Analysis of metabolic differences in Tibetan medicinal plant Phlomoides rotata leaves in different habitats based on non-targeted metabolomics

Phlomoides rotata, a traditional Tibetan medicinal herb renowned for its anti-inflammatory and analgesic properties, exhibits distinct metabolite profiles across heterogeneous environments. However, the impacts of altitude and slope orientation on its secondary metabolism remain poorly understood. T...

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Main Authors: Lele Wang, Hongli Wang, Junlin Chen, Yuzhen Lamu, Xiangyang Qi, Lei Lei, Kangshan Mao, Sonam Tso
Format: Article
Language:English
Published: Frontiers Media S.A. 2025-04-01
Series:Frontiers in Plant Science
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Online Access:https://www.frontiersin.org/articles/10.3389/fpls.2025.1503218/full
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author Lele Wang
Lele Wang
Hongli Wang
Hongli Wang
Hongli Wang
Junlin Chen
Yuzhen Lamu
Xiangyang Qi
Lei Lei
Kangshan Mao
Kangshan Mao
Sonam Tso
Sonam Tso
author_facet Lele Wang
Lele Wang
Hongli Wang
Hongli Wang
Hongli Wang
Junlin Chen
Yuzhen Lamu
Xiangyang Qi
Lei Lei
Kangshan Mao
Kangshan Mao
Sonam Tso
Sonam Tso
author_sort Lele Wang
collection DOAJ
description Phlomoides rotata, a traditional Tibetan medicinal herb renowned for its anti-inflammatory and analgesic properties, exhibits distinct metabolite profiles across heterogeneous environments. However, the impacts of altitude and slope orientation on its secondary metabolism remain poorly understood. This study aimed to characterize metabolite variations in the leaves of Phlomoides rotata under different elevations and microclimates, providing a mechanistic basis for its quality evaluation and sustainable utilization. Metabolomic analysis was conducted using ultra-high-performance liquid chromatography-quadrupole time-of-flight mass spectrometry (LC-MS). Leaf samples were collected from three altitude gradients (4,300 m, 4,600 m, 5,000 m) and two slope orientations (south vs. north) in Budanla Mountain, Qusong County, Shannan, Xizang Autonomous Region, China. A total of 2,331 metabolites were detected, with lipids (41.93%), organic oxygen compounds (13.95%), and phenylpropanoids (12.4%) dominating the profile. Altitudinal gradients induced significant changes in 5 differentially accumulated metabolites (DAMs), including procyanidin B2 and dihydrocoumarin. Slope orientation influenced 17 DAMs, such as 2,3-secoporrigenin and 2-O-α-D-galactopyranosyl-1-deoxynojirimycin. Kyoto Encyclopedia of Genes and Genomes (KEGG) enrichment analysis revealed altitude-specific enrichment in flavonoid biosynthesis and pantothenate/CoA biosynthesis, while slope-related DAMs were enriched in glycerophospholipid metabolism and galactose metabolism. Altitude-driven increases in flavonoids (e.g., procyanidin B2) likely reflect adaptive responses to UV radiation and oxidative stress. Slope-related metabolite shifts, particularly glycerophospholipids, may relate to microclimate differences in temperature and moisture. These findings highlight the critical role of environmental factors in shaping the metabolic phenotype of Phlomoides rotata, with implications for pharmacologically active compound biosynthesis. The identified DAMs serve as potential biomarkers for quality control, while pathway analysis provides targets for metabolic engineering in conservation and cultivation practices.
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spelling doaj-art-7a2941506fb9417f997706de416120932025-08-20T02:16:21ZengFrontiers Media S.A.Frontiers in Plant Science1664-462X2025-04-011610.3389/fpls.2025.15032181503218Analysis of metabolic differences in Tibetan medicinal plant Phlomoides rotata leaves in different habitats based on non-targeted metabolomicsLele Wang0Lele Wang1Hongli Wang2Hongli Wang3Hongli Wang4Junlin Chen5Yuzhen Lamu6Xiangyang Qi7Lei Lei8Kangshan Mao9Kangshan Mao10Sonam Tso11Sonam Tso12Key Laboratory of Biodiversity and Environment on the Qinghai-Tibetan Plateau, Ministry of Education, School of Ecology and Environment, Xizang University, Lhasa, ChinaLhasa, Urban Wetland Ecosystem, Observation and Research Station of Tibet Autonomous Region, Lhasa, ChinaKey Laboratory of Biodiversity and Environment on the Qinghai-Tibetan Plateau, Ministry of Education, School of Ecology and Environment, Xizang University, Lhasa, ChinaFruit and Vegetable Breeding Laboratory, Qinzhou Branch of Guangxi Academy of Agricultural Sciences/Qinzhou Institute of Agricultural Sciences, Qinzhou, ChinaKey Laboratory of Bio-Resource and Eco-Environment of Ministry of Education, Sichuan Zoige Alpine Wetland Ecosystem National Observation and Research Station, College of Life Sciences, Sichuan University, Chengdu, ChinaKey Laboratory of Biodiversity and Environment on the Qinghai-Tibetan Plateau, Ministry of Education, School of Ecology and Environment, Xizang University, Lhasa, ChinaKey Laboratory of Biodiversity and Environment on the Qinghai-Tibetan Plateau, Ministry