Synergistic Effects in Copolymerized Carbon Nitride/MoO3 Heterojunction Composites for Efficient Visible‐Light‐Driven Photocatalysis

ABSTRACT The engineering of very effective and sustainable photocatalysts is needed to confront both environmental and energy problems. This work included the synthesis and evaluation of a range of copolymerized graphitic carbon nitride (CN)‐based materials (CN‐PAx) and their heterojunction composit...

Full description

Saved in:
Bibliographic Details
Main Authors: Junsheng Ye, Abeer M. Beagan, Sheng‐Rong Guo, Asif Hayat, Yasin Orooji
Format: Article
Language:English
Published: Wiley 2025-05-01
Series:EcoMat
Subjects:
Online Access:https://doi.org/10.1002/eom2.70015
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849321916022652928
author Junsheng Ye
Abeer M. Beagan
Sheng‐Rong Guo
Asif Hayat
Yasin Orooji
author_facet Junsheng Ye
Abeer M. Beagan
Sheng‐Rong Guo
Asif Hayat
Yasin Orooji
author_sort Junsheng Ye
collection DOAJ
description ABSTRACT The engineering of very effective and sustainable photocatalysts is needed to confront both environmental and energy problems. This work included the synthesis and evaluation of a range of copolymerized graphitic carbon nitride (CN)‐based materials (CN‐PAx) and their heterojunction composite materials with molybdenum trioxide (MoO3) for photocatalytic hydrogen (H2) generation and methylene blue (MB) degradation under visible‐light illumination. Pristine CN and MoO3 had lower photocatalytic performance, but copolymerized CN materials (CN‐PA200, CN‐PA400, CN‐PA600) and their heterojunction composite materials (CN/MoO3, CN‐PA400/MoO3(3%), CN‐PA400/MoO3(6%), and CN‐PA400/MoO3(9%)) demonstrated substantial enhancements. Of them, CN‐PA400/MoO3(6%) had the greatest H2 production rate of 127.22 μmol/h, almost 6.8 times higher than pure CN. It attained an outstanding MB photodegradation performance of 99.3% in 1 h, demonstrating exceptional stability by maintaining over 95% effectiveness throughout four successive cycles. The exceptional efficiency of CN‐PA400/MoO3(6%) is ascribed to its improved heterojunction design, which improves the separation of charge particles, minimizes recombination, and promotes visible‐light absorption. The band alignment among CN‐PA400 and MoO3 facilitates effective electron transport, whereas the presence of many active sites enhances the photocatalytic processes. These results present significant insights into the development of effective heterojunction photocatalysts and highlight the promise of CN‐PA400/MoO3(6%) for renewable energy generation and environmental cleanup purposes.
format Article
id doaj-art-7b4e4d668f40445dbd356232eff1d0c3
institution Kabale University
issn 2567-3173
language English
publishDate 2025-05-01
publisher Wiley
record_format Article
series EcoMat
spelling doaj-art-7b4e4d668f40445dbd356232eff1d0c32025-08-20T03:49:36ZengWileyEcoMat2567-31732025-05-0175n/an/a10.1002/eom2.70015Synergistic Effects in Copolymerized Carbon Nitride/MoO3 Heterojunction Composites for Efficient Visible‐Light‐Driven PhotocatalysisJunsheng Ye0Abeer M. Beagan1Sheng‐Rong Guo2Asif Hayat3Yasin Orooji4College of Geography and Environmental Sciences Zhejiang Normal University Jinhua ChinaDepartment of Chemistry, College of Science King Saud University Riyadh Saudi ArabiaDepartment of Chemistry Lishui University Lishui ChinaDepartment of Chemistry Lishui University Lishui ChinaCollege of Geography and Environmental Sciences Zhejiang Normal University Jinhua ChinaABSTRACT The engineering of very effective and sustainable photocatalysts is needed to confront both environmental and energy problems. This work included the synthesis and evaluation of a range of copolymerized