Study on microscopic pore structures and mechanical properties

The pore structures and mechanical properties of coal are key parameters for geological evaluation of coalbed methane, reflecting its reservoir capacity and compressibility. The study investigated four coal samples from the Qinshui and Datong basins in Shanxi Province, including Jurassic coal from D...

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Main Authors: Shihu ZHAO, Yong LI, Yali LIU, Yanbin WANG, Zengqin LIU, Gang CHEN, Xinjun CHEN
Format: Article
Language:zho
Published: Editorial Office of Petroleum Geology and Experiment 2025-01-01
Series:Shiyou shiyan dizhi
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Online Access:https://www.sysydz.net/cn/article/doi/10.11781/sysydz2025010173
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author Shihu ZHAO
Yong LI
Yali LIU
Yanbin WANG
Zengqin LIU
Gang CHEN
Xinjun CHEN
author_facet Shihu ZHAO
Yong LI
Yali LIU
Yanbin WANG
Zengqin LIU
Gang CHEN
Xinjun CHEN
author_sort Shihu ZHAO
collection DOAJ
description The pore structures and mechanical properties of coal are key parameters for geological evaluation of coalbed methane, reflecting its reservoir capacity and compressibility. The study investigated four coal samples from the Qinshui and Datong basins in Shanxi Province, including Jurassic coal from Datong (Ro=0.91%), No. 2 coal from the Shanxi Formation in Gujiao (Ro=1.34%), No. 8 coal of the Taiyuan Formation in Gujiao (Ro=1.70%), and No. 2 coal of the Shanxi Formation in Yicheng (Ro=1.77%). Using atomic force microscopy (AFM), a combined characterization technique was established for microscopic pore structure and mechanical properties based on image segmentation and Derjaguin-Muller-Toporov (DMT) mechanical model. This method clarified the microscopic pore structure and mechanical properties of coal samples and revealed the influence of material composition, pore structure, and thermal evolution level on their microscopic mechanical properties. The results showed that the surface porosity of coal samples mainly ranged from 2.72% to 4.60%, with an average of 3.58%. The total pore surface area and total pore volume were (3.413-5.638)×10-2 μm2/μm2 and (0.5-3.9)×10-4 μm3/μm2, respectively. The pore sizes were mainly distributed between 10-100 nm, and the Young's modulus ranged from 2.24 to 3.10 GPa, with an average of 2.77 GPa. The mechanical properties of coal were influenced by the material composition, pore structure, and thermal evolution level. As moisture decreased and volatile and mineral content increased, the Young's modulus showed an increasing trend. With an increase in surface roughness, mean pore size, porosity surface, specific surface area, and total pore volume, the Young's modulus decreased. As thermal evolution progressed, the Young's modulus decreased. AFM enables simultaneous analysis of microscopic pore structure and mechanical properties of coal, providing new methods and insights for studying reservoir capacity and mechanical behavior of coal reservoirs. It holds significant implications for the evaluation of reservoir capacity and compressibility in unconventional reservoirs.