of Education, School of Ecology and Environment, Xizang University, Lhasa, ChinaKey Laboratory of Biodiversity and Environment on the Qinghai-Tibetan Plateau, Ministry of Education, School of Ecology and Environment, Xizang University, Lhasa, ChinaKey Laboratory of Biodiversity and Environment on the Qinghai-Tibetan Plateau, Ministry of Education, School of Ecology and Environment, Xizang University, Lhasa, ChinaKey Laboratory of Biodiversity and Environment on the Qinghai-Tibetan Plateau, Ministry of Education, School of Ecology and Environment, Xizang University, Lhasa, ChinaKey Laboratory of Bio-Resource and Eco-Environment of Ministry of Education, Sichuan Zoige Alpine Wetland Ecosystem National Observation and Research Station, College of Life Sciences, Sichuan University, Chengdu, ChinaKey Laboratory of Biodiversity and Environment on the Qinghai-Tibetan Plateau, Ministry of Education, School of Ecology and Environment, Xizang University, Lhasa, ChinaLhasa, Urban Wetland Ecosystem, Observation and Research Station of Tibet Autonomous Region, Lhasa, ChinaPhlomoides rotata, a traditional Tibetan medicinal herb renowned for its anti-inflammatory and analgesic properties, exhibits distinct metabolite profiles across heterogeneous environments. However, the impacts of altitude and slope orientation on its secondary metabolism remain poorly understood. This study aimed to characterize metabolite variations in the leaves of Phlomoides rotata under different elevations and microclimates, providing a mechanistic basis for its quality evaluation and sustainable utilization. Metabolomic analysis was conducted using ultra-high-performance liquid chromatography-quadrupole time-of-flight mass spectrometry (LC-MS). Leaf samples were collected from three altitude gradients (4,300 m, 4,600 m, 5,000 m) and two slope orientations (south vs. north) in Budanla Mountain, Qusong County, Shannan, Xizang Autonomous Region, China. A total of 2,331 metabolites were detected, with lipids (41.93%), organic oxygen compounds (13.95%), and phenylpropanoids (12.4%) dominating the profile. Altitudinal gradients induced significant changes in 5 differentially accumulated metabolites (DAMs), including procyanidin B2 and dihydrocoumarin. Slope orientation influenced 17 DAMs, such as 2,3-secoporrigenin and 2-O-α-D-galactopyranosyl-1-deoxynojirimycin. Kyoto Encyclopedia of Genes and Genomes (KEGG) enrichment analysis revealed altitude-specific enrichment in flavonoid biosynthesis and pantothenate/CoA biosynthesis, while slope-related DAMs were enriched in glycerophospholipid metabolism and galactose metabolism. Altitude-driven increases in flavonoids (e.g., procyanidin B2) likely reflect adaptive responses to UV radiation and oxidative stress. Slope-related metabolite shifts, particularly glycerophospholipids, may relate to microclimate differences in temperature and moisture. These findings highlight the critical role of environmental factors in shaping the metabolic phenotype of Phlomoides rotata, with implications for pharmacologically active compound biosynthesis. The identified DAMs serve as potential biomarkers for quality control, while pathway analysis provides targets for metabolic engineering in conservation and cultivation practices.https://www.frontiersin.org/articles/10.3389/fpls.2025.1503218/fullTibetan medicinePhlomoides rotatametabolomicsaltitude gradientslope directiondifferential metabolites
spellingShingle Lele Wang
Lele Wang
Hongli Wang
Hongli Wang
Hongli Wang
Junlin Chen
Yuzhen Lamu
Xiangyang Qi
Lei Lei
Kangshan Mao
Kangshan Mao
Sonam Tso
Sonam Tso
Analysis of metabolic differences in Tibetan medicinal plant Phlomoides rotata leaves in different habitats based on non-targeted metabolomics
Frontiers in Plant Science
Tibetan medicine
Phlomoides rotata
metabolomics
altitude gradient
slope direction
differential metabolites
title Analysis of metabolic differences in Tibetan medicinal plant Phlomoides rotata leaves in different habitats based on non-targeted metabolomics
title_full Analysis of metabolic differences in Tibetan medicinal plant Phlomoides rotata leaves in different habitats based on non-targeted metabolomics
title_fullStr Analysis of metabolic differences in Tibetan medicinal plant Phlomoides rotata leaves in different habitats based on non-targeted metabolomics
title_full_unstemmed Analysis of metabolic differences in Tibetan medicinal plant Phlomoides rotata leaves in different habitats based on non-targeted metabolomics
title_short Analysis of metabolic differences in Tibetan medicinal plant Phlomoides rotata leaves in different habitats based on non-targeted metabolomics
title_sort analysis of metabolic differences in tibetan medicinal plant phlomoides rotata leaves in different habitats based on non targeted metabolomics
topic Tibetan medicine
Phlomoides rotata
metabolomics
altitude gradient
slope direction
differential metabolites
url https://www.frontiersin.org/articles/10.3389/fpls.2025.1503218/full
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