Novel Composite Materials for Chiral Separation from Cellulose and Barium Sulfate

Cellulose was dissolved in an aqueous solution of sodium hydroxide (NaOH) and urea followed by the addition of barium sulfate (BaSO4) to yield the BaSO4/cellulose composite particles. The morphology, particle size, and BaSO4 content of the composite particles were adjusted by controlling the feed ra...

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Main Authors: Wei Chen, Zhaoqun Wang, Xiaolin Xie, Xingping Zhou, Zheng-Wu Bai
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:International Journal of Polymer Science
Online Access:http://dx.doi.org/10.1155/2013/312615
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author Wei Chen
Zhaoqun Wang
Xiaolin Xie
Xingping Zhou
Zheng-Wu Bai
author_facet Wei Chen
Zhaoqun Wang
Xiaolin Xie
Xingping Zhou
Zheng-Wu Bai
author_sort Wei Chen
collection DOAJ
description Cellulose was dissolved in an aqueous solution of sodium hydroxide (NaOH) and urea followed by the addition of barium sulfate (BaSO4) to yield the BaSO4/cellulose composite particles. The morphology, particle size, and BaSO4 content of the composite particles were adjusted by controlling the feed ratio of cellulose and BaSO4. The cellulose within the composite particles then reacted with 3,5-dimethylphenyl isocyanate. The resulting materials were utilized as the chiral stationary phases (CSPs) whose enantioseparation capabilities were evaluated by various chiral analytes. Due to the mechanical enhancement effect of BaSO4, the composite particles could be applied to the chromatographic packing materials.
format Article
id doaj-art-7a90c1deea024c6ba58966b1206be8e2
institution Kabale University
issn 1687-9422
1687-9430
language English
publishDate 2013-01-01
publisher Wiley
record_format Article
series International Journal of Polymer Science
spelling doaj-art-7a90c1deea024c6ba58966b1206be8e22025-08-20T03:35:41ZengWileyInternational Journal of Polymer Science1687-94221687-94302013-01-01201310.1155/2013/312615312615Novel Composite Materials for Chiral Separation from Cellulose and Barium SulfateWei Chen0Zhaoqun Wang1Xiaolin Xie2Xingping Zhou3Zheng-Wu Bai4Key Lab for Large-Format Battery Materials and Systems, Ministry of Education, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, ChinaKey Laboratory of Green Chemical Process of the Ministry of Education, Hubei Key Laboratory of Novel Chemical Reactor and Green Chemical Technology, Wuhan Institute of Technology, Wuhan 430073, ChinaKey Lab for Large-Format Battery Materials and Systems, Ministry of Education, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, ChinaKey Lab for Large-Format Battery Materials and Systems, Ministry of Education, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, ChinaKey Laboratory of Green Chemical Process of the Ministry of Education, Hubei Key Laboratory of Novel Chemical Reactor and Green Chemical Technology, Wuhan Institute of Technology, Wuhan 430073, ChinaCellulose was dissolved in an aqueous solution of sodium hydroxide (NaOH) and urea followed by the addition of barium sulfate (BaSO4) to yield the BaSO4/cellulose composite particles. The morphology, particle size, and BaSO4 content of the composite particles were adjusted by controlling the feed ratio of cellulose and BaSO4. The cellulose within the composite particles then reacted with 3,5-dimethylphenyl isocyanate. The resulting materials were utilized as the chiral stationary phases (CSPs) whose enantioseparation capabilities were evaluated by various chiral analytes. Due to the mechanical enhancement effect of BaSO4, the composite particles could be applied to the chromatographic packing materials.http://dx.doi.org/10.1155/2013/312615
spellingShingle Wei Chen
Zhaoqun Wang
Xiaolin Xie
Xingping Zhou
Zheng-Wu Bai
Novel Composite Materials for Chiral Separation from Cellulose and Barium Sulfate
International Journal of Polymer Science
title Novel Composite Materials for Chiral Separation from Cellulose and Barium Sulfate
title_full Novel Composite Materials for Chiral Separation from Cellulose and Barium Sulfate
title_fullStr Novel Composite Materials for Chiral Separation from Cellulose and Barium Sulfate
title_full_unstemmed Novel Composite Materials for Chiral Separation from Cellulose and Barium Sulfate
title_short Novel Composite Materials for Chiral Separation from Cellulose and Barium Sulfate
title_sort novel composite materials for chiral separation from cellulose and barium sulfate
url http://dx.doi.org/10.1155/2013/312615
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AT xiaolinxie novelcompositematerialsforchiralseparationfromcelluloseandbariumsulfate
AT xingpingzhou novelcompositematerialsforchiralseparationfromcelluloseandbariumsulfate
AT zhengwubai novelcompositematerialsforchiralseparationfromcelluloseandbariumsulfate