Chemical and Sensory Evaluation of Blackberry (<i>Rubus</i> sp.) Juice Concentrated by Reverse Osmosis and Osmotic Evaporation

Blackberry can be considered a source of phenolic compounds with antioxidant properties, especially anthocyanins, which are responsible for the attractive color of the juice. However, blackberry juice quality can be reduced under severe heat treatments, resulting in darkened color and altered taste....

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Main Authors: Juliana Vilar, Flavia Monteiro, Luiz Corrêa-Filho, Flávia Gomes, Renata Tonon, Daniela Freitas-Sá, Suely Freitas, Lourdes Cabral
Format: Article
Language:English
Published: MDPI AG 2025-01-01
Series:Membranes
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Online Access:https://www.mdpi.com/2077-0375/15/1/10
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author Juliana Vilar
Flavia Monteiro
Luiz Corrêa-Filho
Flávia Gomes
Renata Tonon
Daniela Freitas-Sá
Suely Freitas
Lourdes Cabral
author_facet Juliana Vilar
Flavia Monteiro
Luiz Corrêa-Filho
Flávia Gomes
Renata Tonon
Daniela Freitas-Sá
Suely Freitas
Lourdes Cabral
author_sort Juliana Vilar
collection DOAJ
description Blackberry can be considered a source of phenolic compounds with antioxidant properties, especially anthocyanins, which are responsible for the attractive color of the juice. However, blackberry juice quality can be reduced under severe heat treatments, resulting in darkened color and altered taste. Membrane separation processes are an alternative for the clarification and concentration of fruit juices, with advantages as the maintenance of the nutritional, sensory, and functional characteristics of the product. The aim of this work was to evaluate the effect of membrane concentration on the physicochemical and sensory characteristics of blackberry juice. The juice was first clarified by an enzymatic treatment associated with microfiltration and then concentrated by reverse osmosis and osmotic evaporation. Samples were analyzed for pH, titratable acidity, soluble and total solids, phenolic content, antioxidant activity, and total anthocyanins. The concentrated juices were then reconstituted for sensory evaluation. It was verified that reverse osmosis and osmotic evaporation resulted in juices with total solid concentrations of 29 and 53 g∙100 g<sup>−1</sup>, respectively, with slight differences in pH and acidity. Some phenolic compounds were lost during processing. The concentration of anthocyanins and the antioxidant capacity of the osmotic evaporation-concentrated juice increased 6.2 and 7.7 times, respectively, compared to the initial juice. Regarding sensory analysis, the juices concentrated by RO and EO presented acceptance percentages (scores between 6 and 9) of 58% and 55%, respectively. Consumers described them as “good appearance”, “refreshing”, “tasty”, “sweet”, or “with ideal sweetness”, in agreement with the high acceptance scores (6.2 and 6.9, respectively).
