Ultrasensitive label-free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue-Au NCs

In this work, Au nanoclusters was prepared under the guidance of a synthetic colorant brilliant blue (BB-Au NCs). The microstructure and crystal structure of the resulting products were characterized by transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS). The absorbance...

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Main Authors: Dongning Li, Yanli Liu, Xin Xu, Wenfang Sun, Haiping Ni, Xiangping Liu
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:Sensing and Bio-Sensing Research
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Online Access:http://www.sciencedirect.com/science/article/pii/S2214180425000510
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author Dongning Li
Yanli Liu
Xin Xu
Wenfang Sun
Haiping Ni
Xiangping Liu
author_facet Dongning Li
Yanli Liu
Xin Xu
Wenfang Sun
Haiping Ni
Xiangping Liu
author_sort Dongning Li
collection DOAJ
description In this work, Au nanoclusters was prepared under the guidance of a synthetic colorant brilliant blue (BB-Au NCs). The microstructure and crystal structure of the resulting products were characterized by transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS). The absorbance of BB-Au NCs at 247 nm was enhanced while the absorbance at 308 and 630 nm was reduced by free chlorine, an unavoidable and ubiquitous disinfection byproduct. The optical properties of BB-Au NCs and the influence of free chlorine were analyzed using computational chemistry methods based on density functional theory (DFT). The ratio of absorbance of BB-Au NCs at 247 and 630 nm was used for accurate quantitative determination of free chlorine in a range from 5 to 50 μM, with the detection limit is 1 μM. This method demonstrates potential application for simple and environmentally friendly detection of free chlorine in water samples.
format Article
id doaj-art-77bb8281e46a4f92a22419fce94704f1
institution DOAJ
issn 2214-1804
language English
publishDate 2025-06-01
publisher Elsevier
record_format Article
series Sensing and Bio-Sensing Research
spelling doaj-art-77bb8281e46a4f92a22419fce94704f12025-08-20T03:21:01ZengElsevierSensing and Bio-Sensing Research2214-18042025-06-014810078510.1016/j.sbsr.2025.100785Ultrasensitive label-free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue-Au NCsDongning Li0Yanli Liu1Xin Xu2Wenfang Sun3Haiping Ni4Xiangping Liu5Nanjing Municipal Key Laboratory for Public Health Laboratory Technology, Nanjing Municipal Center for Disease Control and Preventio, Jiangsu, Nanjing 210003, China; Corresponding authors.Department of Pharmacy, Nanjing Drum Tower Hospital, The Affiliated Hospital of Nanjing University Medical School, Jiangsu, Nanjing 210003, ChinaNanjing Municipal Key Laboratory for Public Health Laboratory Technology, Nanjing Municipal Center for Disease Control and Preventio, Jiangsu, Nanjing 210003, ChinaNanjing Municipal Key Laboratory for Public Health Laboratory Technology, Nanjing Municipal Center for Disease Control and Preventio, Jiangsu, Nanjing 210003, ChinaNanjing Municipal Key Laboratory for Public Health Laboratory Technology, Nanjing Municipal Center for Disease Control and Preventio, Jiangsu, Nanjing 210003, ChinaNanjing Municipal Key Laboratory for Public Health Laboratory Technology, Nanjing Municipal Center for Disease Control and Preventio, Jiangsu, Nanjing 210003, China; Corresponding authors.In this work, Au nanoclusters was prepared under the guidance of a synthetic colorant brilliant blue (BB-Au NCs). The microstructure and crystal structure of the resulting products were characterized by transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS). The absorbance of BB-Au NCs at 247 nm was enhanced while the absorbance at 308 and 630 nm was reduced by free chlorine, an unavoidable and ubiquitous disinfection byproduct. The optical properties of BB-Au NCs and the influence of free chlorine were analyzed using computational chemistry methods based on density functional theory (DFT). The ratio of absorbance of BB-Au NCs at 247 and 630 nm was used for accurate quantitative determination of free chlorine in a range from 5 to 50 μM, with the detection limit is 1 μM. This method demonstrates potential application for simple and environmentally friendly detection of free chlorine in water samples.http://www.sciencedirect.com/science/article/pii/S2214180425000510Brilliant blueAu nanoclustersFree chlorine detectionRatio colorimetricMolecular computation
spellingShingle Dongning Li
Yanli Liu
Xin Xu
Wenfang Sun
Haiping Ni
Xiangping Liu
Ultrasensitive label-free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue-Au NCs
Sensing and Bio-Sensing Research
Brilliant blue
Au nanoclusters
Free chlorine detection
Ratio colorimetric
Molecular computation
title Ultrasensitive label-free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue-Au NCs
title_full Ultrasensitive label-free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue-Au NCs
title_fullStr Ultrasensitive label-free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue-Au NCs
title_full_unstemmed Ultrasensitive label-free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue-Au NCs
title_short Ultrasensitive label-free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue-Au NCs
title_sort ultrasensitive label free ratiometric colorimetric sensor for free chlorine detection in tap water based on a novel brilliant blue au ncs
topic Brilliant blue
Au nanoclusters
Free chlorine detection
Ratio colorimetric
Molecular computation
url http://www.sciencedirect.com/science/article/pii/S2214180425000510
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