Quad-heterostructure precipitation-strengthened high-entropy alloy overcomes strength-ductility trade-off from cryogenic to intermediate temperatures

We use a multi-heterostructure strategy to mitigate temperature-induced brittleness and strain-softening in precipitation-strengthened high-entropy alloys (PSHEAs). A PSHEA consisting of four types of heterostructures, including deformed/recrystallization grains bands inside with irregularly-shaped/...

Full description

Saved in:
Bibliographic Details
Main Authors: J.X. Zhu, Shiwei Wu, C. Ren, Yuefei Jia, B.X. Cao, J.L. Ren, T. Yang, P.K. Liaw, G. Wang
Format: Article
Language:English
Published: Taylor & Francis Group 2025-04-01
Series:Materials Research Letters
Subjects:
Online Access:https://www.tandfonline.com/doi/10.1080/21663831.2025.2465803
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849763246112768000
author J.X. Zhu
Shiwei Wu
C. Ren
Yuefei Jia
B.X. Cao
J.L. Ren
T. Yang
P.K. Liaw
G. Wang
author_facet J.X. Zhu
Shiwei Wu
C. Ren
Yuefei Jia
B.X. Cao
J.L. Ren
T. Yang
P.K. Liaw
G. Wang
author_sort J.X. Zhu
collection DOAJ
description We use a multi-heterostructure strategy to mitigate temperature-induced brittleness and strain-softening in precipitation-strengthened high-entropy alloys (PSHEAs). A PSHEA consisting of four types of heterostructures, including deformed/recrystallization grains bands inside with irregularly-shaped/spheroidal coherent precipitates, and smooth/serrated grain and precipitate-matrix interfaces, is successfully synthesized. The resultant PSHEA exhibits significantly-enhanced strength and uniform elongation simultaneously at −196–700 °C. This overcoming of the strength-ductility trade-off is attributed to a synergistic hetero-deformation-induced strengthening effect, and a two-level strain-delocalization toughening effect. Our findings offer a promising pathway to develop ultra-strong, ductile, and strain-hardenable PSHEAs and superalloys in a wide temperature range.
format Article
id doaj-art-788caf1ef7a446a2b08a32b3d76bebc9
institution DOAJ
issn 2166-3831
language English
publishDate 2025-04-01
publisher Taylor & Francis Group
record_format Article
series Materials Research Letters
spelling doaj-art-788caf1ef7a446a2b08a32b3d76bebc92025-08-20T03:05:27ZengTaylor & Francis GroupMaterials Research Letters2166-38312025-04-0113441141910.1080/21663831.2025.2465803Quad-heterostructure precipitation-strengthened high-entropy alloy overcomes strength-ductility trade-off from cryogenic to intermediate temperaturesJ.X. Zhu0Shiwei Wu1C. Ren2Yuefei Jia3B.X. Cao4J.L. Ren5T. Yang6P.K. Liaw7G. Wang8Institute of Materials, Shanghai University, Shanghai, People’s Republic of ChinaDepartment of Materials·Science and Engineering, City·University·of Hong Kong, Hong Kong, People’s Republic of ChinaInstitute of Materials, Shanghai University, Shanghai, People’s Republic of ChinaInstitute of Materials, Shanghai University, Shanghai, People’s Republic of ChinaSchool·of Materials Science and Engineering, Harbin Institute·of Technology (Shenzhen), Shenzhen, People’s Republic of ChinaSchool of Mathematics·and Statistics, Zhengzhou University, Zhengzhou, People’s Republic of ChinaDepartment of Materials·Science and Engineering, City·University·of Hong Kong, Hong Kong, People’s Republic of ChinaDepartment of Materials Science and Engineering,·The University·of Tennessee, Knoxville, USAInstitute of Materials, Shanghai University, Shanghai, People’s Republic of ChinaWe use a multi-heterostructure strategy to mitigate temperature-induced brittleness and strain-softening in precipitation-strengthened high-entropy alloys (PSHEAs). A PSHEA consisting of four types of heterostructures, including deformed/recrystallization grains bands inside with irregularly-shaped/spheroidal coherent precipitates, and smooth/serrated grain and precipitate-matrix interfaces, is successfully synthesized. The resultant PSHEA exhibits significantly-enhanced strength and uniform elongation simultaneously at −196–700 °C. This overcoming of the strength-ductility trade-off is attributed to a synergistic hetero-deformation-induced strengthening effect, and a two-level strain-delocalization toughening effect. Our findings offer a promising pathway to develop ultra-strong, ductile, and strain-hardenable PSHEAs and superalloys in a wide temperature range.https://www.tandfonline.com/doi/10.1080/21663831.2025.2465803Precipitation-strengthened high-entropy alloymulti-heterostructurestrength-ductility trade-offuniform ductilitywide temperature range
spellingShingle J.X. Zhu
Shiwei Wu
C. Ren
Yuefei Jia
B.X. Cao
J.L. Ren
T. Yang
P.K. Liaw
G. Wang
Quad-heterostructure precipitation-strengthened high-entropy alloy overcomes strength-ductility trade-off from cryogenic to intermediate temperatures
Materials Research Letters
Precipitation-strengthened high-entropy alloy
multi-heterostructure
strength-ductility trade-off
uniform ductility
wide temperature range
title Quad-heterostructure precipitation-strengthened high-entropy alloy overcomes strength-ductility trade-off from cryogenic to intermediate temperatures
title_full Quad-heterostructure precipitation-strengthened high-entropy alloy overcomes strength-ductility trade-off from cryogenic to intermediate temperatures
title_fullStr Quad-heterostructure precipitation-strengthened high-entropy alloy overcomes strength-ductility trade-off from cryogenic to intermediate temperatures
title_full_unstemmed Quad-heterostructure precipitation-strengthened high-entropy alloy overcomes strength-ductility trade-off from cryogenic to intermediate temperatures
title_short Quad-heterostructure precipitation-strengthened high-entropy alloy overcomes strength-ductility trade-off from cryogenic to intermediate temperatures
title_sort quad heterostructure precipitation strengthened high entropy alloy overcomes strength ductility trade off from cryogenic to intermediate temperatures
topic Precipitation-strengthened high-entropy alloy
multi-heterostructure
strength-ductility trade-off
uniform ductility
wide temperature range
url https://www.tandfonline.com/doi/10.1080/21663831.2025.2465803
work_keys_str_mv AT jxzhu quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures
AT shiweiwu quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures
AT cren quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures
AT yuefeijia quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures
AT bxcao quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures
AT jlren quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures
AT tyang quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures
AT pkliaw quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures
AT gwang quadheterostructureprecipitationstrengthenedhighentropyalloyovercomesstrengthductilitytradeofffromcryogenictointermediatetemperatures