X-Ray-induced Photochemistry of Hydrocarbons: Implications for the Formation of Organic Haze in (Exo)Planetary Atmospheres

We present a laboratory study of X-ray-induced chemistry of organic molecules (CH _4 , C _2 H _4 , and C _2 H _6 ) irradiated with synchrotron X-rays in the 200–1000 eV range from the Advanced Light Source beamline 9.3.2 at the Lawrence Berkeley National Laboratory. Broadband nonmonochromated X-rays...

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Main Authors: Salma Bejaoui, David Dubois, Slavomir Nemsak, Farid Salama
Format: Article
Language:English
Published: IOP Publishing 2025-01-01
Series:The Planetary Science Journal
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Online Access:https://doi.org/10.3847/PSJ/adf4d3
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author Salma Bejaoui
David Dubois
Slavomir Nemsak
Farid Salama
author_facet Salma Bejaoui
David Dubois
Slavomir Nemsak
Farid Salama
author_sort Salma Bejaoui
collection DOAJ
description We present a laboratory study of X-ray-induced chemistry of organic molecules (CH _4 , C _2 H _4 , and C _2 H _6 ) irradiated with synchrotron X-rays in the 200–1000 eV range from the Advanced Light Source beamline 9.3.2 at the Lawrence Berkeley National Laboratory. Broadband nonmonochromated X-rays beams used in this study partially simulate X-rays emitted from low-mass young stellar objects (0.2–2 keV). The experiment is conducted by irradiating a vacuum chamber prefilled with the selected hydrocarbon at a pressure of 100 mTorr at room temperature during predefined exposure times of 5, 10, 20, and 30 minutes and 1 hr. After each exposure, the chemical photoproducts deposited on Si substrates are analyzed in situ using X-ray photoelectron spectroscopy (XPS). Secondary-ion mass spectrometry is also performed ex situ to determine the hydrogen content of the deposited samples. Our analysis indicates that the photoproducts formed from X-ray irradiation of C _2 H _4 undergo more extensive photoprocessing than those derived from CH _4 and C _2 H _6 . XPS results show that sp ^2 - and sp ^3 -fitted XPS bands correspond to amorphous carbon particles with hybridization that depends on the parent precursor molecules. When irradiating pure CH _4 , a fully sp ^3 -hybridized molecule, we found that X-ray photons induce photochemical reactions leading to the formation of heavier organics with sp ^2 C=C bonds. Possible chemical pathways and astrophysical implications are discussed.
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spelling doaj-art-78db1fda57b3467e97461fb6d766ec962025-08-26T06:25:34ZengIOP PublishingThe Planetary Science Journal2632-33382025-01-016820310.3847/PSJ/adf4d3X-Ray-induced Photochemistry of Hydrocarbons: Implications for the Formation of Organic Haze in (Exo)Planetary AtmospheresSalma Bejaoui0https://orcid.org/0000-0001-8646-9464David Dubois1https://orcid.org/0000-0001-6754-8933Slavomir Nemsak2https://orcid.org/0000-0002-6103-2925Farid Salama3https://orcid.org/0000-0002-6064-4401Space Science & Astrobiology Division, NASA Ames Research Center , Moffett Field, CA 94035, USA; Bay Area Environmental Research Institute , Moffett Field, CA 95476, USASpace Science & Astrobiology Division, NASA Ames Research Center , Moffett Field, CA 94035, USA; Bay Area Environmental Research Institute , Moffett Field, CA 95476, USAAdvanced Light Source, Lawrence Berkeley National Laboratory , Berkeley, CA 94720, USA; Department of Physics and Astronomy, University of California , Davis, CA 95616, USASpace Science & Astrobiology Division, NASA Ames Research Center , Moffett Field, CA 94035, USAWe present a laboratory study of X-ray-induced chemistry of organic molecules (CH _4 , C _2 H _4 , and C _2 H _6 ) irradiated with synchrotron X-rays in the 200–1000 eV range from the Advanced Light Source beamline 9.3.2 at the Lawrence Berkeley National Laboratory. Broadband nonmonochromated X-rays beams used in this study partially simulate X-rays emitted from low-mass young stellar objects (0.2–2 keV). The experiment is conducted by irradiating a vacuum chamber prefilled with the selected hydrocarbon at a pressure of 100 mTorr at room temperature during predefined exposure times of 5, 10, 20, and 30 minutes and 1 hr. After each exposure, the chemical photoproducts deposited on Si substrates are analyzed in situ using X-ray photoelectron spectroscopy (XPS). Secondary-ion mass spectrometry is also performed ex situ to determine the hydrogen content of the deposited samples. Our analysis indicates that the photoproducts formed from X-ray irradiation of C _2 H _4 undergo more extensive photoprocessing than those derived from CH _4 and C _2 H _6 . XPS results show that sp ^2 - and sp ^3 -fitted XPS bands correspond to amorphous carbon particles with hybridization that depends on the parent precursor molecules. When irradiating pure CH _4 , a fully sp ^3 -hybridized molecule, we found that X-ray photons induce photochemical reactions leading to the formation of heavier organics with sp ^2 C=C bonds. Possible chemical pathways and astrophysical implications are discussed.https://doi.org/10.3847/PSJ/adf4d3Astrochemistry
spellingShingle Salma Bejaoui
David Dubois
Slavomir Nemsak
Farid Salama
X-Ray-induced Photochemistry of Hydrocarbons: Implications for the Formation of Organic Haze in (Exo)Planetary Atmospheres
The Planetary Science Journal
Astrochemistry
title X-Ray-induced Photochemistry of Hydrocarbons: Implications for the Formation of Organic Haze in (Exo)Planetary Atmospheres
title_full X-Ray-induced Photochemistry of Hydrocarbons: Implications for the Formation of Organic Haze in (Exo)Planetary Atmospheres
title_fullStr X-Ray-induced Photochemistry of Hydrocarbons: Implications for the Formation of Organic Haze in (Exo)Planetary Atmospheres
title_full_unstemmed X-Ray-induced Photochemistry of Hydrocarbons: Implications for the Formation of Organic Haze in (Exo)Planetary Atmospheres
title_short X-Ray-induced Photochemistry of Hydrocarbons: Implications for the Formation of Organic Haze in (Exo)Planetary Atmospheres
title_sort x ray induced photochemistry of hydrocarbons implications for the formation of organic haze in exo planetary atmospheres
topic Astrochemistry
url https://doi.org/10.3847/PSJ/adf4d3
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AT daviddubois xrayinducedphotochemistryofhydrocarbonsimplicationsfortheformationoforganichazeinexoplanetaryatmospheres
AT slavomirnemsak xrayinducedphotochemistryofhydrocarbonsimplicationsfortheformationoforganichazeinexoplanetaryatmospheres
AT faridsalama xrayinducedphotochemistryofhydrocarbonsimplicationsfortheformationoforganichazeinexoplanetaryatmospheres