Ion irradiation introduced high-density core-shell structured nanoprecipitates in FeCrNi
This study explores the novel synthesis of high-density core-shell structured nanoprecipitates (NPs) within FeCrNi alloys via ion irradiation, aiming to enhance mechanical properties through NPs. We have successfully prepared NPs in FeCrNi with an average diameter of ∼15.2 nm and a number density of...
Saved in:
Main Authors: | , , , , , , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Elsevier
2025-03-01
|
Series: | Journal of Materials Research and Technology |
Subjects: | |
Online Access: | http://www.sciencedirect.com/science/article/pii/S2238785425002753 |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
_version_ | 1823861189428379648 |
---|---|
author | Yizhou Qian Xiaolei Ma Kangkang Wen Siyu Chen Yiheng Chen Yugang Wang Tongde Shen Gang Sha Chenxu Wang |
author_facet | Yizhou Qian Xiaolei Ma Kangkang Wen Siyu Chen Yiheng Chen Yugang Wang Tongde Shen Gang Sha Chenxu Wang |
author_sort | Yizhou Qian |
collection | DOAJ |
description | This study explores the novel synthesis of high-density core-shell structured nanoprecipitates (NPs) within FeCrNi alloys via ion irradiation, aiming to enhance mechanical properties through NPs. We have successfully prepared NPs in FeCrNi with an average diameter of ∼15.2 nm and a number density of ∼2.03 × 1022 m−3 by employing ion irradiation. Transmission Electron Microscopy (TEM) and Atom Probe Tomography (APT) results show the unique core-shell structure of these NPs, consisting of Cr-rich M23C6 carbides cores and Ni-rich shells. The ion irradiation process facilitated the controlled formation of these nanostructures by inducing localized vacancies, which allowed the nucleation and growth of NPs uniformly distributed within the alloy matrix. This synthesis method overcomes traditional limitations posed by thermodynamic constraints and grain boundary (GB) agglomeration, providing a potential pathway for the precise tailoring of microstructures. The combination of APT and TEM analysis offers detailed insight into the structural evolution of the core-shell NPs. These findings represent ion irradiation as an effective technique for fabricating novel nanostructures and hold potential for further improvements in mechanical properties, particularly in the strength, of FeCrNi alloys. Future studies will focus on evaluating the impact of varying irradiation parameters and carbon content on the structural and mechanical characteristics of these alloys. |
format | Article |
id | doaj-art-7b08742f27484021bbd03b2d3e815ca5 |
institution | Kabale University |
issn | 2238-7854 |
language | English |
publishDate | 2025-03-01 |
publisher | Elsevier |
record_format | Article |
series | Journal of Materials Research and Technology |
spelling | doaj-art-7b08742f27484021bbd03b2d3e815ca52025-02-10T04:34:25ZengElsevierJournal of Materials Research and Technology2238-78542025-03-013532363244Ion irradiation introduced high-density core-shell structured nanoprecipitates in FeCrNiYizhou Qian0Xiaolei Ma1Kangkang Wen2Siyu Chen3Yiheng Chen4Yugang Wang5Tongde Shen6Gang Sha7Chenxu Wang8State Key Laboratory of Nuclear Physics and Technology, Center for Applied Physics and Technology, Peking University, Beijing, 100871, ChinaState Key Laboratory of Nuclear Physics and Technology, Center for Applied Physics and Technology, Peking University, Beijing, 100871, China; Corresponding author.Clean Nano Energy Center, State Key Laboratory of Metastable Materials Technology and Science, Yanshan University, Qinhuangdao, 066004, ChinaDepartment of Materials Science and Engineering, Nanjing University of Science and Technology, Nanjing, 210094, ChinaState Key Laboratory of Nuclear Physics and Technology, Center for Applied Physics and Technology, Peking University, Beijing, 100871, ChinaState Key Laboratory of Nuclear Physics and Technology, Center for Applied Physics and Technology, Peking University, Beijing, 100871, ChinaClean Nano Energy Center, State Key Laboratory of Metastable Materials Technology and Science, Yanshan University, Qinhuangdao, 066004, ChinaDepartment of Materials Science and Engineering, Nanjing University of Science and Technology, Nanjing, 210094, ChinaState Key Laboratory of Nuclear Physics and Technology, Center for Applied Physics and Technology, Peking University, Beijing, 100871, China; Corresponding author.This study explores the novel synthesis of high-density core-shell structured nanoprecipitates (NPs) within FeCrNi alloys via ion irradiation, aiming to enhance mechanical properties through NPs. We have successfully prepared NPs in FeCrNi with an average diameter of ∼15.2 nm and a number density of ∼2.03 × 1022 m−3 by employing ion irradiation. Transmission Electron Microscopy (TEM) and Atom Probe Tomography (APT) results show the unique core-shell structure of these NPs, consisting of Cr-rich M23C6 carbides cores and Ni-rich shells. The ion irradiation process facilitated the controlled formation of these nanostructures by inducing localized vacancies, which allowed the nucleation and growth of NPs uniformly distributed within the alloy matrix. This synthesis method overcomes traditional limitations posed by thermodynamic constraints and grain boundary (GB) agglomeration, providing a potential pathway for the precise tailoring of microstructures. The combination of APT and TEM analysis offers detailed insight into the structural evolution of the core-shell NPs. These findings represent ion irradiation as an effective technique for fabricating novel nanostructures and hold potential for further improvements in mechanical properties, particularly in the strength, of FeCrNi alloys. Future studies will focus on evaluating the impact of varying irradiation parameters and carbon content on the structural and mechanical characteristics of these alloys.http://www.sciencedirect.com/science/article/pii/S2238785425002753FeCrNi alloysIon irradiationMicrostructureNanoprecipitatesCore-shell structure |
spellingShingle | Yizhou Qian Xiaolei Ma Kangkang Wen Siyu Chen Yiheng Chen Yugang Wang Tongde Shen Gang Sha Chenxu Wang Ion irradiation introduced high-density core-shell structured nanoprecipitates in FeCrNi Journal of Materials Research and Technology FeCrNi alloys Ion irradiation Microstructure Nanoprecipitates Core-shell structure |
title | Ion irradiation introduced high-density core-shell structured nanoprecipitates in FeCrNi |
title_full | Ion irradiation introduced high-density core-shell structured nanoprecipitates in FeCrNi |
title_fullStr | Ion irradiation introduced high-density core-shell structured nanoprecipitates in FeCrNi |
title_full_unstemmed | Ion irradiation introduced high-density core-shell structured nanoprecipitates in FeCrNi |
title_short | Ion irradiation introduced high-density core-shell structured nanoprecipitates in FeCrNi |
title_sort | ion irradiation introduced high density core shell structured nanoprecipitates in fecrni |
topic | FeCrNi alloys Ion irradiation Microstructure Nanoprecipitates Core-shell structure |
url | http://www.sciencedirect.com/science/article/pii/S2238785425002753 |
work_keys_str_mv | AT yizhouqian ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni AT xiaoleima ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni AT kangkangwen ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni AT siyuchen ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni AT yihengchen ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni AT yugangwang ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni AT tongdeshen ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni AT gangsha ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni AT chenxuwang ionirradiationintroducedhighdensitycoreshellstructurednanoprecipitatesinfecrni |