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spelling doaj-art-7639c01235b546c085a53de21130b1cd2025-02-09T07:48:48ZzhoEditorial Office of Petroleum Geology and ExperimentShiyou shiyan dizhi1001-61122025-01-0147117318310.11781/sysydz2025010173sysydz-47-1-173Study on microscopic pore structures and mechanical propertiesShihu ZHAO0Yong LI1Yali LIU2Yanbin WANG3Zengqin LIU4Gang CHEN5Xinjun CHEN6State Key Laboratory of Shale Oil and Gas Enrichment Mechanisms and Effective Development, Beijing 102206, ChinaChina University of Mining and Technology (Beijing), Beijing 100083, ChinaState Key Laboratory of Shale Oil and Gas Enrichment Mechanisms and Effective Development, Beijing 102206, ChinaChina University of Mining and Technology (Beijing), Beijing 100083, ChinaState Key Laboratory of Shale Oil and Gas Enrichment Mechanisms and Effective Development, Beijing 102206, ChinaState Key Laboratory of Shale Oil and Gas Enrichment Mechanisms and Effective Development, Beijing 102206, ChinaState Key Laboratory of Shale Oil and Gas Enrichment Mechanisms and Effective Development, Beijing 102206, ChinaThe pore structures and mechanical properties of coal are key parameters for geological evaluation of coalbed methane, reflecting its reservoir capacity and compressibility. The study investigated four coal samples from the Qinshui and Datong basins in Shanxi Province, including Jurassic coal from Datong (Ro=0.91%), No. 2 coal from the Shanxi Formation in Gujiao (Ro=1.34%), No. 8 coal of the Taiyuan Formation in Gujiao (Ro=1.70%), and No. 2 coal of the Shanxi Formation in Yicheng (Ro=1.77%). Using atomic force microscopy (AFM), a combined characterization technique was established for microscopic pore structure and mechanical properties based on image segmentation and Derjaguin-Muller-Toporov (DMT) mechanical model. This method clarified the microscopic pore structure and mechanical properties of coal samples and revealed the influence of material composition, pore structure, and thermal evolution level on their microscopic mechanical properties. The results showed that the surface porosity of coal samples mainly ranged from 2.72% to 4.60%, with an average of 3.58%. The total pore surface area and total pore volume were (3.413-5.638)×10-2 μm2/μm2 and (0.5-3.9)×10-4 μm3/μm2, respectively. The pore sizes were mainly distributed between 10-100 nm, and the Young's modulus ranged from 2.24 to 3.10 GPa, with an average of 2.77 GPa. The mechanical properties of coal were influenced by the material composition, pore structure, and thermal evolution level. As moisture decreased and volatile and mineral content increased, the Young's modulus showed an increasing trend. With an increase in surface roughness, mean pore size, porosity surface, specific surface area, and total pore volume, the Young's modulus decreased. As thermal evolution progressed, the Young's modulus decreased. AFM enables simultaneous analysis of microscopic pore structure and mechanical properties of coal, providing new methods and insights for studying reservoir capacity and mechanical behavior of coal reservoirs. It holds significant implications for the evaluation of reservoir capacity and compressibility in unconventional reservoirs.https://www.sysydz.net/cn/article/doi/10.11781/sysydz2025010173surface roughnesspore size distributionyoung's modulusatomic force microscopeimage segmentationcoalbed methane
spellingShingle Shihu ZHAO
Yong LI
Yali LIU
Yanbin WANG
Zengqin LIU
Gang CHEN
Xinjun CHEN
Study on microscopic pore structures and mechanical properties
Shiyou shiyan dizhi
surface roughness
pore size distribution
young's modulus
atomic force microscope
image segmentation
coalbed methane
title Study on microscopic pore structures and mechanical properties
title_full Study on microscopic pore structures and mechanical properties
title_fullStr Study on microscopic pore structures and mechanical properties
title_full_unstemmed Study on microscopic pore structures and mechanical properties
title_short Study on microscopic pore structures and mechanical properties
title_sort study on microscopic pore structures and mechanical properties
topic surface roughness
pore size distribution
young's modulus
atomic force microscope
image segmentation
coalbed methane
url https://www.sysydz.net/cn/article/doi/10.11781/sysydz2025010173
work_keys_str_mv AT shihuzhao studyonmicroscopicporestructuresandmechanicalproperties
AT yongli studyonmicroscopicporestructuresandmechanicalproperties
AT yaliliu studyonmicroscopicporestructuresandmechanicalproperties
AT yanbinwang studyonmicroscopicporestructuresandmechanicalproperties
AT zengqinliu studyonmicroscopicporestructuresandmechanicalproperties
AT gangchen studyonmicroscopicporestructuresandmechanicalproperties
AT xinjunchen studyonmicroscopicporestructuresandmechanicalproperties