Analytical QBD Approach to Redefine the Quality of Pharmaceuticals: A Review

As per the present scenario traditional techniques of quality by testing of finished pharmaceutical products have proved to be unsatisfactory, although focus on 'Total quality assurance can be attained only by in-process testing and analysis. The Quality by Design (QbD) idea has alread...

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Main Authors: Shaik Ayesha Ameen, Nagaraju Pappula
Format: Article
Language:English
Published: Krupanidhi College of Pharmacy 2023-12-01
Series:Journal of Pharmaceutical Research
Online Access:https://jopcr.com/articles/analytical-qbd-approach-to-redefine-the-quality-of-pharmaceuticals-a-review
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author Shaik Ayesha Ameen
Nagaraju Pappula
author_facet Shaik Ayesha Ameen
Nagaraju Pappula
author_sort Shaik Ayesha Ameen
collection DOAJ
description As per the present scenario traditional techniques of quality by testing of finished pharmaceutical products have proved to be unsatisfactory, although focus on 'Total quality assurance can be attained only by in-process testing and analysis. The Quality by Design (QbD) idea has already been established and applied in all nations that adhere to the International Conference on Harmonization Guidelines. The proposed ICH Guidelines Q8 for pharmaceutical development, Q9 for quality risk management, and Q10 for pharmaceutical quality systems offer a foundation for incorporating quality into the product. Other components are being added and integrated into the analytical method development process, including as Quality Risk Management, the Pharmaceutical Quality System, and Process Analytical Technology (PAT) guidelines. The Quality by Design (QbD) idea has already been established and applied in all nations that adhere to the International Conference on Harmonization Guidelines. The proposed ICH Guidelines Q8 for pharmaceutical development, Q9 for quality risk management, and Q10 for pharmaceutical quality systems offer a foundation for incorporating quality into the product. Other components are being added and integrated into the analytical method development process, including as Quality Risk Management, the Pharmaceutical Quality System, and Process Analytical Technology (PAT) guidelines. They are widely acknowledged in the business as AQbD (Analytical Quality by Design) ideas. This paper attempts to summarize QbD achievements to date, regulatory perspectives on QbD, a comparative examination of conventional and analytical QbD techniques in method development, and issues about its fundamental application. Keywords Quality by Design, Design of Experiments, Analytical Quality, Critical Quality Attributes Analytical Target Profile, Process Control
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spelling doaj-art-772bd31f380f44b596a45860e9944a3c2025-08-21T09:34:09ZengKrupanidhi College of PharmacyJournal of Pharmaceutical Research0973-72002454-84052023-12-0122417818510.18579/jopcr/v22.4.81Analytical QBD Approach to Redefine the Quality of Pharmaceuticals: A ReviewShaik Ayesha AmeenNagaraju Pappula As per the present scenario traditional techniques of quality by testing of finished pharmaceutical products have proved to be unsatisfactory, although focus on 'Total quality assurance can be attained only by in-process testing and analysis. The Quality by Design (QbD) idea has already been established and applied in all nations that adhere to the International Conference on Harmonization Guidelines. The proposed ICH Guidelines Q8 for pharmaceutical development, Q9 for quality risk management, and Q10 for pharmaceutical quality systems offer a foundation for incorporating quality into the product. Other components are being added and integrated into the analytical method development process, including as Quality Risk Management, the Pharmaceutical Quality System, and Process Analytical Technology (PAT) guidelines. The Quality by Design (QbD) idea has already been established and applied in all nations that adhere to the International Conference on Harmonization Guidelines. The proposed ICH Guidelines Q8 for pharmaceutical development, Q9 for quality risk management, and Q10 for pharmaceutical quality systems offer a foundation for incorporating quality into the product. Other components are being added and integrated into the analytical method development process, including as Quality Risk Management, the Pharmaceutical Quality System, and Process Analytical Technology (PAT) guidelines. They are widely acknowledged in the business as AQbD (Analytical Quality by Design) ideas. This paper attempts to summarize QbD achievements to date, regulatory perspectives on QbD, a comparative examination of conventional and analytical QbD techniques in method development, and issues about its fundamental application. Keywords Quality by Design, Design of Experiments, Analytical Quality, Critical Quality Attributes Analytical Target Profile, Process Controlhttps://jopcr.com/articles/analytical-qbd-approach-to-redefine-the-quality-of-pharmaceuticals-a-review
spellingShingle Shaik Ayesha Ameen
Nagaraju Pappula
Analytical QBD Approach to Redefine the Quality of Pharmaceuticals: A Review
Journal of Pharmaceutical Research
title Analytical QBD Approach to Redefine the Quality of Pharmaceuticals: A Review
title_full Analytical QBD Approach to Redefine the Quality of Pharmaceuticals: A Review
title_fullStr Analytical QBD Approach to Redefine the Quality of Pharmaceuticals: A Review
title_full_unstemmed Analytical QBD Approach to Redefine the Quality of Pharmaceuticals: A Review
title_short Analytical QBD Approach to Redefine the Quality of Pharmaceuticals: A Review
title_sort analytical qbd approach to redefine the quality of pharmaceuticals a review
url https://jopcr.com/articles/analytical-qbd-approach-to-redefine-the-quality-of-pharmaceuticals-a-review
work_keys_str_mv AT shaikayeshaameen analyticalqbdapproachtoredefinethequalityofpharmaceuticalsareview
AT nagarajupappula analyticalqbdapproachtoredefinethequalityofpharmaceuticalsareview