graphitic carbon nitride (CN)‐based materials (CN‐PAx) and their heterojunction composite materials with molybdenum trioxide (MoO3) for photocatalytic hydrogen (H2) generation and methylene blue (MB) degradation under visible‐light illumination. Pristine CN and MoO3 had lower photocatalytic performance, but copolymerized CN materials (CN‐PA200, CN‐PA400, CN‐PA600) and their heterojunction composite materials (CN/MoO3, CN‐PA400/MoO3(3%), CN‐PA400/MoO3(6%), and CN‐PA400/MoO3(9%)) demonstrated substantial enhancements. Of them, CN‐PA400/MoO3(6%) had the greatest H2 production rate of 127.22 μmol/h, almost 6.8 times higher than pure CN. It attained an outstanding MB photodegradation performance of 99.3% in 1 h, demonstrating exceptional stability by maintaining over 95% effectiveness throughout four successive cycles. The exceptional efficiency of CN‐PA400/MoO3(6%) is ascribed to its improved heterojunction design, which improves the separation of charge particles, minimizes recombination, and promotes visible‐light absorption. The band alignment among CN‐PA400 and MoO3 facilitates effective electron transport, whereas the presence of many active sites enhances the photocatalytic processes. These results present significant insights into the development of effective heterojunction photocatalysts and highlight the promise of CN‐PA400/MoO3(6%) for renewable energy generation and environmental cleanup purposes.https://doi.org/10.1002/eom2.70015carbon nitridecopolymerization processheterojunction compositesmolybdenum trioxidephotocatalytic hydrogen evolutionPhotodegradation performance
spellingShingle Junsheng Ye
Abeer M. Beagan
Sheng‐Rong Guo
Asif Hayat
Yasin Orooji
Synergistic Effects in Copolymerized Carbon Nitride/MoO3 Heterojunction Composites for Efficient Visible‐Light‐Driven Photocatalysis
EcoMat
carbon nitride
copolymerization process
heterojunction composites
molybdenum trioxide
photocatalytic hydrogen evolution
Photodegradation performance
title Synergistic Effects in Copolymerized Carbon Nitride/MoO3 Heterojunction Composites for Efficient Visible‐Light‐Driven Photocatalysis
title_full Synergistic Effects in Copolymerized Carbon Nitride/MoO3 Heterojunction Composites for Efficient Visible‐Light‐Driven Photocatalysis
title_fullStr Synergistic Effects in Copolymerized Carbon Nitride/MoO3 Heterojunction Composites for Efficient Visible‐Light‐Driven Photocatalysis
title_full_unstemmed Synergistic Effects in Copolymerized Carbon Nitride/MoO3 Heterojunction Composites for Efficient Visible‐Light‐Driven Photocatalysis
title_short Synergistic Effects in Copolymerized Carbon Nitride/MoO3 Heterojunction Composites for Efficient Visible‐Light‐Driven Photocatalysis
title_sort synergistic effects in copolymerized carbon nitride moo3 heterojunction composites for efficient visible light driven photocatalysis
topic carbon nitride
copolymerization process
heterojunction composites
molybdenum trioxide
photocatalytic hydrogen evolution
Photodegradation performance
url https://doi.org/10.1002/eom2.70015
work_keys_str_mv AT junshengye synergisticeffectsincopolymerizedcarbonnitridemoo3heterojunctioncompositesforefficientvisiblelightdrivenphotocatalysis
AT abeermbeagan synergisticeffectsincopolymerizedcarbonnitridemoo3heterojunctioncompositesforefficientvisiblelightdrivenphotocatalysis
AT shengrongguo synergisticeffectsincopolymerizedcarbonnitridemoo3heterojunctioncompositesforefficientvisiblelightdrivenphotocatalysis
AT asifhayat synergisticeffectsincopolymerizedcarbonnitridemoo3heterojunctioncompositesforefficientvisiblelightdrivenphotocatalysis
AT yasinorooji synergisticeffectsincopolymerizedcarbonnitridemoo3heterojunctioncompositesforefficientvisiblelightdrivenphotocatalysis