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publisher MDPI AG
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series Membranes
spelling doaj-art-7831cb4f12634018afa8ce2988d7720e2025-01-24T13:41:00ZengMDPI AGMembranes2077-03752025-01-011511010.3390/membranes15010010Chemical and Sensory Evaluation of Blackberry (<i>Rubus</i> sp.) Juice Concentrated by Reverse Osmosis and Osmotic EvaporationJuliana Vilar0Flavia Monteiro1Luiz Corrêa-Filho2Flávia Gomes3Renata Tonon4Daniela Freitas-Sá5Suely Freitas6Lourdes Cabral7Postgraduate Program in Food Science (PPGCAL), Federal University of Rio de Janeiro, Cidade Universitária—Ilha do Fundão, Rio de Janeiro 21949-900, RJ, BrazilPostgraduate Program in Food Science (PPGCAL), Federal University of Rio de Janeiro, Cidade Universitária—Ilha do Fundão, Rio de Janeiro 21949-900, RJ, BrazilPostgraduate Program in Food Science and Technology (PPGCTA), Federal Rural University of Rio de Janeiro, BR-465, km 7, Seropédica 23070-200, RJ, BrazilEmbrapa Food Technology—Av. das Américas, 29501, Rio de Janeiro 23020-470, RJ, BrazilEmbrapa Food Technology—Av. das Américas, 29501, Rio de Janeiro 23020-470, RJ, BrazilEmbrapa Food Technology—Av. das Américas, 29501, Rio de Janeiro 23020-470, RJ, BrazilPostgraduate Program in Food Science (PPGCAL), Federal University of Rio de Janeiro, Cidade Universitária—Ilha do Fundão, Rio de Janeiro 21949-900, RJ, BrazilEmbrapa Food Technology—Av. das Américas, 29501, Rio de Janeiro 23020-470, RJ, BrazilBlackberry can be considered a source of phenolic compounds with antioxidant properties, especially anthocyanins, which are responsible for the attractive color of the juice. However, blackberry juice quality can be reduced under severe heat treatments, resulting in darkened color and altered taste. Membrane separation processes are an alternative for the clarification and concentration of fruit juices, with advantages as the maintenance of the nutritional, sensory, and functional characteristics of the product. The aim of this work was to evaluate the effect of membrane concentration on the physicochemical and sensory characteristics of blackberry juice. The juice was first clarified by an enzymatic treatment associated with microfiltration and then concentrated by reverse osmosis and osmotic evaporation. Samples were analyzed for pH, titratable acidity, soluble and total solids, phenolic content, antioxidant activity, and total anthocyanins. The concentrated juices were then reconstituted for sensory evaluation. It was verified that reverse osmosis and osmotic evaporation resulted in juices with total solid concentrations of 29 and 53 g∙100 g<sup>−1</sup>, respectively, with slight differences in pH and acidity. Some phenolic compounds were lost during processing. The concentration of anthocyanins and the antioxidant capacity of the osmotic evaporation-concentrated juice increased 6.2 and 7.7 times, respectively, compared to the initial juice. Regarding sensory analysis, the juices concentrated by RO and EO presented acceptance percentages (scores between 6 and 9) of 58% and 55%, respectively. Consumers described them as “good appearance”, “refreshing”, “tasty”, “sweet”, or “with ideal sweetness”, in agreement with the high acceptance scores (6.2 and 6.9, respectively).https://www.mdpi.com/2077-0375/15/1/10membrane separation processesanthocyaninantioxidant capacitysensory
spellingShingle Juliana Vilar
Flavia Monteiro
Luiz Corrêa-Filho
Flávia Gomes
Renata Tonon
Daniela Freitas-Sá
Suely Freitas
Lourdes Cabral
Chemical and Sensory Evaluation of Blackberry (<i>Rubus</i> sp.) Juice Concentrated by Reverse Osmosis and Osmotic Evaporation
Membranes
membrane separation processes
anthocyanin
antioxidant capacity
sensory
title Chemical and Sensory Evaluation of Blackberry (<i>Rubus</i> sp.) Juice Concentrated by Reverse Osmosis and Osmotic Evaporation
title_full Chemical and Sensory Evaluation of Blackberry (<i>Rubus</i> sp.) Juice Concentrated by Reverse Osmosis and Osmotic Evaporation
title_fullStr Chemical and Sensory Evaluation of Blackberry (<i>Rubus</i> sp.) Juice Concentrated by Reverse Osmosis and Osmotic Evaporation
title_full_unstemmed Chemical and Sensory Evaluation of Blackberry (<i>Rubus</i> sp.) Juice Concentrated by Reverse Osmosis and Osmotic Evaporation
title_short Chemical and Sensory Evaluation of Blackberry (<i>Rubus</i> sp.) Juice Concentrated by Reverse Osmosis and Osmotic Evaporation
title_sort chemical and sensory evaluation of blackberry i rubus i sp juice concentrated by reverse osmosis and osmotic evaporation
topic membrane separation processes
anthocyanin
antioxidant capacity
sensory
url https://www.mdpi.com/2077-0375/15/1/10
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