Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples

In the present work ordered mesoporous carbon materials soft templating-acidic (STA) were applied as adsorbents in magnetic solid phase extraction technique for isolation of selected phthalates from water samples. STA materials were obtained by soft-templating method in acidic environment. Nickel na...

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Main Authors: Dariusz Wideł, Katarzyna Jedynak, Zygfryd Witkiewicz, Jerzy Oszczudłowski
Format: Article
Language:English
Published: SAGE Publishing 2016-10-01
Series:Adsorption Science & Technology
Online Access:https://doi.org/10.1177/0263617416661333
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author Dariusz Wideł
Katarzyna Jedynak
Zygfryd Witkiewicz
Jerzy Oszczudłowski
author_facet Dariusz Wideł
Katarzyna Jedynak
Zygfryd Witkiewicz
Jerzy Oszczudłowski
author_sort Dariusz Wideł
collection DOAJ
description In the present work ordered mesoporous carbon materials soft templating-acidic (STA) were applied as adsorbents in magnetic solid phase extraction technique for isolation of selected phthalates from water samples. STA materials were obtained by soft-templating method in acidic environment. Nickel nanoparticles were added on the STA synthesis stage, thus the obtained material acquired magnetic properties. The analysis of phthalates after the extraction was carried out by gas chromatography-mass spectrometry method. Fast and easy procedure was elaborated, obtaining recoveries close to 90% for some phthalates.
format Article
id doaj-art-74ef0acd912d40df82dcd0f6efb4ae95
institution DOAJ
issn 0263-6174
2048-4038
language English
publishDate 2016-10-01
publisher SAGE Publishing
record_format Article
series Adsorption Science & Technology
spelling doaj-art-74ef0acd912d40df82dcd0f6efb4ae952025-08-20T02:42:59ZengSAGE PublishingAdsorption Science & Technology0263-61742048-40382016-10-013410.1177/0263617416661333Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samplesDariusz WidełKatarzyna JedynakZygfryd WitkiewiczJerzy OszczudłowskiIn the present work ordered mesoporous carbon materials soft templating-acidic (STA) were applied as adsorbents in magnetic solid phase extraction technique for isolation of selected phthalates from water samples. STA materials were obtained by soft-templating method in acidic environment. Nickel nanoparticles were added on the STA synthesis stage, thus the obtained material acquired magnetic properties. The analysis of phthalates after the extraction was carried out by gas chromatography-mass spectrometry method. Fast and easy procedure was elaborated, obtaining recoveries close to 90% for some phthalates.https://doi.org/10.1177/0263617416661333
spellingShingle Dariusz Wideł
Katarzyna Jedynak
Zygfryd Witkiewicz
Jerzy Oszczudłowski
Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples
Adsorption Science & Technology
title Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples
title_full Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples
title_fullStr Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples
title_full_unstemmed Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples
title_short Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples
title_sort investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples
url https://doi.org/10.1177/0263617416661333
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AT katarzynajedynak investigationofmesoporouscarbonmaterialsbymagneticsolidphaseextractionofselectedphthalatesfromwatersamples
AT zygfrydwitkiewicz investigationofmesoporouscarbonmaterialsbymagneticsolidphaseextractionofselectedphthalatesfromwatersamples
AT jerzyoszczudłowski investigationofmesoporouscarbonmaterialsbymagneticsolidphaseextractionofselectedphthalatesfromwatersamples