1Oksana Novgorodtseva2Novosibirsk State Technical UniversityNovosibirsk State Technical UniversityNovosibirsk State Technical UniversityElectrodeposited coatings are in demand in many industries: due to the high adhesive strength to the base metal, they can be applied to complex-shaped products, and the thickness of the deposited coating can be controlled. However, standard electrolytic coatings do not always meet the necessary operating requirements. In this case, the formation of composite electrolytic coatings, which consist in the modification of electrolytes by various dispersed particles, becomes an urgent task. These particles are introduced into the electrolyte and deposited together with the precipitate metals, which leads to changes in the coating properties. In this article, the structure, adhesive and corrosion properties of nickel-chromium diboride composite coatings obtained in the electrodeposition process are studied. Precipitation was carried out in sulfuric acid and sulfamate electrolytes with a concentration of dispersed chromium diboride particles of 10-40 g/l. The coatings consist of nickel and CrB2 phases. The adhesive strength of the coating with a steel base is satisfactory; chipping and peeling were not observed. The corrosion resistance of sulfamate electrolyte coatings is higher than that of the coatings obtained from sulfuric acid electrolyte due to the compactness of nickel precipitates. Chromium diboride in the coating provides 1.5-2 times greater corrosion resistance.https://chimicatechnoacta.ru/article/view/8019electrodepositionnickel platingcomposite electrolytic coatingschromium diboridecorrosion resistance
spellingShingle Polina Petukhova
Evdokiya Bushueva
Oksana Novgorodtseva
Composite electrochemical coatings of Ni-CrB2 from sulfuric acid and sulfamate electrolytes: formation, structure and properties
Chimica Techno Acta
electrodeposition
nickel plating
composite electrolytic coatings
chromium diboride
corrosion resistance
title Composite electrochemical coatings of Ni-CrB2 from sulfuric acid and sulfamate electrolytes: formation, structure and properties
title_full Composite electrochemical coatings of Ni-CrB2 from sulfuric acid and sulfamate electrolytes: formation, structure and properties
title_fullStr Composite electrochemical coatings of Ni-CrB2 from sulfuric acid and sulfamate electrolytes: formation, structure and properties
title_full_unstemmed Composite electrochemical coatings of Ni-CrB2 from sulfuric acid and sulfamate electrolytes: formation, structure and properties
title_short Composite electrochemical coatings of Ni-CrB2 from sulfuric acid and sulfamate electrolytes: formation, structure and properties
title_sort composite electrochemical coatings of ni crb2 from sulfuric acid and sulfamate electrolytes formation structure and properties
topic electrodeposition
nickel plating
composite electrolytic coatings
chromium diboride
corrosion resistance
url https://chimicatechnoacta.ru/article/view/8019
work_keys_str_mv AT polinapetukhova compositeelectrochemicalcoatingsofnicrb2fromsulfuricacidandsulfamateelectrolytesformationstructureandproperties
AT evdokiyabushueva compositeelectrochemicalcoatingsofnicrb2fromsulfuricacidandsulfamateelectrolytesformationstructureandproperties
AT oksananovgorodtseva compositeelectrochemicalcoatingsofnicrb2fromsulfuricacidandsulfamateelectrolytesformationstructureandproperties