SYNTHESIS OF 1, l1-DIHYDROXY-2,2'- (THIODIMETHYLENE) BIS-9(1 OH)-ANTHRONE
An efficient synthesis of the 1,l'-dihydroxy-2,2'-(thiodimethy1ene)bis-9(10H)- anthrone (5) is described. Reaction of 1 -methoxy-2-(bromomethy1)-9,lOanthraquinone (1) with excess sodium sulfide in ethanol, demethylation to the corresponding hydroxy and subsequent selective reduction produc...
Saved in:
| Format: | Article |
|---|---|
| Language: | English |
| Published: |
University of Tehran
1996-06-01
|
| Series: | Journal of Sciences, Islamic Republic of Iran |
| Online Access: | https://jsciences.ut.ac.ir/article_31097_8395b53bded722021abf80cad2cd9ed9.pdf |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| Summary: | An efficient synthesis of the 1,l'-dihydroxy-2,2'-(thiodimethy1ene)bis-9(10H)-
anthrone (5) is described. Reaction of 1 -methoxy-2-(bromomethy1)-9,lOanthraquinone
(1) with excess sodium sulfide in ethanol, demethylation to the
corresponding hydroxy and subsequent selective reduction produced the title compound
in high yield. |
|---|---|
| ISSN: | 1016-1104 2345-6914 |